Biodegradable mulch film capable of weeding
A technology of biodegradation and mulching, which is applied in the direction of weed elimination equipment, plant protection, plant protection cover, etc., can solve the problem of not having the function of weeding, and achieve the improvement of tear propagation, mechanical strength and transparency, and production The effect of simple process
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Embodiment 1
[0024] 1. First resin synthesis
[0025] Mix 1.00 mol of terephthalic acid, 1.5 mol of adipic acid, 3.0 mol of 1,4-butanediol, 0.05 mol of glycerol and 0.2 mol of pentaerythritol to obtain a slurry. The slurry in the raw material storage tank is continuously transported to the esterification reactor through the raw material transport pipeline, and at the same time, a solution containing 0.007mol tetrabutyl titanate at 75°C is transported from the catalyst pipeline. The internal reaction temperature of the esterification reactor is 230°C, and the atmospheric pressure nitrogen atmosphere collects the esterification water and by-products and the remaining polymerized monomer mixture and the rectification tower container through the pipeline, and keeps the system stable until the esterification rate reaches 90. % or more, reduce the pressure to 100Pa, increase the temperature to 250°C, and continue the reaction for 3 hours. After the end of the melt polycondensation, add the firs...
Embodiment 2
[0035] 1. First resin synthesis
[0036] Mix 1.00 mol of terephthalic acid, 1.5 mol of adipic acid, 3.0 mol of 1,4-butanediol, 0.05 mol of pentaerythritol and 0.2 mol of trimethylolethane to obtain a slurry. The raw material is transported to the raw material storage tank at 70°C, and the slurry in the raw material storage tank is continuously transported to the esterification reactor through the raw material delivery pipeline. At the same time, a solution containing 0.007mol tetrabutyl titanate is transported from the catalyst pipeline . The internal reaction temperature of the esterification reactor is 160°C, and the atmospheric pressure nitrogen atmosphere collects the esterification water and by-products and the remaining polymerized monomer mixture and the rectification tower container through the pipeline, and keeps the system stable until the esterification rate reaches 90. % or more, reduce the pressure to 100Pa, increase the temperature to 250°C, and continue the rea...
Embodiment 3
[0046] 1. First resin synthesis
[0047] The terephthalic acid that is equivalent to 1.00mol, the adipic acid of 1.5mol, the 1,4-butanediol of 3.0mol, the glycerin of 0.5mol and the sorbitol of 0.2mol are mixed to obtain slurry, and slurry is in 70 ℃ to the raw material storage tank, the slurry in the raw material storage tank is continuously transported to the esterification reactor through the raw material delivery pipeline, and at the same time, a solution containing 0.015mol tetrabutyl titanate at 75 ℃ is transported from the catalyst pipeline. The internal reaction temperature of the esterification reactor is 250°C, and the atmospheric pressure nitrogen atmosphere collects the esterification water and by-products and the remaining polymerized monomer mixture and the rectification tower container through the pipeline, and keeps the system stable until the esterification rate reaches 90. % or more, reduce the pressure to 100Pa, increase the temperature to 250°C, and continu...
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