One-component polyurethane adhesive for furniture and preparation method of one-component polyurethane adhesive
A polyurethane adhesive, one-component technology, applied in the direction of polyurea/polyurethane adhesives, adhesives, adhesive additives, etc., can solve the problems of difficult pollutant treatment and discharge, human harm, and high content, and achieve flame retardant performance. Good effect of improving antibacterial properties and excellent toughness
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Embodiment 1
[0020] A preparation method of one-component polyurethane adhesive for furniture, comprising the following steps:
[0021] (1) Add graphene oxide and tetraglycidyl ether tetraphenylethane into acetone, stir at reflux for 20 minutes, add glyceryl monostearate and diphenylsilanediol, continue stirring for 10 minutes, and then add paraffin , ammonium hexachloroiridate, stirred for 30 minutes to obtain a functional system;
[0022] (2) Mixing mass concentration of 10% polyvinyl alcohol (the average molecular weight of polyvinyl alcohol is 4800) aqueous solution, tetraphenyl porphyrin iron, hydrogen peroxide, stirred at 80°C for 3 hours, then rotary evaporated to remove water, then added hexaethylene oxide Methyl diisocyanate, 1,3,5-triglycidyl-S-triazinetrione, reflux and stir for 5 minutes, then add glycerol, stir to obtain a modified system;
[0023] (3) After mixing diethylene glycol, o-hydroxybenzoic acid, and N-methylpyrrolidone, stir at 60°C for 1 hour, then add 2-mercaptop...
Embodiment 2
[0027] A preparation method of one-component polyurethane adhesive for furniture, comprising the following steps:
[0028] (1) Add graphene oxide and tetraglycidyl ether tetraphenylethane into acetone, stir at reflux for 20 minutes, add glyceryl monostearate and diphenylsilanediol, continue stirring for 10 minutes, and then add paraffin , ammonium hexachloroiridate, stirred for 30 minutes to obtain a functional system;
[0029] (2) Mixing mass concentration of 10% polyvinyl alcohol (the average molecular weight of polyvinyl alcohol is 4200) aqueous solution, tetraphenyl porphyrin iron, hydrogen peroxide, stirred at 80°C for 3 hours, then rotary evaporated to remove water, then added hexaethylene oxide Methyl diisocyanate, 1,3,5-triglycidyl-S-triazinetrione, reflux and stir for 5 minutes, then add glycerol, stir to obtain a modified system;
[0030](3) After mixing diethylene glycol, o-hydroxybenzoic acid, and N-methylpyrrolidone, stir at 60°C for 1 hour, then add 2-mercaptopy...
Embodiment 3
[0034] A preparation method of one-component polyurethane adhesive for furniture, comprising the following steps:
[0035] (1) Add graphene oxide and tetraglycidyl ether tetraphenylethane into acetone, stir at reflux for 20 minutes, add glyceryl monostearate and diphenylsilanediol, continue stirring for 10 minutes, and then add paraffin , ammonium hexachloroiridate, stirred for 30 minutes to obtain a functional system;
[0036] (2) Mixing mass concentration of 10% polyvinyl alcohol (the average molecular weight of polyvinyl alcohol is 4800) aqueous solution, tetraphenyl porphyrin iron, hydrogen peroxide, stirred at 80°C for 3 hours, then rotary evaporated to remove water, then added hexaethylene oxide Methyl diisocyanate, 1,3,5-triglycidyl-S-triazinetrione, reflux and stir for 5 minutes, then add glycerol, stir to obtain a modified system;
[0037] (3) After mixing diethylene glycol, o-hydroxybenzoic acid, and N-methylpyrrolidone, stir at 60°C for 1 hour, then add 2-mercaptop...
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