Cationic dextran-based polymer and preparation thereof, and applications as flocculant
A dextran-based, cationic technology, which is applied in the field of cationic dextran derivative flocculants and its preparation, can solve secondary pollution, environmental problems, etc., achieve improved flocculation efficiency, simple operation steps, and good biodegradability and biocompatibility effects
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[0026] First, prepare 0.58mol / L sucrose solution with acetic acid-calcium acetate buffer solution with pH=5.4, and carry out catalytic fermentation reaction with 5.0U / mL dextran sucrase in T=25℃ water bath for 24 hours. , react until the dynamic viscosity reaches 8000CPS, adopt ethanol to precipitate high molecular weight dextran and dissolve it in water after washing 2-3 times to obtain a polymer dextran solution with a solid content of 5-10%; then the obtained dextran solution (about 100mL) Stir in the 250mL three-necked reaction bottle that has mechanical stirring device and make it dissolve fully; Then the potassium persulfate (as free radical initiator initiation system) of 3% mass content is slowly added in the three-necked bottle, at T=60 Initiate at ℃ for 15 minutes; then add METAC monomer according to the reaction molar ratio of cationic monomer 2-(methacryloyloxy)-ethyltrimethylammonium chloride (METAC) and dextran is 3:1 (mol / mol) , Stir the polymerization reaction ...
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