A kind of preparation method of hydrophobic natural fiber composite lead dioxide anode
A natural fiber and lead dioxide technology, applied in chemical instruments and methods, water/sewage treatment, water/sludge/sewage treatment, etc., can solve the lack of hydrophobic groups on the surface of the electrode, which does not conform to green chemistry, and the catalytic effect is general and other issues, to achieve the effect of long service life, efficiency improvement and energy consumption reduction
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0032] 1) Using a 3mm thick titanium sheet as the substrate, cut the titanium sheet into a size of 4cm×3cm with scissors; use 200-mesh coarse sandpaper and 40-mesh fine sandpaper to smooth the surface of the titanium sheet to remove the surface oxide layer and expose the metallic luster. Put the matrix in 10% sodium hydroxide solution and heat and boil for 10 minutes to remove surface oil; then place it in 10% oxalic acid and heat and boil for 1.5 hours to acid-etch the surface, rinse with deionized water and set aside ;
[0033] 2) Add 55% ethanol and 5% nitric acid to 40% tetrabutyl titanate by volume percentage, stir for 10 minutes until the solution is uniform, and obtain a light yellow precursor solution.
[0034] Immerse the clean and dry flaky titanium substrate into the light yellow precursor solution, ultrasonicate at 200W for 5 minutes, so that the surface of the titanium substrate is evenly covered with the impregnation solution, dry it at room temperature, put it i...
Embodiment 2
[0040] 1) Using a 3mm thick titanium sheet as the substrate, cut the titanium sheet into a size of 4cm×3cm with scissors; use 200-mesh coarse sandpaper and 40-mesh fine sandpaper to smooth the surface of the titanium sheet to remove the surface oxide layer and expose the metallic luster. Put the substrate into 10% by mass fraction of sodium hydroxide solution and heat and boil for 5 minutes to remove surface oil stains; then place it in 10% by mass fraction of oxalic acid and heat and boil for 1 hour to acid-etch the surface, rinse it with deionized water and set aside;
[0041] 2) Add 35% ethanol and 1% nitric acid to 64% tetrabutyl titanate by volume percentage, stir for 15 minutes until the solution is uniform, and obtain a light yellow precursor solution.
[0042] Immerse the clean and dry flaky titanium substrate into the light yellow precursor solution, ultrasonicate at 200W for 15 minutes, so that the surface of the titanium substrate is evenly covered with the impregnat...
Embodiment 3
[0047] 1) Using a 3mm thick titanium sheet as the substrate, cut the titanium sheet into a size of 4cm×3cm with scissors; use 200-mesh coarse sandpaper and 40-mesh fine sandpaper to smooth the surface of the titanium sheet to remove the surface oxide layer and expose the metallic luster. Put the substrate into 10% by mass fraction of sodium hydroxide solution and heat and boil for 7 minutes to remove surface oil stains; then place it in 10% by mass fraction of oxalic acid and heat and boil for 2 hours to acid-etch the surface, rinse it with deionized water and set aside;
[0048] 2) Add 46% ethanol and 4% nitric acid to 50% tetrabutyl titanate by volume percentage, stir for 20 minutes until the solution is uniform, and obtain a light yellow precursor solution.
[0049] Immerse the clean and dry flaky titanium substrate into the light yellow precursor solution, ultrasonicate at 200W for 10 minutes, so that the surface of the titanium substrate is evenly covered with the impregna...
PUM
| Property | Measurement | Unit |
|---|---|---|
| density | aaaaa | aaaaa |
| density | aaaaa | aaaaa |
| density | aaaaa | aaaaa |
Abstract
Description
Claims
Application Information
Login to View More