Flexible fabric electrode as well as preparation method and application thereof
A flexible fabric and electrode technology, applied in chemical instruments and methods, hybrid capacitor electrodes, hybrid/electric double layer capacitor manufacturing, etc., can solve the problem of poor bonding between active materials and fabric skeletons, difficulty in maintaining the porosity of electrode materials, and affecting activity Effective use of materials and other issues to achieve the effect of facilitating wettability, enhancing electrochemical activity, and enhancing adhesion
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Embodiment 1
[0030] This embodiment provides a flexible fabric electrode and a preparation method thereof.
[0031] The preparation method of the flexible fabric electrode is as follows:
[0032] (1) Soak cotton fabric (2×4cm) in deionized water, absolute ethanol and deionized water in sequence, and ultrasonically clean them for 10 min respectively to remove inorganic and organic impurities.
[0033] (2) Soak the cleaned cotton fabric in 200ml of hydrochloric acid-Tris buffer solution (pH 7), add 100mg of dopamine monomer, and polymerize for 12h under stirring conditions.
[0034] (3) The polymerized fabric is taken out from the buffer solution, and the physically adsorbed polydopamine particles are washed out with deionized water.
[0035] (4) Soak the rinsed fabric in activated carbon solution (0.5 mg / ml) for 10 min, dry at 80°C for 20 min, and cycle 5 times.
[0036] (5) The dried fabric loaded with activated carbon was carbonized for 1 h under the protection of nitrogen, the carboniz...
Embodiment 2
[0038] This embodiment provides a flexible fabric electrode and its preparation method and application.
[0039] The preparation method of the flexible fabric electrode is as follows:
[0040] (1) The linen fabric (2×4cm) was soaked in deionized water, absolute ethanol and deionized water in sequence, and ultrasonically cleaned for 10 min respectively to remove inorganic and organic impurities.
[0041] (2) Soak the cleaned hemp fabric in 200ml hydrochloric acid-Tris buffer solution (pH 8), add different concentrations of dopamine monomer (100mg, 200mg, 400mg, 600mg, 1000mg), and polymerize for 48h under stirring conditions .
[0042] (3) The polymerized fabric is taken out from the buffer solution, and the physically adsorbed polydopamine particles are washed out with deionized water.
[0043] (4) Soak the rinsed fabric in activated carbon solution (1 mg / ml) for 10 min, dry at 80°C for 20 min, and cycle 10 times.
[0044] (5) The dried fabric loaded with activated carbon w...
Embodiment 3
[0047] This embodiment provides a flexible fabric electrode and a preparation method thereof.
[0048] The preparation method of the flexible fabric electrode is as follows:
[0049] (1) The polyester fabric (2×4cm) was immersed in deionized water, absolute ethanol and deionized water in sequence, and ultrasonically cleaned for 10 min respectively to remove inorganic and organic impurities.
[0050] (2) Soak the cleaned polyester fabric in 200ml of hydrochloric acid-Tris buffer solution (pH 9), add 400mg of dopamine monomer, and polymerize for 36h under stirring conditions.
[0051] (3) The polymerized fabric is taken out from the buffer solution, and the physically adsorbed polydopamine particles are washed out with deionized water.
[0052] (4) Soak the rinsed fabric in the carbon nanotube solution (2 mg / ml) for 10 min, dry at 80° C. for 20 min, and cycle 7 times.
[0053] (5) Carbonize the dried fabric loaded with carbon nanotubes under the protection of nitrogen for 1 ho...
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