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Low-dielectric-constant organic silicon pouring sealant and preparation method thereof

A technology of silicone potting glue and low dielectric constant, applied in the field of potting glue, can solve the problem of unstable porous material, and achieve the effect of reducing the dielectric constant, improving compatibility, and reducing signal interference

Active Publication Date: 2020-07-17
GUANGZHOU HUITIAN FINE CHEM
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] Aiming at the defects and deficiencies in the background technology, the present invention provides a low dielectric constant silicone potting compound, which can solve the problem of unstable porous materials containing air in the silicone system. The silicone potting compound is stable in storage, the dielectric constant is lower than 3.0 (1MHz), and the thermal conductivity and viscosity are moderate

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0036] Embodiment 1: a kind of low dielectric constant silicone encapsulant, including A component and B component;

[0037] Component A includes the following parts by weight: 10 parts of single-end vinyl silicone oil, 25 parts of side chain vinyl silicone oil; 4.5 parts of dimethyl silicone oil; 60 parts of microporous silicon powder; 0.5 parts of platinum catalyst.

[0038] Component B includes the following materials in parts by weight: 10 parts of single-end vinyl silicone oil, 20 parts of side chain vinyl silicone oil; 9.8 parts of side-containing hydrogen silicone oil; 60 parts of microporous silicon micropowder; 0.2 parts of methyl butynol.

[0039] and prepared by the following steps:

[0040] 1) Put 120 parts of microporous silicon micropowder into the modification machine. When the speed of the modification machine is 800r / min and the temperature of the modified material is 70°C, spray 1.2 parts of stearic acid and A mixture of isopropanol, the mixing ratio of stea...

Embodiment 2

[0046] Embodiment 2: a kind of low dielectric constant silicone encapsulant, including A component and B component;

[0047] Component A includes the following substances in parts by weight: 40 parts of double-ended vinyl silicone oil; 9.2 parts of dimethyl silicone oil; 10 parts of silicon dioxide; 40 parts of microporous ceramic powder; 0.8 parts of platinum catalyst.

[0048] Component B includes the following materials in parts by weight: 34.6 parts of double-ended vinyl silicone oil; 15 parts of hydrogen-containing silicone oil; 10 parts of silicon dioxide; 40 parts of microporous ceramic powder; 0.4 parts of acetylene cyclohexanol.

[0049] and prepared by the following steps:

[0050] 1) Put 80 parts of microporous ceramic powder into the modification machine. When the speed of the modification machine is 1000r / min and the temperature of the modified material is 75°C, spray 0.92 parts of stearic acid and A mixture of isopropanol, the mixing ratio of stearic acid and is...

Embodiment 3

[0056] Embodiment 3: A kind of low dielectric constant silicone encapsulant, comprises A component and B component;

[0057] Component A includes the following parts by weight: 30 parts of double-ended vinyl silicone oil; 20 parts of single-ended vinyl silicone oil; 8.8 parts of dimethyl silicone oil; 10 parts of alumina; 30 parts of hollow glass microspheres; 1.2 parts of platinum catalyst share.

[0058] Component B includes the following parts by weight: 30 parts of double-ended vinyl silicone oil; 10 parts of single-ended vinyl silicone oil; 19.5 parts of hydrogen-containing silicone oil at the end side; 10 parts of aluminum oxide; 30 parts of hollow glass microspheres; 0.5 parts of alcohol.

[0059] and prepared by the following steps:

[0060] 1) Put 60 parts of hollow glass microspheres into the modifier. When the speed of the modifier is 800r / min and the temperature of the modified material is 75°C, spray 0.5 parts of KH-560, A -171 with H 2 A mixed modifier of O, ...

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Abstract

The invention provides an organic silicon pouring sealant with a low dielectric constant. The invention belongs to the technical field of organosilicon pouring sealants. The organic silicon pouring sealant comprises a component A and a component B. The component A comprises, by weight, 10-40 parts of vinyl silicone oil, 1-10 parts of a diluent, 0-20 parts of a heat conduction filler, 10-60 parts of a low dielectric material, and 0.1-2.0 parts of a catalyst. The component B comprises, in parts by weight: 10 to 40 parts of vinyl silicone oil, 5 to 30 parts of a cross-linking agent, 0 to 20 partsof a heat conduction filler, 10 to 60 parts of a low dielectric material and 0.1 to 1.0 part of an inhibitor; the preparation method comprises the following steps: carrying out organic treatment on alow-dielectric material, stirring in a reaction kettle, cooling, stirring again, cooling again to obtain the finished product A and the finished product B, and uniformly mixing the prepared finishedproduct A and the finished product B according to the mass ratio of 1: 1 for later use. The phase change pouring sealant can solve the problem that a porous material containing air is unstable in an organic silicon system, the organic silicon pouring sealant is stable in storage, the dielectric constant is lower than 3.0 (1MHz), and heat conduction and viscosity are moderate.

Description

technical field [0001] The invention relates to the technical field of potting glue, in particular to a silicone potting glue and a preparation method thereof. Background technique [0002] With the rapid development of the microelectronics industry, more and more electronic products are developing towards miniaturization, integration and functionalization. The integration of circuits is getting higher and higher, and the types and quantities of electronic devices per unit volume are also increasing. more. The distance between different electronic devices is further reduced, and at the same time it will bring some negative effects, such as signal interference between wires, resistance and capacitance delays, and increased energy consumption. At present, in the academic circle, the most effective way to solve this problem is to use low dielectric constant materials to prepare copper clad laminates, so as to reduce the above-mentioned negative effects. For example, Chinese p...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09J183/07C09J183/05C09J11/04C09J11/08
CPCC09J183/04C09J11/04C09J11/08C08K2003/2227C08L2203/206C08L2205/035C08L2205/025C08L83/04C08K7/26C08K9/04C08K3/22C08K7/28C08K9/06C08K7/24
Inventor 张探张银华赵勇刚孔丽芬岑昌丽
Owner GUANGZHOU HUITIAN FINE CHEM
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