Rapid-heating constant-temperature hot compress patch and preparation method thereof
It is a warm and fast technology, which is applied in the direction of heating appliances for therapeutic treatment, cooling appliances for therapeutic treatment, contraceptives, etc. It can solve the problems of difficult temperature control, heavy hot compress, short heating time, etc., and achieve flexible use , Low manufacturing cost, constant heating temperature
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Embodiment 1
[0062] The preparation method of the self-temperature-controlling heating layer comprises the following steps:
[0063] (1) Pretreatment of conductive particles: soak and clean the acetylene carbon black powder with acetone, filter and distill under reduced pressure to remove the acetone, then heat at 120°C for 100 minutes to remove the volatile substances adsorbed on the surface of the acetylene carbon black powder;
[0064] (2) Melting: melt the low-density polyethylene particles, and at a temperature of 120°C, according to the ratio of raw materials (in terms of parts by mass, 25 parts of low-density polyethylene, 20 parts of stearic acid, 40 parts of myristic acid, acetylene 10 parts of carbon black, 5 parts of dioctyl phthalates), add myristic acid, stearic acid, step (1) pretreated acetylene carbon black and dioctyl phthalate while hot, vigorously stir and mix Homogenize to obtain a homogeneous mixture;
[0065] (3) Tablet pressing: Pour the mixture in step (2) onto the...
Embodiment 2
[0076] The preparation method of the self-temperature-controlling heating layer comprises the following steps:
[0077] (1) Pretreatment of conductive particles: Soak and clean the graphite powder with acetone, filter and distill off the acetone under reduced pressure, and then heat at 120°C for 120 minutes to remove the volatile substances adsorbed on the surface of the graphite powder;
[0078] (2) Melting: melt the ethylene vinyl acetate copolymer, and at a temperature of 100°C, according to the ratio of raw materials (by mass parts, 20 parts of ethylene vinyl acetate copolymer, 17 parts of stearic acid, 33 parts of myristic acid, 25 parts of graphite powder, 5 parts of dioctyl phthalates), add myristic acid, stearic acid, step (1) pretreated graphite and dioctyl phthalate while hot, vigorously stir and mix, obtain a homogeneous mixture;
[0079] (3) Tablet pressing: Pour the mixture in step (2) onto the pre-made enamel plate, and pre-set copper wires on both sides of the ...
Embodiment 3
[0090] The preparation method of the self-temperature-controlling heating layer comprises the following steps:
[0091] (1) Pretreatment of conductive particles: fully stir and wash the copper powder with 10% citric acid aqueous solution, filter and dry after washing for 10 hours;
[0092] (2) Melting: Melt the low-density polyethylene particles, and at a temperature of 120°C, according to the ratio of raw materials (in parts by mass, 15 parts of low-density polyethylene, 30 parts of stearic acid, 35 parts of myristic acid, copper 15 parts of powder, 3 parts of dioctyl phthalates, 2 parts of isopropyl three isostearyl phthalates), add myristic acid, stearic acid, step (1) copper powder after pretreatment while hot , dioctyl phthalate and isopropyl triisostearyl phthalate, stirred vigorously to obtain a homogeneous mixture;
[0093] (3) Tablet pressing: Pour the mixture in step (2) onto the pre-made enamel plate, and pre-set copper wires on both sides of the slurry, lightly pr...
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