Method for preparing carbon-copper-coated ferroferric oxide composite magnetic oil removal particles

A technology of ferroferric oxide and composite magnetism, applied in chemical instruments and methods, separation methods, alkali metal compounds, etc., can solve the problems of high cost of polymer compounds, inability to produce in large quantities, cumbersome preparation process, etc., and achieve stable carbon layer , efficient recovery, and strong controllability

Active Publication Date: 2018-09-25
SHENYANG POLYTECHNIC UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, most of the auxiliary materials used to synthesize them are high-molecular compounds with high cost, cumbersome preparation process, poor temperature resistance, and cannot be mass-produced

Method used

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  • Method for preparing carbon-copper-coated ferroferric oxide composite magnetic oil removal particles
  • Method for preparing carbon-copper-coated ferroferric oxide composite magnetic oil removal particles
  • Method for preparing carbon-copper-coated ferroferric oxide composite magnetic oil removal particles

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Experimental program
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Effect test

Embodiment 1

[0037] Such as figure 1 as shown, figure 1 is Fe 3 o 4 Flow chart of the preparation of @C / Cu composite magnetic degreasing particles.

[0038]In the preparation of 0.1mol / L citric acid modified solution, first weigh 0.600g of citric acid with an electronic balance and put it into a beaker, then add 20ml of distilled water and 4ml of absolute ethanol, put the beaker into a water bath heating pot at 60°C Heat the water for 5-10 minutes and stir until it is completely dissolved until the solution is clear to obtain a 0.1mol / L citric acid modified solution.

[0039] When preparing a saturated glucose solution, first weigh 15.0-20.0g of glucose with an electronic balance and put it into another beaker, then add 15-20ml of distilled water, put the beaker into a water-bath heating pot, heat it at 60°C and stir it. It dissolved completely until the solution was clear, giving a saturated glucose solution.

[0040] When preparing the Span-60 solution, first weigh 0.8-1.0g Span-60 ...

Embodiment 2

[0057] A method for preparing carbon copper-coated ferric oxide composite magnetic degreasing particles, characterized in that: the specific steps of the method are as follows:

[0058] Step 1: Prepare 0.1mol / L citric acid modification solution: distilled water and absolute ethanol are prepared as a solvent in a volume ratio of 4:1, heated in a water bath at 50°C for 5 minutes, and stirred until completely dissolved to obtain 0.1mol / L citric acid modified solution;

[0059] Step 2: Prepare a saturated glucose solution: at room temperature, weigh 15.0 g of glucose and put it into a beaker, add 15 ml of distilled water, heat and stir in a water bath at 50°C to completely dissolve until the solution is clear, and obtain a saturated glucose solution;

[0060] Step 3: Prepare Sipan-60 solution: prepare Sipan-60 solution with a concentration of 0.4g / mL, heat in a water bath at 50°C for 5min, stir until completely dissolved, and obtain a Sipan-60 solution with a concentration of 0.4g...

Embodiment 3

[0075] A method for preparing carbon copper-coated ferric oxide composite magnetic degreasing particles, characterized in that: the specific steps of the method are as follows:

[0076] Step 1: Prepare 0.1mol / L citric acid modification solution: distilled water and absolute ethanol are prepared as a solvent in a volume ratio of 4:1, heat in a water bath at 70°C for 10 minutes, stir until completely dissolved, and obtain 0.1mol / L citric acid modified solution;

[0077] Step 2: Prepare a saturated glucose solution: at room temperature, weigh 20.0 g of glucose and put it into a beaker, add 20 ml of distilled water, heat and stir in a water bath at 70°C to completely dissolve until the solution is clear, and obtain a saturated glucose solution;

[0078] Step 3: Prepare Sipan-60 solution: prepare Sipan-60 solution with a concentration of 0.5g / mL, heat in a water bath at 70°C for 10min, stir until completely dissolved, and obtain a Sipan-60 solution with a concentration of 0.5g / mL; ...

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Abstract

The invention discloses a method for preparing carbon-copper-coated ferroferric oxide composite magnetic oil removal particles. The method comprises the following steps of modifying ferroferric oxide,introducing a carbon source, adding a lubricant, an emulsifying and thickening agent and a stabilizer, and then carrying out heat treatment so as to prepare the Fe3O4@C/Cu composite magnetic oil removal particles. The method has the advantages that the technical problems that a floating oil cleaning technology is tedious in preparation process, incapable of realizing mass production and the likecan be solved; and the particles prepared through the method is high in surface carbonization degree and stable in carbon layer, mass production can be realized, and the good particle preparation method solves the problem of floating oil on the water surface.

Description

Technical field: [0001] The invention belongs to the field of nanometer preparation, and in particular relates to a method for preparing carbon copper-coated ferric oxide composite magnetic degreasing particles. Background technique: [0002] During the production, transportation, storage, refining and use of petroleum, it will cause environmental pollution, especially water surface pollution. With the increasingly stringent water quality standards and regulations, the cleaning technology of oil slicks on the water surface has become more and more comprehensive. However, it is still a technical problem to effectively solve large-area oil layers with a thickness less than 50 μm. Nano-iron oxide materials that have high hydrophobicity and high lipophilicity through surface modification or combination with functional materials and can overcome viscous resistance, surface tension and gravity to recover from water surface under external magnetic field have become the first choice...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01J20/28B01J20/06B01J20/20B01J20/02B01D17/022C02F1/40
CPCB01D17/0202B01J20/02B01J20/06B01J20/20B01J20/28009C02F1/40
Inventor 刘泰奇李志杰史桂梅陈旭陈鑫力李懿霖王晓燕
Owner SHENYANG POLYTECHNIC UNIV
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