Titanium dioxide/polymer composite dielectric hydrophobic material and preparation method thereof
A hydrophobic material, titanium dioxide technology, applied in coatings and other directions, can solve the problems of limited application and low dielectric constant, and achieve the effects of low glass transition temperature, increased dielectric constant, and low dielectric loss
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[0022] (1) 2.5 grams of titanium dioxide, 12.5 milliliters of absolute ethanol, 12.5 milliliters of absolute ethylene glycol, and 100 milliliters of concentration of 10 mol / liter sodium hydroxide are placed in a 200 milliliter hydrothermal reaction kettle, stirred for 10 minutes, and ultrasonically treated for 10 minutes minutes, and stir for another 10 minutes. Then the reaction kettle was put into a blast drying oven to react at a constant temperature of 180°C for 48 hours;
[0023] (2) After the reaction is over, take out the precipitate, soak it with 37wt% concentrated hydrochloric acid for 6 hours, wash the soaked precipitate with deionized water several times, and move it to a 60°C oven for drying to obtain the precursor H 2 Ti 3 o 7 ;
[0024] (3) The precursor H 2 Ti 3 o 7 Burning in the air for 2 hours, the burning temperature is 600°C, and the heating rate is 5°C / min, to obtain white relatively fluffy titanium dioxide powder (its microstructure is linear, such ...
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