a b 4 C fiber mat and preparation method thereof
A technology of fiber felt and activated carbon fiber felt, which is applied in the field of B4C fiber felt and its preparation, can solve the problems of complex production process, high cost of reaction equipment, long cycle, etc., and achieve complete reaction process, easy control of reaction process and easy price Effect
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Embodiment 1
[0032] This embodiment adopts activated carbon fiber felt (carbon content ≥ 90.0%, Jiangsu Sutong Carbon Fiber Co., Ltd.), magnesium powder (purity ≥ 99.9%, Changsha Tianjiu Metal Material Co., Ltd.) and diboron trioxide (purity ≥ 98.8%, Xi’an City You Li Electronic Chemical Co., Ltd.) as raw material, anhydrous MgCl 2 (Tianjin Fuchen Chemical Reagent Factory) is molten salt. According to the mass percentage, the active carbon fiber felt in the raw material is 4.1%, the diboron trioxide in the raw material is 47.3%, the magnesium powder in the raw material is 48.6%, and the raw material and MgCl 2 The mass ratio is 1:4.
[0033] (1) As attached figure 2 , according to the above mass percentage, grind and mix the weighed boron trioxide and magnesium powder in a mortar; MgCl 2 Add in the mixture of boron trioxide and magnesium powder for mixing; weigh half of the mass of boron trioxide, magnesium powder and MgCl 2 The mixture is placed in the crucible, and then the activated...
Embodiment 2
[0038] With embodiment 1, but different from embodiment 1 is Na 2 B 4 o 7 It is molten salt, calculated by mass percentage, activated carbon fiber mat is 3% in the raw material, diboron trioxide is 42% in the raw material, magnesium powder is 55% in the raw material, the raw material and Na 2 B 4 o 7 The mass ratio is 1:3.
Embodiment 3
[0040] Same as Example 1, but different from Example 1, NaCl is the molten salt. In terms of mass percentage, activated carbon fiber felt is 3% in the raw material, boron trioxide is 50% in the raw material, and magnesium powder is 47% in the raw material. , the mass ratio of raw material to NaCl is 1:4.
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