The invention discloses a preparation method of a high catalytic activity magnetic particle loading 2.5-dimensional
anode. The preparation method comprises the following steps of preparing a titaniumoxide layer on ferroferric
oxide magnetic particles by utilizing a dipping-heat oxidation method firstly, and then further
coating the particles, covered with
titanium oxide, with a
antimony-doped tindioxide layer through the dipping-heat oxidation method to enable the
antimony-doped
tin dioxide layer to be tightly combined with the
titanium oxide layer which is adhered to a magnetic particle substrate to form a
solid solution; and attracting the magnetic particles by adopting the magnetic force to enable the magnetic particles to be adhered to the surface of a
cylindrical electrode to form the 2.5-dimensional magnetic particle loading
anode. According to the preparation method, due to the flexibility of the magnetic force, the magnetic particles on a novel
electrode can be recovered in situ, so that operation is simple; and the experiment condition requirements are relatively low, the technological process is liable to control, and the prepared composite
anode has high electro-catalytic activity, is high in
oxygen evolution potential and long in service life and is suitable for being applied to industrially electrolyzing waste water in a large scale.