A high-magnification spherical oxide alloy composite electrode material and its preparation method
A composite electrode and high-magnification technology, which is applied in chemical instruments and methods, battery electrodes, titanium compounds, etc., can solve the problems of reducing product life, precipitation of metal lithium, and safety, so as to prolong cycle life and improve electronic conductivity , improve the effect of flatulence
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[0041] The present invention also provides a method for preparing a high-magnification spherical oxide alloy composite electrode material, comprising the following steps:
[0042] (1) Put lithium source, titanium dioxide, M metal ion source, highly conductive carbon phase raw material and medium solution in the reaction kettle, and disperse to obtain the precursor;
[0043] (2) Grinding the precursor obtained in step (1) to obtain a uniformly dispersed nanoscale precursor;
[0044] (3) spraying and granulating the nano-precursor obtained in step (2) to obtain a dry spherical precursor;
[0045] (4) Place the dried spherical precursor obtained in step (3) in an inert gas atmosphere for pre-sintering and re-sintering. The re-sintering temperature is 700~850°C, the re-sintering time is 10~16h, and cooled to room temperature.
[0046] In the present invention, unless otherwise specified, the raw materials used are commercially available products well known to those skilled in the ...
Embodiment 1
[0062] Ratio of materials: The high conductive carbon phase raw material is carbon nanotubes, metal ions are Mg, the molar ratio of titanium ions to metal ions is 5:0.05, the molar ratio of lithium ions to titanium ions is 4.1:5, carbon nanotubes and titanium The molar ratio is 0.05:5.
[0063] (1) Lithium hydroxide monohydrate, titanium dioxide, zirconium nitrate, lithium niobate, ammonium metavanadate, nano-magnesium oxide, carbon nanotubes and ethanol solution are placed in a reaction kettle with a solid-to-liquid ratio of 1:2. Stir continuously and ultrasonically disperse for 4 hours at a speed of 200 r / min to obtain a precursor.
[0064] (2) Place the precursor obtained in step (1) in a high-energy ball mill for high-intensity ball milling for 5 hours at a speed of 1500 r / min, and control D50 to 0.5 μm to obtain a uniformly dispersed nano precursor.
[0065] (3) Spray and granulate the nano-precursor obtained in step (2), the air inlet temperature is 200°C, the outlet ai...
Embodiment 2
[0068] Ratio of materials: The high-conductivity carbon phase raw material is carbon nanotubes, the metal ions are Ba and Ag, the molar ratio of the two metal ions satisfies Ba:Ag =1:1, and the molar ratio of titanium ions and the above two other metal ions is 5:0.2, the molar ratio of lithium ions to titanium ions is 4.4:5, and the molar ratio of carbon nanotubes to titanium is 0.03:5.
[0069] (1) Put lithium hydroxide monohydrate, titanium dioxide, barium carbonate, silver nitrate, carbon nanotubes and ethanol solution in a reaction kettle with a solid-to-liquid ratio of 1:2, stir continuously and ultrasonically disperse for 5 hours at a speed of 200r / min to get the precursor.
[0070] (2) Place the precursor obtained in step (1) in a high-energy ball mill for high-intensity ball milling for 4.5 hours at a rotational speed of 1800r / min, and control D50 to 0.1 μm to obtain a uniformly dispersed nano precursor.
[0071] (3) Spray and granulate the nano-precursor obtained in...
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