A monolithic integrated green pulse laser based on neodymium doped yttrium vanadate and potassium titanium oxyphosphate bonding crystal and preparation method thereof
A technology of potassium titanyl phosphate and pulsed laser, applied in lasers, laser parts, phonon exciters, etc., to achieve the effect of high conversion efficiency, good beam quality and long life
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Embodiment 1
[0038] Such as figure 1 , 2 As shown, the preparation of a monolithic integrated green pulsed laser based on neodymium-doped yttrium vanadate and potassium titanyl phosphate cemented crystals includes the following steps:
[0039] (1) cut Nd:YVO with a 4 Crystal 2 is used as the substrate, and the surface perpendicular to the a-axis of the crystal is polished, and the polished sample is ultrasonically cleaned with 99.7% alcohol to remove impurities on the polished surface to obtain a polished surface;
[0040] (2) Using an ion beam accelerator, silver ions 1 are implanted into the polished surface of the crystal along the direction of the vertical direction of the a-axis beam exit surface at an angle of 7°; the implantation energy is 180 kiloelectron volts (keV), and the implantation dose is 7×10 16 ions / cm 2 ; Make silver ions distributed in the range of 200nm below the crystal surface;
[0041] (3) Perform annealing treatment 3 on the sample implanted with silver ions, fir...
Embodiment 2
[0046] The preparation of a monolithic integrated green pulsed laser based on neodymium-doped yttrium vanadate and potassium titanyl phosphate cemented crystals includes the following steps:
[0047] (1) cut Nd:YVO with a 4 Crystal 2 is used as the substrate, and the surface perpendicular to the a-axis of the crystal is polished, and the polished sample is ultrasonically cleaned with 99.7% alcohol to remove impurities on the polished surface to obtain a polished surface;
[0048] (2) Using an ion beam accelerator, implant silver ions 1 into the crystal polishing surface along the vertical direction of the a-axis beam exit surface or the direction at an angle of 7°; the implantation energy is 120 kiloelectron volts (keV), and the implantation dose is 5×10 16 ions / cm 2 ; Make silver ions distributed in the range of 150nm below the crystal surface;
[0049] (3) Perform annealing treatment 3 on the sample implanted with silver ions, first raise the temperature to 1000° C. for 6 ...
Embodiment 3
[0054] The preparation of a monolithic integrated green pulsed laser based on neodymium-doped yttrium vanadate and potassium titanyl phosphate cemented crystals includes the following steps:
[0055] (1) cut Nd:YVO with a 4 Crystal 2 is used as the substrate, and the surface perpendicular to the a-axis of the crystal is polished, and the polished sample is ultrasonically cleaned with 99.7% alcohol to remove impurities on the polished surface to obtain a polished surface;
[0056] (2) Using an ion beam accelerator, gold ions are implanted into the crystal polishing surface along the vertical direction of the a-axis beam exit surface or the direction at an angle of 7°; the implantation energy is 180 kiloelectron volts (keV), and the implantation dose is 7×10 16 ions / cm 2 ; Make gold ions distributed in the range of 200nm below the crystal surface;
[0057] (3) Perform annealing treatment 3 on the sample implanted with gold ions, first raise the temperature for 6 hours to 1000°...
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