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Preparation method of shaft disc type rotary ceramic membrane

A technology of ceramic membranes and shaft disks, which is applied in the field of inorganic membrane separation materials and inorganic porous materials, can solve the problems of difficult manufacturing of disc-type ceramic membranes, high manufacturing costs and investment costs, high operating energy consumption and operating costs, and achieve Simple manufacturing process, good oxidation resistance, and high yield

Active Publication Date: 2019-12-13
ZHEJIANG SCI-TECH UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] The purpose of the present invention is to solve the problems of complex ceramic membrane manufacturing process, high manufacturing cost and investment cost, high operating energy consumption and operating cost;

Method used

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  • Preparation method of shaft disc type rotary ceramic membrane
  • Preparation method of shaft disc type rotary ceramic membrane
  • Preparation method of shaft disc type rotary ceramic membrane

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0038] Silica microspheres with a median diameter of 45 μm, hydroxypropylmethylcellulose and sintering aids (45wt% silica sol, 20wt% aluminum sol, 15wt% magnesium carbonate, 10wt% aluminum dihydrogen phosphate and 10wt% kaolin) The blending ratio is 85:2:13 by mass percentage, wherein silica microspheres, hydroxypropyl methylcellulose, magnesium carbonate, aluminum dihydrogen phosphate and kaolin are first mixed in a strong mixer for 15 minutes, and then press Add liquid silica sol and aluminum sol in proportion; transfer the mixed raw materials to the granulator, and then slowly add 10wt% and 4.5% of the total weight of silica microspheres, hydroxypropylmethylcellulose and sintering aids respectively Wt% water and tung oil, until the big soybean particles are formed, seal the wet material with a vacuum bag, and stale for 24 hours at a temperature of 20-25°C and a humidity of 50-80%; The material particles are added to the mold groove that has been sprinkled with a layer of gr...

Embodiment 2

[0043] Only the median diameter of the β-silicon carbide powder sprayed on the film layer was changed to 0.5 μm, and the other operation steps, addition amount and control parameters were the same as in Example 1.

Embodiment 3

[0045] Only the median diameter of the β-silicon carbide powder sprayed on the film layer was changed to 1.5 μm, and the other operation steps, addition amount and control parameters were the same as in Example 1.

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Abstract

The invention relates to the technical fields of porous ceramic materials and membrane separation, in particular to a preparation method of a shaft disc type rotary ceramic membrane. The preparation method is mainly characterized in that a microsphere ceramic raw material is selected as aggregate of a support body, ceramic fibers are selected as a transition layer, beta-silicon carbide is selectedas a membrane layer, and the shaft disc type rotary ceramic membrane is formed by pressing through a hydraulic press and firing through a low-temperature liquid phase process. The preparation methodhas the characteristics of being low in sintering temperature, low in production energy consumption, simple in process method, low in equipment requirement, low in production cost and investment cost,flexible to control, easy to form, suitable for industrial customization and capable of meeting large-scale production; and the shaft disc type rotary ceramic membrane prepared by the method has thecharacteristics of good hydrophilicity, large permeation flux, high porosity, a high yield, no need of forming a diversion trench, good acid and alkali resistance and long service life.

Description

technical field [0001] The patent of the present invention relates to the technical field of inorganic porous materials, in particular to the technical field of inorganic membrane separation materials, specifically a method for preparing a shaft-disc rotating ceramic membrane. Background technique [0002] Compared with traditional polymer separation membrane materials, ceramic membranes have the advantages of good chemical stability, acid and alkali resistance, organic solvent resistance, high mechanical strength, backwashing, strong anti-microbial ability, high temperature resistance, narrow pore size distribution and high separation efficiency. , It has been widely used in the fields of food industry, biological engineering, environmental engineering, chemical industry, petrochemical industry and metallurgical industry. [0003] However, ceramic membranes also have the problem of membrane fouling, resulting in a series of disadvantages such as low membrane permeation flux...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01D71/02B01D69/02B01D69/10B01D67/00
CPCB01D71/027B01D69/02B01D69/105B01D67/0041B01D67/0076
Inventor 陈锋涛俞三传
Owner ZHEJIANG SCI-TECH UNIV
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