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Paper-based/silica sol/polyvinyl alcohol (PVA) color-changing composite film for detecting water-injected meat, preparation method and application thereof

A technology of polyvinyl alcohol and silica sol, which is applied in the direction of synthetic cellulose/non-cellulose material pulp/paper, papermaking, paper, etc., can solve the problems of inability to realize quantitative detection of water-injected meat, poor dissolution resistance and mechanical properties, and individual sensory Differential effects and other issues, to achieve the effect of excellent tensile strength, excellent mechanical properties, and good resistance to dissolution

Inactive Publication Date: 2019-08-06
JILIN UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At present, the methods commonly used by consumers to identify water-injected meat include sensory evaluation, that is, observing the color of the meat, observing the new cut surface of the meat, etc. The method is simple, but it is seriously affected by individual sensory differences and lacks accuracy; there are still some in the market that are more accurate. However, the cost is relatively high and professional testing is required; some existing test papers for water-injected meat also have problems such as short life, inconvenient storage, and low sensitivity, and the existing test papers can only realize the qualitative analysis of water-injected meat Detection, that is, to detect whether the meat sample is water-injected meat, cannot realize the quantitative detection of water-injected meat. In addition, the existing water-injected meat detection test papers are all disposable test papers, which have poor dissolution resistance and mechanical properties and cannot be repeated. use

Method used

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  • Paper-based/silica sol/polyvinyl alcohol (PVA) color-changing composite film for detecting water-injected meat, preparation method and application thereof
  • Paper-based/silica sol/polyvinyl alcohol (PVA) color-changing composite film for detecting water-injected meat, preparation method and application thereof
  • Paper-based/silica sol/polyvinyl alcohol (PVA) color-changing composite film for detecting water-injected meat, preparation method and application thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0033] A paper base / silica sol / PVA color-changing composite film for detecting water-injected meat and its production method:

[0034] Step 1: Pretreatment of ion exchange resin: Soak 732 strong acid styrene cation exchange resin with 10% sodium chloride solution with solute mass fraction for 24 hours, then rinse with clear water until the washing water is colorless, and use a mass fraction of 2% Soak in sodium hydroxide solution for 2 hours, drain the lye, rinse with distilled water until the pH of the lotion is 8.5, then soak in 5% hydrochloric acid solution for 4 hours, drain the acid, and then rinse with distilled water until the pH of the lotion is 8.5. The pH is 5, and finally the resin is dried to constant weight;

[0035] Step 2: Configuration of sodium metasilicate solution with a mass fraction of 3.5%: Weigh 7 g of sodium metasilicate reagent and dissolve it in 193 ml of distilled water, stir with a glass rod to make it evenly mixed;

[0036] Step 3: Preparation of ...

Embodiment 2

[0043] Step 1: Pretreatment of ion exchange resin: Soak 732 strong acid styrene cation exchange resin with 10% sodium chloride solution with solute mass fraction for 24 hours, then rinse with clear water until the washing water is colorless, and use 4% mass fraction Soak in sodium hydroxide solution for 2 hours, drain the lye, rinse with distilled water until the pH of the lotion is 9.5, then soak in 5% hydrochloric acid solution for 4 hours, drain the acid, and then rinse with distilled water until the pH of the lotion is 9.5. The pH is 6, and finally the resin is dried to constant weight;

[0044] Step 2: The configuration of sodium metasilicate solution with a mass fraction of 3.5%: weigh 7g of sodium metasilicate reagent and dissolve it in 193ml of distilled water, stir with a glass rod to make it evenly mixed;

[0045] Step 3: Preparation of silica sol: Accurately weigh 1.000g of the ion exchange resin obtained in step 1 into a 250ml Erlenmeyer flask, then add 100ml of th...

Embodiment 3

[0052] Step 1: Cut the pork tenderloin sample to be tested into meat pieces whose length, width and height are respectively 3×2×1cm (mass 7-10g) along the direction perpendicular to the muscle fibers;

[0053] Step 2: Use a 0.5ml syringe to inject distilled water into the center of the four sides of the meat sample, take eight kinds of meat samples and inject the meat sample quality 0, 4%, 8%, 12%, 16%, 20%, 24%, 28% distilled water (each sample is carried out 3 parallel tests);

[0054] Step 3: Use tweezers to attach the color-changing composite film to the surface of the meat sample, and quickly place a weight composed of 12 glass slides on the color-changing composite film to make the color-changing composite film fully contact with the meat sample;

[0055] Step 4: Remove the weight immediately after 3 minutes, use tweezers to peel off the color-changing composite film from the meat sample, and use the TCS34725 color sensor to collect 6 points on the color-changing area of...

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PUM

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Abstract

The invention discloses a paper base / silica sol / polyvinyl alcohol (PVA) color-changing composite film for detecting water-injected meat, a preparation method and application thereof, belonging to thefield of meat quality detection. A paper base selected by the composite film is dust-free paper which is a non-woven mixed structure composed of 55% cellulose and 45% polyester fiber and has excellenttensile strength, excellent liquid absorption performance and anti-dissolution performance. A composite coating composed of silica sol and PVA has the characteristics of good film-forming property and strong water absorption. The film has excellent mechanical properties, good stability and long service life. The paper base / silica sol / polyvinyl alcohol (PVA) color-changing composite film is less affected by moisture in the environment and is convenient to store. The used color-changing composite film can be put into an oven with 100 DEG C for re-drying to realize recycling. According to the method, a mixed liquid containing a color-changing reagent and the dust-free paper are combined to detect the water injection quantity of the water injected meat, the water injection quantity can be judged not only by the color change of the composite film but also by a wet area of the composite film. The preparation method is simple and does not need special instruments and equipment. All the reagents used are low in price, the preparation method can effectively reduce the cost of the composite film and is beneficial to realizing industrialization.

Description

technical field [0001] The invention belongs to the field of meat product quality detection, and in particular relates to a paper base / silica sol / polyvinyl alcohol (PVA) color-changing composite film for detecting water-injected meat, a preparation method and an application thereof. Background technique [0002] Water-injected meat is raw meat that increases the weight of the meat by watering the livestock some time before slaughter or injecting water into the meat shortly after slaughter to make huge profits. After injecting raw meat with water, it will not only cause cell rupture and loss of nutrients, which will greatly reduce the quality of the meat, but also cause contamination of pathogenic microorganisms, and may even spread the epidemic, seriously damaging the economic interests of consumers and endangering human health. Therefore, the detection of water-injected meat is of great significance in the process of meat quality detection. At present, the methods commonly...

Claims

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Application Information

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IPC IPC(8): D21H19/38D21H19/60D21H19/40D21H13/24G01N21/78
CPCD21H13/24D21H19/38D21H19/40D21H19/60G01N21/78
Inventor 王笑丹李星刘登勇段晋娇胡凤董艳丽
Owner JILIN UNIV
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