Far-infrared energy-saving radiation coating for high-temperature furnace
A technology of far-infrared radiation and high-temperature furnaces, applied in sustainable manufacturing/processing, climate sustainability, chemical industry, etc., can solve problems such as energy constraints on global economic development, energy and environmental pollution, and environmental pollution, and achieve good long-term Infrared radiation performance, high emissivity, high yield effect
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[0036] An embodiment of the present invention also provides a preparation method of the above-mentioned infrared radiation base material, using a sol-gel method, which comprises the following steps:
[0037] - make lanthanum nitrate, aluminum nitrate, ruthenium nitrate into aqueous solution and mix to prepare liquid A;
[0038] - Dissolve amino acid and organic acid in water, add catalyst to prepare liquid B;
[0039] - Stir and mix liquid A and liquid B, then microwave, dry and grind to obtain the precursor;
[0040] - calcining the precursor and grinding to obtain LaAl after cooling 1-x Ru x O 3 Nanoparticles.
[0041] In one embodiment of the present invention, the calcination temperature is 1000-1200°C, such as 1050°C, 1085°C, 1100°C, 1110°C, 1125°C, 1140°C, 1150°C, 1160°C, 1175°C, 1180°C, 1190°C, etc. . The preparation method of the present invention utilizes the sol-gel method to prepare LaAl 1-x Ru x O 3 Nanoparticles polymerize amino acids and organic acids by...
Embodiment 1
[0069] The preparation method of infrared radiation base material comprises the following steps:
[0070] 1) after lanthanum nitrate, aluminum nitrate and ruthenium nitrate are made into the aqueous solution of 0.2mol / L, then, by the mol ratio of La:Al:Ni, it is 1:0.6:0.4 to be mixed and prepared into A liquid;
[0071] 2) Dissolve glutamic acid and citric acid in water at a molar ratio of 1:1, add a catalyst, and prepare liquid B;
[0072] 3) Mixing liquid A and liquid B according to the mass ratio of 1.25:1 for 1.5 h, then microwave irradiation for 4 min at a microwave power of 1000 W, then baked at 100 ° C for 15 h, and ground to obtain the precursor;
[0073] 4) The precursor was calcined in an air atmosphere of 1100 ° C for 3.5 h, cooled naturally in the furnace, and ground to obtain LaAl after cooling 0.6 Ru 0.4 O 3 Nanoparticles, i.e. base material for infrared radiation.
[0074] A far-infrared energy-saving radiation coating for high temperature furnaces and kilns...
Embodiment 2
[0077] The preparation method of infrared radiation base material comprises the following steps:
[0078] 1) after lanthanum nitrate, aluminum nitrate and ruthenium nitrate are made into the aqueous solution of 0.2mol / L, then, the mol ratio of La:Al:Ni is 1:0.5:0.5 to be mixed and prepared into A liquid;
[0079] 2) Dissolve glutamic acid and malic acid in water according to a molar ratio of 1:1, add a catalyst, and prepare liquid B;
[0080] 3) Mixing liquid A and liquid B according to the mass ratio of 1.25:1 for 1.5 h, then microwave irradiation for 4 min at a microwave power of 1000 W, then baked at 100 ° C for 15 h, and ground to obtain the precursor;
[0081] 4) The precursor was calcined in an air atmosphere of 1100 ° C for 3.5 h, cooled naturally in the furnace, and ground to obtain LaAl after cooling 0.5 Ru 0.5 O 3 Nanoparticles, i.e. base material for infrared radiation.
[0082] A far-infrared energy-saving radiation coating for high temperature furnaces and kil...
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