Bacteriostatic glyoxalated polyacrylamide-lanthanum carbonate modified graphene phosphorus chloride adsorbent
A technology for glyoxalating polyacrylamide and polyacrylamide, which is applied in adsorption water/sewage treatment, other chemical processes, chemical instruments and methods, etc. Contaminants and other problems, to achieve the effect of increasing volume and quality
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[0022] In order to achieve the above object, the present invention provides the following technical solutions: a bacteriostatic glyoxalated polyacrylamide-lanthanum carbonate modified graphene phosphorus chloride adsorbent, comprising the following raw materials in parts by weight, 75-87 parts Aminated graphene, 10-15 parts of polyacrylamide, 0.5-3 parts of lanthanum carbonate hydrate, 2-5 parts of glyoxal, 0.5-2 parts of titanate coupling agent, aminated graphene, the size is 2- 6μm, thickness: 1-3nm, ammoniation rate: about 3.7-4.2%, structural formula is Polyacrylamide is a non-ionic polyacrylamide with a molecular weight of 2.6 million-3.3 million, a degree of polymerization of 36600-46400, an aqueous solution viscosity (0.1% SOL): 330-470 (CPS), and a structural formula of The molecular formula of lanthanum carbonate hydrate is La 2 (CO 3 ) 3 ·8H 2 O, where La 2 o 3 The mass fraction is 71.5-74.6%, positive trivalent La 3+ With a high affinity for phosphate ions,...
Embodiment 1
[0029] (1) Preparation of glyoxalated polyacrylamide: add 100mL of distilled water and 200mL of ethanol to a 500mL three-necked bottle, weigh 8 parts of polyacrylamide and 2 parts of glyoxal in turn, add them to the three-necked bottle, and then configure 0.4mol / L of dilute sulfuric acid, slowly add dropwise into the three-necked flask until the pH is 3-4, place the three-necked flask in an oil bath and heat to 110-115°C, stir at a constant speed for 12-15h to make the glyoxal and Polyacrylamide fully reacted, after the reaction is complete, add sodium carbonate to the three-neck flask to quench the reaction until the pH is 7-8, filter the material to obtain white floc, wash with 2500-3500mL distilled water to completely remove sulfuric acid , sodium sulfate, sodium carbonate and impurities to obtain pure glyoxalated polyacrylamide component 1, the reaction equation is:
[0030]
[0031] (2) Preparation of glyoxalated polyacrylamide-lanthanum carbonate hybrid polymer: Weig...
Embodiment 2
[0034] (1) Preparation of glyoxalated polyacrylamide: Add 100mL distilled water and 200mL ethanol to a 500mL three-necked bottle, weigh 10 parts of polyacrylamide and 3 parts of glyoxal into the three-necked bottle, and then configure 0.4mol / L of dilute sulfuric acid, slowly add dropwise into the three-necked flask until the pH is 3-4, place the three-necked flask in an oil bath and heat to 110-115°C, stir at a constant speed for 12-15h to make the glyoxal and Polyacrylamide fully reacted, after the reaction is complete, add sodium carbonate to the three-neck flask to quench the reaction until the pH is 7-8, filter the material to obtain white floc, wash with 2500-3500mL distilled water to completely remove sulfuric acid , sodium sulfate, sodium carbonate and impurities to obtain pure glyoxalated polyacrylamide component 2, the reaction equation is:
[0035]
[0036] (2) Preparation of glyoxalated polyacrylamide-lanthanum carbonate hybrid polymer: Weigh 1 part of lanthanum...
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