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Inferior heavy oil treatment method

A low-quality heavy oil and treatment method technology, applied in the field of oil refining and chemical industry, can solve the problems of high liquid recovery loss, frequent backwashing, pollution, etc., and achieve the effect of increasing the utilization rate of heavy oil, improving the overall value, and improving the economic value

Pending Publication Date: 2020-05-01
CHINA PETROLEUM & CHEM CORP +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0007] The traditional heavy oil thermal processing technology has the problems of low liquid yield and serious pollution, while the catalytic oil slurry obtained by the heavy oil catalytic cracking technology has the problem of high solid content and small particle size, and there is a loss of liquid yield when the catalytic oil slurry is treated by conventional filtration. High, incomplete removal of catalyst powder, easy clogging of filters, frequent backwashing, and unstable operation of filter devices, most of the catalytic oil slurry can only be used as feed to the coking unit, and a large amount of low-value coke is produced by-product, catalytic oil slurry value is not fully realized

Method used

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Effect test

Embodiment 1

[0048]Example 1. Residual oil is used as raw material, and the inferior heavy oil treatment method described in the present invention is adopted. The inferior heavy oil enters the first hydroprocessing unit (the first hydroprocessing unit adopts a fixed-bed reactor), and the hydrogen and the first hydrogenation The hydrogenation reaction is carried out in the presence of a treatment catalyst. The reaction conditions of the first hydrogenation reactor are: reaction temperature 385°C, reaction pressure 15.5Mpa, volume space velocity 0.28h -1 , the volume ratio of hydrogen to oil is 450; the liquid phase effluent obtained after the reaction directly enters the catalytic cracking unit without fractionation, and the reaction product is separated to obtain dry gas, liquefied gas, catalytic gasoline, catalytic diesel, catalytic heavy cycle oil and catalytic oil slurry; The catalytic oil slurry is firstly mixed with the whole fraction of the first auxiliary agent coal tar, the ratio of...

Embodiment 2

[0050] Example 2 Using residual oil as raw material, using the inferior heavy oil treatment method described in the present invention, the inferior heavy oil enters the first hydroprocessing unit (the first hydroprocessing unit adopts a fixed-bed reactor), and the hydrogen and the first hydrogenation The hydrogenation reaction is carried out in the presence of a treatment catalyst. The reaction conditions of the first hydrogenation reactor are: reaction temperature 385°C, reaction pressure 15.8Mpa, volume space velocity 0.30h -1 , the volume ratio of hydrogen to oil is 500; the liquid phase effluent obtained after the reaction directly enters the catalytic cracking unit without fractionation, and the reaction product is separated to obtain dry gas, liquefied gas, catalytic gasoline, catalytic diesel oil, catalytic heavy cycle oil and catalytic oil slurry; The catalytic oil slurry is first mixed with the first auxiliary agent coal tar whole distillate and the second auxiliary ag...

Embodiment 3

[0052] Example 3 Using residual oil as raw material, using the inferior heavy oil treatment method described in the present invention, the inferior heavy oil enters the first hydroprocessing unit (the first hydroprocessing unit adopts a fixed-bed reactor), and the hydrogen and the first hydrogenation The hydrogenation reaction is carried out in the presence of a treatment catalyst. The reaction conditions of the first hydrogenation reactor are: reaction temperature 390°C, reaction pressure 16.5Mpa, volume space velocity 0.32h -1 , the volume ratio of hydrogen to oil is 550; the liquid phase effluent obtained after the reaction directly enters the catalytic cracking unit without fractionation, and the reaction product is separated to obtain dry gas, liquefied petroleum gas, catalytic gasoline, catalytic diesel oil, catalytic heavy cycle oil and catalytic oil slurry; The catalytic oil slurry is mixed with the first auxiliary agent coal tar distillate oil (fraction -1 , the volume...

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Abstract

The invention discloses an inferior heavy oil treatment method. The treatment method comprises the following steps: introducing inferior heavy oil into a first hydro-processing unit; carrying out a hydrogenation reaction in the presence of hydrogen and a first hydro-processing catalyst, directly introducing a liquid phase effluent obtained after the reaction into a catalytic cracking unit withoutfractionation, separating a reaction product to obtain catalytic slurry oil, mixing the catalytic slurry oil with a first auxiliary agent, carrying out settlement separation after the mixing treatment, obtaining a first material and residues after separation; introducing the first material into a second hydro-processing unit, carrying out a hydrogenation reaction under the action of a second hydro-processing catalyst and hydrogen, introducing a liquid-phase effluent obtained after the reaction into a clarification unit, obtaining clarified oil after separation, and subjecting the clarified oilto further solid-liquid separation to obtain purified oil slurry. According to the treatment method, heavy oil is cleaned, catalytic slurry oil generated by catalytic cracking can be purified, solidsand sulfur in catalytic slurry oil are removed, and the economic value of the catalytic slurry oil is greatly increased.

Description

technical field [0001] The invention belongs to the field of oil refining and chemical industry, and in particular relates to a method for processing inferior heavy oil. Background technique [0002] As crude oil becomes heavier and inferior, the proportion of residual oil, which is the heaviest component in crude oil, continues to increase. With increasingly stringent environmental protection requirements, the efficient use of heavy oil, especially residual oil, is not only related to whether it can meet The requirements of cleaner production have also become an important factor affecting the economic benefits and even the survival of enterprises. From the traditional processing methods of residual oil, residual oil processing can be divided into two routes: hydrogenation and decarburization. Decarburization mainly refers to thermal cracking, visbreaking and solvent deasphalting, etc., while hydrogenation routes can be divided into fixed Bed hydrogenation, suspension bed h...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C10G67/02
CPCC10G67/02
Inventor 代萌孟兆会陈博葛海龙姜来杨涛
Owner CHINA PETROLEUM & CHEM CORP
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