Mongolian drug compound preparation for treating insomnia and preparation method thereof
A technology of compound preparations and Mongolian medicines, which is applied in the direction of medical formulas, medical preparations with non-active ingredients, medical preparations containing active ingredients, etc., can solve the problems of patient dependence and unsatisfactory treatment effects, and achieve the reduction of ingestion of drugs time, good linear relationship, and strong specificity
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[0084] Solution preparation:
[0085] (1) Preparation of internal standard solution: Accurately weigh an appropriate amount of cyclohexanone, add n-hexane to make an internal standard solution containing 50 mg of n-hexane per 1 mL.
[0086] (2) Preparation of reference substance solution: Take an appropriate amount of eucalyptol reference substance, weigh it accurately, add n-hexane to make a solution containing 25mg of n-hexane per 1mL, and add 1mL of internal standard solution.
[0087] (3) Preparation of the test solution: Take 5g of the Mongolian medicine compound preparation, weigh it accurately, add 200mL of water to the round bottom flask, connect the volatile oil measuring device, add water from the upper end of the measuring device to the scale of 3mL, add 2-3mL of n-hexane, Connect the reflux condenser, heat to a slight boil, and keep it for 2 hours, let it cool, separate the n-hexane liquid, filter it through a funnel covered with 1g of anhydrous sodium sulfate, put...
Embodiment 1
[0096] A Mongolian medicine compound preparation for treating insomnia. The Mongolian medicine compound preparation is a solid granule prepared from the Mongolian medicine compound composition. The preparation method specifically includes the following steps:
[0097] Crushing of the original drug: take 1 part of Longan longan, 2 parts of Baiju Sheng, 3 parts of white cardamom, and 6 parts of fried jujube, and then pulverize and pass through a 24-mesh sieve to make the coarse powder of the original drug;
[0098] Coarse powder extraction of the original drug: Take 1 part of the coarse powder of the original drug, add 10 parts of water, mix well, soak for 2 hours, then extract by steam distillation for 4-8 hours, collect the volatile oil and the extraction filtrate of the original drug;
[0099] Inclusion of volatile oil: Grinding method: take volatile oil and β-CD and mix them evenly at a ratio of 1:10, add 3 times the amount of water to grind for 80 minutes, filter with suctio...
Embodiment 2
[0105] A Mongolian medicine compound preparation for treating insomnia. The Mongolian medicine compound preparation is a solid granule prepared from the Mongolian medicine compound composition. The preparation method specifically includes the following steps:
[0106] Crushing of the original drug: take 3 parts of longan longan, 4 parts of white lettuce, 6 parts of white cardamom, and 12 parts of fried jujube, and pulverize and pass through a 24-mesh sieve to make the coarse powder of the original drug;
[0107] Coarse powder extraction of the original drug: take 1 part of the coarse powder of the original drug, add 9 parts of water, mix well, soak for 3 hours, then extract by steam distillation for 5 hours, collect the volatile oil and the extraction filtrate of the original drug;
[0108] Inclusion of volatile oil: Grinding method: mix volatile oil and β-CD at a ratio of 1:9, add 3.5 times the amount of water to grind for 90 minutes, filter with suction, wash the filter resid...
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