A low-density reinforcing agent for oil well cement and its preparation method
An oil well cement, low-density technology, used in chemical instruments and methods, sustainable waste treatment, solid waste management, etc., can solve the problems of low-density external admixtures in material availability, cost control, and thickening time. , the problem of high cost, to achieve the effect of good slurry fluidity, good comprehensive performance, and lower production costs
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Embodiment 1
[0042] The low-density reinforcing agent for oil well cement in this embodiment consists of the following components: 232kg of special early strength agent, 600kg of micro-silica fume and 168kg of superfine slag powder. The ultrafine slag powder is S95 grade granulated blast furnace slag powder; the particle size of the micro silicon powder is 160-300 mesh.
[0043] The special early strength agent is composed of the following materials: 90 kg of sodium sulfate, 42 kg of aluminum ammonium sulfate, 50 kg of calcium chloride, 40 kg of polyaluminum chloride, and 10 kg of a mixture of white carbon black and triisopropanolamine, white carbon black and triisopropanolamine The mass ratio of isopropanolamine is 3:2.
[0044] The preparation method of the low-density reinforcing agent for oil well cement in this embodiment comprises the following steps:
[0045] (1) Add 10 kg of the mixture of white carbon black and triisopropanolamine into the mixing kettle, and mix for 20 minutes; ...
Embodiment 2
[0050] The low-density reinforcing agent for oil well cement in this embodiment consists of the following components: 246 kg of special early strength agent, 600 kg of microsilica fume and 154 kg of ultrafine slag powder. The ultrafine slag powder is S95 grade granulated blast furnace slag powder; the particle size of the micro silicon powder is 160-300 mesh.
[0051]The special early strength agent is composed of the following materials: 90 kg of sodium sulfate, 42 kg of aluminum ammonium sulfate, 50 kg of calcium chloride, 40 kg of polyaluminum chloride, 14 kg of nano silicon dioxide and 10 kg of a mixture of white carbon black and triisopropanolamine , the mass ratio of white carbon black to triisopropanolamine is 3:2.
[0052] The preparation method of the low-density reinforcing agent for oil well cement in this embodiment comprises the following steps:
[0053] (1) Add 10 kg of the mixture of white carbon black and triisopropanolamine into the mixing kettle, and mix for...
Embodiment 3
[0058] The low-density reinforcing agent for oil well cement in this embodiment consists of the following components: 246 kg of special early strength agent, 600 kg of microsilica fume and 154 kg of ultrafine slag powder. The ultrafine slag powder is S95 grade granulated blast furnace slag powder; the particle size of the micro silicon powder is 160-300 mesh.
[0059] The special early strength agent is composed of the following materials: 50 kg of sodium sulfate, 42 kg of aluminum ammonium sulfate, 40 kg of calcium chloride, 40 kg of polyaluminum chloride, 14 kg of nano silicon dioxide, 50 kg of hydrotalcite, white carbon black and triisopropanol The mixture of amines is 10kg, and the mass ratio of white carbon black to triisopropanolamine is 3:2.
[0060] The preparation method of the low-density reinforcing agent for oil well cement in this embodiment comprises the following steps:
[0061] (1) Add 10 kg of the mixture of white carbon black and triisopropanolamine into the...
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