Separator for non-aqueous secondary battery and non-aqueous secondary battery
A secondary battery, non-aqueous technology, applied in the field of non-aqueous secondary battery separators and non-aqueous secondary batteries, can solve the problems of decreased cycle life, blocked surface pores of the separator, increased internal resistance of the battery, etc. Good adhesion, excellent adhesion, and excellent cycle characteristics
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Embodiment 1
[0211] At room temperature, polyvinylidene fluoride resin (VDF-HFP copolymer, HFP unit content is 12.4% by mass, weight average molecular weight is 860,000), maleic anhydride modified acrylic resin (methyl methacrylate-benzene Tertiary copolymer of ethylene-maleic anhydride, the polymerization ratio [mass ratio] is 10:70:20, the weight-average molecular weight is 113,000, and the glass transition temperature is 130°C), and polyvinyl alcohol-based resin (JAPAN VAM&POVAL CO .,LTD. 10MZ, the degree of polymerization is 250, the degree of saponification is 70 mol%) dissolved in a mixed solvent of dimethylacetamide and tripropylene glycol (dimethylacetamide:tripropylene glycol=80:20 [mass ratio] ), and reacted at 80° C. for 2 hours to prepare a coating liquid for forming an adhesive porous layer. The mass ratio of polyvinylidene fluoride-based resin, polyvinyl alcohol-based resin, and maleic anhydride-modified acrylic resin contained in the coating liquid was 80:18:2, and the resin...
Embodiment 2
[0214] As the maleic anhydride-modified acrylic resin, it was changed to a ternary copolymer of methyl methacrylate-styrene-maleic anhydride (the polymerization ratio [mass ratio] is 30:50:20, the weight average molecular weight is 130,000, and the glass Transition temperature is 115° C.), except that, it was carried out in the same manner as in Example 1 to produce a separator.
Embodiment 3
[0216] As the polyvinyl alcohol-based resin, it was changed to a binary copolymer of vinyl acetate and ethoxydiethylene glycol acrylate (the polymerization ratio [mass ratio] is 90:10, the degree of polymerization is 1000, and the degree of saponification is 98 mol % ), except that, the same operation as in Example 1 was performed to produce a separator.
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