Preparation method of shaft disc type rotary ceramic membrane
A technology of ceramic membranes and shaft disks, which is applied in the field of inorganic membrane separation materials and inorganic porous materials, can solve the problems of difficult manufacturing of disc-type ceramic membranes, high manufacturing costs and investment costs, high operating energy consumption and operating costs, and achieve Simple manufacturing process, good oxidation resistance, and high yield
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Embodiment 1
[0038] Silica microspheres with a median diameter of 45 μm, hydroxypropylmethylcellulose and sintering aids (45wt% silica sol, 20wt% aluminum sol, 15wt% magnesium carbonate, 10wt% aluminum dihydrogen phosphate and 10wt% kaolin) The blending ratio is 85:2:13 by mass percentage, wherein silica microspheres, hydroxypropyl methylcellulose, magnesium carbonate, aluminum dihydrogen phosphate and kaolin are first mixed in a strong mixer for 15 minutes, and then press Add liquid silica sol and aluminum sol in proportion; transfer the mixed raw materials to the granulator, and then slowly add 10wt% and 4.5% of the total weight of silica microspheres, hydroxypropylmethylcellulose and sintering aids respectively Wt% water and tung oil, until the big soybean particles are formed, seal the wet material with a vacuum bag, and stale for 24 hours at a temperature of 20-25°C and a humidity of 50-80%; The material particles are added to the mold groove that has been sprinkled with a layer of gr...
Embodiment 2
[0043] Only the median diameter of the β-silicon carbide powder sprayed on the film layer was changed to 0.5 μm, and the other operation steps, addition amount and control parameters were the same as in Example 1.
Embodiment 3
[0045] Only the median diameter of the β-silicon carbide powder sprayed on the film layer was changed to 1.5 μm, and the other operation steps, addition amount and control parameters were the same as in Example 1.
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