A low-density reinforcing agent for oil well cement and its preparation method

An oil well cement, low-density technology, used in chemical instruments and methods, sustainable waste treatment, solid waste management, etc., can solve the problems of low-density external admixtures in material availability, cost control, and thickening time. , the problem of high cost, to achieve the effect of good slurry fluidity, good comprehensive performance, and lower production costs

Active Publication Date: 2021-10-22
卫辉市化工有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] (1) Fly ash low-density cement slurry system has disadvantages such as long thickening time and low cement stone strength;
[0005] (2) Bentonite affects the thickening time and slurry fluidity, and at the same time, the strength of cement stone is low;
[0006] (3) The pressure resistance of ordinary floating beads is poor. Although the pressure resistance of power plant floating beads and glass beads is improved, the cost is high and it cannot be widely used.
[0011] Therefore, the current low-density cement slurry systems often have problems such as poor pressure resistance, poor slurry stability, and low compressive strength. efficiency requirements

Method used

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  • A low-density reinforcing agent for oil well cement and its preparation method
  • A low-density reinforcing agent for oil well cement and its preparation method
  • A low-density reinforcing agent for oil well cement and its preparation method

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0042] The low-density reinforcing agent for oil well cement in this embodiment consists of the following components: 232kg of special early strength agent, 600kg of micro-silica fume and 168kg of superfine slag powder. The ultrafine slag powder is S95 grade granulated blast furnace slag powder; the particle size of the micro silicon powder is 160-300 mesh.

[0043] The special early strength agent is composed of the following materials: 90 kg of sodium sulfate, 42 kg of aluminum ammonium sulfate, 50 kg of calcium chloride, 40 kg of polyaluminum chloride, and 10 kg of a mixture of white carbon black and triisopropanolamine, white carbon black and triisopropanolamine The mass ratio of isopropanolamine is 3:2.

[0044] The preparation method of the low-density reinforcing agent for oil well cement in this embodiment comprises the following steps:

[0045] (1) Add 10 kg of the mixture of white carbon black and triisopropanolamine into the mixing kettle, and mix for 20 minutes; ...

Embodiment 2

[0050] The low-density reinforcing agent for oil well cement in this embodiment consists of the following components: 246 kg of special early strength agent, 600 kg of microsilica fume and 154 kg of ultrafine slag powder. The ultrafine slag powder is S95 grade granulated blast furnace slag powder; the particle size of the micro silicon powder is 160-300 mesh.

[0051]The special early strength agent is composed of the following materials: 90 kg of sodium sulfate, 42 kg of aluminum ammonium sulfate, 50 kg of calcium chloride, 40 kg of polyaluminum chloride, 14 kg of nano silicon dioxide and 10 kg of a mixture of white carbon black and triisopropanolamine , the mass ratio of white carbon black to triisopropanolamine is 3:2.

[0052] The preparation method of the low-density reinforcing agent for oil well cement in this embodiment comprises the following steps:

[0053] (1) Add 10 kg of the mixture of white carbon black and triisopropanolamine into the mixing kettle, and mix for...

Embodiment 3

[0058] The low-density reinforcing agent for oil well cement in this embodiment consists of the following components: 246 kg of special early strength agent, 600 kg of microsilica fume and 154 kg of ultrafine slag powder. The ultrafine slag powder is S95 grade granulated blast furnace slag powder; the particle size of the micro silicon powder is 160-300 mesh.

[0059] The special early strength agent is composed of the following materials: 50 kg of sodium sulfate, 42 kg of aluminum ammonium sulfate, 40 kg of calcium chloride, 40 kg of polyaluminum chloride, 14 kg of nano silicon dioxide, 50 kg of hydrotalcite, white carbon black and triisopropanol The mixture of amines is 10kg, and the mass ratio of white carbon black to triisopropanolamine is 3:2.

[0060] The preparation method of the low-density reinforcing agent for oil well cement in this embodiment comprises the following steps:

[0061] (1) Add 10 kg of the mixture of white carbon black and triisopropanolamine into the...

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Abstract

The invention discloses a low-density strengthening agent for oil well cement and a preparation method thereof. It is composed of a special early strength agent, microsilica fume and ultrafine slag powder, and the special early strength agent is composed of one or more of the following components: Various compositions: a mixture of sodium sulfate, aluminum ammonium sulfate, calcium chloride, polyaluminum chloride, nano-silicon dioxide, hydrotalcite, white carbon black and triisopropanolamine. The fluidity of the cement slurry prepared with low-density reinforcing agent for oil well cement is between 23 and 25cm, and the fluidity of the slurry is good; the density difference of the cement slurry under pressure is ≤0.02g / cm 3 , the stability of the cement slurry is good; zero free water can be realized; the strength of the cement stone develops rapidly, the compressive strength reaches above 7MPa in 24 hours, and the compressive strength reaches above 10MPa in 48MPa hours; , the comprehensive performance of cement slurry is good.

Description

technical field [0001] The invention relates to the technical field of petroleum exploration and development. Specifically, it relates to a low-density reinforcing agent for oil well cement and a preparation method thereof. Background technique [0002] With the process of oil exploration and development, more and more oil and gas wells encounter low-pressure formations, weak formations and other formations that are prone to leakage. The low-density cement slurry system is the main method to solve the problem of low-pressure and leakage-prone formations. [0003] Lightening materials for conventional low density grout systems are: [0004] (1) Fly ash low-density cement slurry system has disadvantages such as long thickening time and low cement stone strength; [0005] (2) Bentonite affects the thickening time and slurry fluidity, and at the same time, the strength of cement stone is low; [0006] (3) The pressure resistance of ordinary floating beads is poor. Although th...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C04B24/12C09K8/473C04B103/12C04B18/14
CPCC04B40/0039C04B2103/12C09K8/426C09K8/473C04B18/141C04B18/146C04B22/06C04B24/122C04B22/147C04B22/148C04B22/124C04B22/12Y02W30/91
Inventor 郭娟李新芬郭峰靳建忠李林锋张峰赵淑丹李浩张珂王爱民
Owner 卫辉市化工有限公司
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