A kind of anti-adhesive coating on the surface of cemented carbide sintered boat and its preparation method
An anti-stick coating, cemented carbide technology, applied in metal material coating process, coating, melt spraying and other directions, can solve the problem that the service life cannot meet the industrial production and other problems
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[0032] The present invention also provides a preparation method of the anti-sticking coating described in the above technical solution, comprising the following steps:
[0033] Preheating the cemented carbide sintered boat to obtain a preheated sintered boat;
[0034] The surface of the preheated sintered boat is sequentially sprayed with an intermediate transition coating and a working surface layer to obtain the anti-adhesive coating.
[0035] In the present invention, unless otherwise specified, all raw material components are commercially available products well known to those skilled in the art.
[0036] The invention preheats the cemented carbide sintered boat to obtain the preheated sintered boat. In the present invention, before the preheating, the cemented carbide sintered boat is preferably cleaned and roughened by sandblasting. In the present invention, the cleaning is preferably sequentially cleaning the sintered boat with alcohol and acetone. In the present inv...
Embodiment 1
[0043] The sintering boat selects a flat graphite boat for sintering of hard alloy numerical control blades;
[0044] After cleaning the sintered boat with alcohol and acetone in sequence, the surface of the sintered boat was sandblasted and roughened at a sandblasting pressure of 0.3 MPa by using a special sandblasting machine with 60 mesh white corundum grains;
[0045] Fix the sintered boat after sandblasting and roughening treatment on the workbench, use plasma flame to preheat the sintered boat, and control the preheating temperature to 160±10°C;
[0046] The aluminum oxide intermediate transition coating is prepared by plasma spraying technology. The spraying process parameters of the coating are: the main gas for spraying is argon, and the auxiliary gas for spraying is hydrogen; the flow rate of argon gas: 2.0m 3 / h, hydrogen flow rate 0.3m 3 / h, current: 780A, powder feeding rate: 40g / min, spraying distance: 100mm; during the spraying process, compressed air is used t...
Embodiment 2
[0050] Described sintering boat selects the slotted graphite boat for sintering of cemented carbide rods;
[0051] After the sintered boat was cleaned with alcohol and acetone in sequence, the surface of the sintered boat was sandblasted and roughened at a sandblasting pressure of 0.2 MPa using a special sandblasting machine with 100 mesh white corundum sand grains;
[0052] Fix the sintered boat after sandblasting and roughening treatment on the workbench, use plasma flame to preheat the sintered boat, and control the preheating temperature to 160±10°C;
[0053] The silicon carbide intermediate transition coating is prepared by plasma spraying technology. The spraying process parameters of the coating are: the main gas for spraying is argon, and the auxiliary gas for spraying is hydrogen; argon flow rate: 3.5m 3 / h, hydrogen flow rate: 0.3m 3 / h, current: 880A, powder feeding rate: 30g / min, spraying distance: 80mm; during the spraying process, compressed air is used to cool ...
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