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Phosphorus-boron-nitrogen-containing composition trace lubricating oil and preparation method thereof

A technology for lubricating oil and lubricating oil composition, applied in the field of lubrication, can solve problems such as affecting the health of operators, unfriendly sulfur- and chlorine-containing additives, processing sites and environmental pollution, etc., and achieves significant environmental protection effects and is degradable. The effect of good performance and excellent biodegradability

Inactive Publication Date: 2020-04-21
SHANGHAI JINZHAO ENERGY SAVING TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] The traditional metal cutting process uses mineral oil or vegetable oil or cutting fluid for a large amount of shower lubrication. The amount of lubricant used is large, which not only wastes resources, but also causes huge pollution to the processing site and the environment, and also seriously affects the health of the operators.
[0003] In order to solve these problems, some progress has been made in the research of micro-quantity lubrication technology recently. The micro-quantity lubrication technology solves the above problems such as large amount of lubricant used and serious pollution. At the same time, in order to make the micro-quantity lubricant used have relatively strong extreme pressure and anti-wear Therefore, it is a meaningful research topic to study a micro-quantity lubricant additive that does not contain sulfur and chlorine and has excellent extreme pressure and anti-wear properties. , since the phosphorus-boron-nitrogen lubricating oil composition has relatively good extreme pressure and anti-wear performance, the research on the material of the phosphorus-boron-nitrogen lubricating oil composition is also of practical significance

Method used

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  • Phosphorus-boron-nitrogen-containing composition trace lubricating oil and preparation method thereof
  • Phosphorus-boron-nitrogen-containing composition trace lubricating oil and preparation method thereof
  • Phosphorus-boron-nitrogen-containing composition trace lubricating oil and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0037] Step 1: Weigh 1000 g of ricinoleic acid, 100 g of isopropanolamine, 80 g of isotridecanol, and 50 g of boric acid into the reaction kettle, and stir evenly.

[0038] Step 2: After slowly adding 50 g of phosphorus pentoxide and stirring the reaction for 60 minutes, the heat of reaction can be used, and at the same time, it can be heated to 150 ° C, and the moisture generated by the reaction can be removed in time, and the pressure in the kettle is kept not more than 200 mmHg. The filtered oil is a lubricating oil composition.

[0039] A trace amount of lubricating oil is obtained when 100 g of the lubricating oil composition, 800 g of diisodecyl adipate, and 100 g of polysucrose caprate are mixed and stirred at room temperature until completely transparent.

[0040] The preparation method of above-mentioned polysucrose caprate:

[0041] Step 1: add 342.3g (1mol) of sucrose, 139.28g (1.2mol) of maleic acid, 1033.56g (6mol) of n-decanoic acid, and 10g of catalyst (10% dil...

Embodiment 2

[0044] Step 1: Weigh 1000 g of ricinoleic acid, 80 g of isopropanolamine, 50 g of isooctyl alcohol, and 30 g of boric acid, and add them into the reaction kettle together, and stir evenly.

[0045] Step 2: After slowly adding 30 g of phosphorus pentoxide and stirring the reaction for 30 minutes, use the heat of reaction to heat to 180 ° C at the same time, remove the moisture generated by the reaction in time, keep the pressure in the kettle not more than 200 mmHg, fully react for 5 hours, and the filtered The oil is a lubricating oil composition.

[0046] A trace amount of lubricating oil is obtained by weighing and stirring 150 g of the lubricating oil composition, 700 g of diisodecyl adipate, and 150 g of polysucrose laurate at room temperature until completely transparent.

[0047] The preparation method of above-mentioned polysucrose laurate:

[0048] Step 1: add 342.3 g (1 mol) of sucrose, 116.07 g (1 mol) of fumaric acid, 900.96 g (3 mol) of lauric acid, and 2 g of lan...

Embodiment 3

[0051] Step 1: Weigh 1000 g of ricinoleic acid, 90 g of isopropanolamine, 60 g of isodecanol, and 40 g of boric acid, and add them to the reaction kettle, and stir evenly.

[0052] Step 2: After slowly adding 40 g of phosphorus pentoxide and stirring the reaction for 40 minutes, use the heat of reaction to heat to 170 ° C at the same time, remove the moisture generated by the reaction in time, keep the pressure in the kettle not more than 200 mmHg, and fully react for 5.5 hours. The oil is a lubricating oil composition.

[0053] A trace amount of lubricating oil is obtained by weighing 120 g of the lubricating oil composition, 750 g of diisodecyl adipate, and 130 g of polysucrose cocoate and mixing and stirring at room temperature until completely transparent.

[0054] The preparation method of above-mentioned polysucrose cocoate:

[0055] Step 1: add 342.3g (1mol) of sucrose, 98.08g (1mol) of maleic anhydride, 1120g (about 4mol) of cocoic acid, and 8g of cerium oxide into th...

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Abstract

The invention provides a lubricating oil composition, which is characterized in that the lubricating oil composition provided by the invention is prepared from the following components (by weight): 100 parts of ricinoleic acid, 8-10 parts of isopropanolamine, 5-8 parts of isomeric alcohol, 3-5 parts of boric acid and 3-5 parts of phosphorus pentoxide. The lubricating oil composition prepared by adopting the preparation method is a B-P-N type friction modifier and an antirust agent, and is good in degradability. The invention also provides trace lubricating oil containing the above lubricatingoil composition, and the trace lubricating oil is characterized by being prepared from the following components (by weight): 10-20% of the lubricating oil composition, 70-80% of diisodecyl adipate and10-20% of polysucrose fatty acid ester. The trace lubricating oil prepared by the invention can meet the requirements of lubrication cooling, extreme pressure wear resistance and rust prevention in metal processing; and the use amount of a lubricant can be saved by more than 95% by matching with a minimal quantity lubricating device, and the effects of energy conservation, emission reduction andenvironmental protection are remarkable.

Description

technical field [0001] The invention belongs to the technical field of lubrication, and in particular relates to a trace lubricating oil of a phosphorus-boron composition and a preparation method. Background technique [0002] The traditional metal cutting process uses mineral oil or vegetable oil or cutting fluid for a large amount of shower lubrication. The use of lubricant is large, which not only wastes resources, causes huge pollution to the processing site and the environment, but also seriously affects the health of operators. . [0003] In order to solve these problems, some progress has been made in the recent research on the minimal quantity lubrication technology. The minimal quantity lubrication technology solves the problems of the above-mentioned lubricants such as large amount of lubricants and serious pollution. Therefore, it is a meaningful research topic to study a micro-lubricant additive that does not contain sulfur and chlorine and has excellent extreme...

Claims

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Application Information

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IPC IPC(8): C10M169/04C10M141/06C10N30/06C10N30/12C10N40/22
CPCC10M141/06C10M169/044C10M2201/087C10M2207/021C10M2207/2825C10M2207/40C10M2209/102C10M2215/042
Inventor 张乃庆蒋宁吴启东丁金波
Owner SHANGHAI JINZHAO ENERGY SAVING TECH
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