Cadmium sulfide quantum dot loaded carbon fibers prepared by utilizing waste cigarette ends, and preparation method and application of cadmium sulfide quantum dot loaded carbon fibers
A carbon fiber and cadmium sulfide technology, applied in the field of carbon fiber loaded with cadmium sulfide particles and its preparation, can solve the problems of photogenerated electron-hole instability, reducing the photo-generated electron-hole pair recombination rate, shortening the carrier migration path, etc. , to achieve the effect of improving life, improving performance, simple equipment and preparation process
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Embodiment 1
[0026] 1. Dry the discarded cigarette butts at 40°C for 12 hours;
[0027] 2. Put the dried cigarette butts into the tube furnace, feed nitrogen gas for 10 minutes, set the temperature of the tube furnace to 500°C, and anneal for 2 hours to obtain carbon fibers;
[0028] 3. Soak the carbon fiber obtained above in cadmium acetate aqueous solution for 30 seconds, then soak it in sodium sulfide aqueous solution for another 30 seconds after natural air drying, put it in a tube furnace after air drying, and calcinate at 400°C under a nitrogen atmosphere, and then cool to room temperature to obtain Carbon fibers loaded with cadmium sulfide particles.
[0029] figure 1 Surface SEM photographs of carbon fibers loaded with cadmium sulfide particles prepared for this example. From figure 1 It can be seen that the complete carbon fiber observed under the scanning electron microscope at 800 times. figure 2 Surface SEM photographs of carbon fibers loaded with cadmium sulfide particles...
Embodiment 2
[0031] 1. Dry the waste cigarette butts at 50°C for 12 hours;
[0032] 2. Put the dried cigarette butts into the tube furnace, feed nitrogen gas for 10 minutes, set the temperature of the tube furnace to 500°C, and anneal for 3 hours to obtain carbon fibers;
[0033] 3. Soak the carbon fiber obtained above in cadmium acetate aqueous solution for 30 seconds, then soak it in sodium sulfide aqueous solution for another 30 seconds after natural air drying, put it in a tube furnace after air drying, and calcinate at 400°C under a nitrogen atmosphere, and then cool to room temperature to obtain Carbon fibers loaded with cadmium sulfide particles.
Embodiment 3
[0035] 1. Dry the discarded cigarette butts at 60°C for 12 hours;
[0036] 2. Put the dried cigarette butts into the tube furnace, feed nitrogen gas for 10 minutes, set the temperature of the tube furnace to 450°C, and anneal for 3 hours to obtain carbon fibers;
[0037] 3. Soak the carbon fiber obtained above in cadmium acetate aqueous solution for 30 seconds, then soak it in sodium sulfide aqueous solution for another 30 seconds after natural air drying, put it in a tube furnace after air drying, and calcinate at 400°C under a nitrogen atmosphere, and then cool to room temperature to obtain Carbon fibers loaded with cadmium sulfide particles.
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