Compound wax microemulsion composition, and preparation method and application thereof
A technology of microemulsion and composition, which is applied in the direction of plant fibers, textiles and papermaking, and improved hand-feeling fibers, can solve the problems of reducing the dynamic friction coefficient of yarn, affecting the post-treatment of yarn, and reducing the number of warp breaks, etc., to achieve reduction Coefficient of dynamic friction, excellent hydrophilicity, and the effect of improving smoothness
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[0034] The preparation method of described hyperbranched quaternary ammonium salt softener is:
[0035] A) Stir and heat chloroacetyl chloride to 60-90°C, blow nitrogen gas, slowly add hyperbranched polyamide (Hybrane S1200, Hybrane P / S80 1200, etc., purchased from Shanghai Xibao Biology), and react for 4-6 hours;
[0036] B) Add C to A) 10 -C 18 Saturated alkyl tertiary amine, using ethyl acetate as a solvent, reacting at 60-70°C for 10-12 hours, then recrystallizing three times with a mixed solvent of ethyl acetate and ethanol to obtain a hyperbranched quaternary ammonium salt softener.
[0037] In a preferred embodiment, the emulsifier is fatty alcohol polyoxyethylene ether (EO number 3-20), fatty amine polyoxyethylene ether (EO number 4-10), cardanol surfactant, and The amount of fatty alcohol polyoxyethylene ether: fatty amine polyoxyethylene ether: cardanol surfactant is 1.5-4:1-3:1-3, preferably 1.8-3:1.2-2.5:0.4-1.
[0038] In a more preferred embodiment, the cardan...
Embodiment
[0049] Below in conjunction with specific embodiment, further illustrate the present invention. It should be understood that these examples are only used to illustrate the present invention and not to limit the present invention. In addition, it should be understood that after reading the teachings of the present invention, those skilled in the art can make various changes or modifications to the present invention, and these equivalent forms also fall within the scope defined by the appended claims of the present application.
[0050] The application performance of the composite wax microemulsion of the present invention is verified by the following experiments.
[0051] 1 Experiment content
[0052] 1.1 Textiles: cotton yarn, cotton knitted fabric
[0053] 1.2 Wax emulsion: domestic product S, foreign product P, wax emulsion of the present invention
[0054] 1.3 Application process:
[0055] Cotton yarn:
[0056] 2% owf working solution, acetic acid to adjust the pH valu...
preparation Embodiment 2
[0079] Preparation Example 2 - hyperbranched quaternary ammonium salt softener 2:
[0080] A) Stir and heat 20g of chloroacetyl chloride to about 90°C, blow nitrogen gas, slowly add 25g of hyperbranched polyamide (Hybrane P / S80 1200, purchased from Shanghai Xibao Biotechnology Co., Ltd.), and react for 6h;
[0081] B) Add 18g of dodecyl diethylamine to A), use 250mL of ethyl acetate as solvent, react at 60°C for 12h, recrystallize 3 times with a mixed solvent of ethyl acetate and ethanol, and obtain 45g of hyperbranched Quaternary ammonium softener 2. The measured melting point of the product is 115-117° C., and the molecular weight is about 3100.
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