Preparation method of pouring material with high dielectric property
A casting material and high-dielectric technology, which is applied in the field of preparation of high-dielectric performance casting materials, can solve problems such as development and application limitations, and achieve the effects of uniform cross-linking structure, good mechanical properties and reasonable composition.
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[0021] A method for preparing a casting material with high dielectric properties, comprising the following steps:
[0022] (1) Disperse manganese nitrate hexahydrate, cobalt nitrate hexahydrate and ferric chloride in deionized water, stir at 110 ° C for 45 minutes to obtain a precursor system; then filter the precursor system to obtain a precursor; then pass the precursor through Drying and calcination to obtain high dielectric fillers; the drying is drying at 105°C under vacuum; the calcination is calcination at 1150°C for 3 hours under a hydrogen / argon mixed atmosphere; the volume ratio of hydrogen / argon is 0.5:10 ;
[0023] (2) At room temperature, mix 3,3'-dithiodipropionic acid, dichloromethane, and acetone; then add pyridinium m-nitrobenzenesulfonate and diphenyl phosphate, stir for 10 minutes, then add methylbutyne Alcohol, after stirring for 35 minutes, add 2,3-epoxycyclopentyl cyclopentyl ether, after stirring for 50 minutes, add benzylidene aniline, and continue sti...
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