Preparation method of high-strength compound glass
A composite glass and high-strength technology, which is applied in the field of glass manufacturing, can solve the problems of complex manufacturing process and low decoration, and achieve the effect of good decoration, wide application and increased strength
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Embodiment 1
[0022] A preparation method of high-strength composite glass, comprising the following steps:
[0023] (1) First, by weight parts of SiO2, 12 parts of Al2O3, 22 parts of CaO, 2 parts of MgO, 12 parts of B2O3, 3 parts of Na2CO3, 2 parts of Na2O, 0.4 parts of Y2O3, Mix 0.6 parts of Sb2O3 evenly and grind to form a mixed powder. Heat the mixed powder to 1580°C to melt it completely to obtain molten glass. Pour the molten glass into water and quench it. Take out the quenched glass and grind it. Dry at 180°C after 800 mesh sieve to obtain glass powder;
[0024] (2) Add nano-ZrO2 to 50% ethanol aqueous solution, add silane coupling agent and ultrasonically disperse for 1 hour, add dropwise citric acid to adjust the pH to 3-5, heat up to 45°C and stir for 3 hours, then suction filter, filter The cake was vacuum-dried for 2 hours to obtain a modified silane coupling agent;
[0025] (3) Add BPO, modified silane coupling agent and methyl methacrylate to distilled water and raise the t...
Embodiment 2
[0028] A preparation method of high-strength composite glass, comprising the following steps:
[0029] (1) First, by weight parts of SiO2, 10 parts of Al2O3, 20 parts of CaO, 4 parts of MgO, 15 parts of B2O3, 2 parts of Na2CO3, 5 parts of Na2O, 0.5 parts of Y2O3, Mix 0.5 parts of Sb2O3 evenly and grind to form a mixed powder. Heat the mixed powder to 1600°C to melt it completely to obtain molten glass. Pour the molten glass into water and quench it. Take out the quenched glass and grind it. Dry at 160°C after 800 mesh sieve to obtain glass powder;
[0030] (2) Add nano-ZrO2 to 60% ethanol aqueous solution, add silane coupling agent and ultrasonically disperse for 1 hour, add dropwise citric acid to adjust the pH to 3-5, heat up to 48° C. and stir for 3 hours before suction filtration, and The cake was vacuum-dried for 3 hours to obtain a modified silane coupling agent;
[0031] (3) Add BPO, modified silane coupling agent and methyl methacrylate to distilled water and raise t...
Embodiment 3
[0034] A preparation method of high-strength composite glass, comprising the following steps:
[0035] (1) First, by weight parts of SiO2, 14 parts of Al2O3, 23 parts of CaO, 4 parts of MgO, 15 parts of B2O3, 5 parts of Na2CO3, 1 part of Na2O, 0.1 part of Y2O3, Mix 0.5 parts of Sb2O3 evenly and grind to form a mixed powder. Heat the mixed powder to 1560°C to melt it completely to obtain molten glass. Pour the molten glass into water and quench it. Take out the quenched glass and grind it. Dry at 150°C after 800 mesh sieve to obtain glass powder;
[0036] (2) Add nano-ZrO2 to 40% ethanol aqueous solution, add silane coupling agent and ultrasonically disperse for 1 hour, add dropwise citric acid to adjust the pH to 3-5, heat up to 50°C and stir for 4 hours, then suction filter, filter The cake was vacuum-dried for 2 hours to obtain a modified silane coupling agent;
[0037] (3) Add BPO, modified silane coupling agent and methyl methacrylate to distilled water and raise the tem...
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