New application of cumin volatile oil
A technology of cumin and volatile oil, applied in the application, chemical for biological control, fungicides and other directions, can solve problems such as environmental pollution, pollute the environment, kill and injure natural enemies, etc., achieve broad application prospects, simple preparation method, and convenient use Effect
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Embodiment 1
[0021] Embodiment 1: Preparation of fennel volatile oil
[0022] (1) Add water 7 times its mass to 1000g cumin, soak for 2 hours, use steam to extract the volatile oil in cumin by heating and distillation, the extraction time is 8 hours, condense and collect the effluent;
[0023] (2) The extracted liquid is dried with anhydrous sodium sulfate to remove the contained water, which is the cumin volatile oil. Put it into a brown sample bottle, seal it, and store it at -20°C for later use.
Embodiment 2
[0024] Embodiment 2: the activation of pathogenic bacteria
[0025] (1) Potato Dextrose Agar Medium (PDA): 200g potato, 20g glucose, 20g agar, 1000mL distilled water;
[0026] (2) Purify and identify the pathogenic bacteria isolated from the roots and shoots of Panax notoginseng, and identify them as Fusarium oxysporum, Fusarium solani, Pythiumaphanidermatum, and Cylindrosporium (Cylindrocarpon destructans), Colletotrichum gloeosporioides (Colletotrichum gloeosporioides) and Rhizoctonia solani (Rhizoctonia solani), the above strains were inoculated on PDA medium for activation, after inoculation 3 to 4 times, the strains with vigorous growth were taken for later use .
Embodiment 3
[0027] Embodiment 3: GC-MS measures the chemical composition of fennel volatile oil
[0028] (1) GC conditions: Instrument model: Agilengt Technologies 7890B-5977B; Chromatographic column: HP-5MS30m×250μm×0.25μm;
[0029] (2) EI source ionization source temperature: 230°C; quadrupole temperature: 150°C; scanning range: 30-500m / z; inlet temperature: 285°C; split ratio 10:1; sample volume: 1μl; Energy: 70eV; temperature program of column oven: 50°C for 4min, 5°C / min to 120°C, 1°C / min to 180°C, 10°C / min to 280°C and hold for 16min; The retention time of the alkane continuous carbon (C9-C25) is calculated, and the retention time and mass spectrum of the compound are compared with the NIST17.L database to determine the final compound. The test results are shown in the table below;
[0030]
PUM
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