A fuel cell electrode assisted by thermocatalysis and its preparation method and application
A fuel cell electrode and auxiliary electrode technology, which is applied in the direction of fuel cells, battery electrodes, solid electrolyte fuel cells, etc., can solve the problems of slow kinetics of biocatalysis process, low maximum power density of discharge performance, and impossibility of practical application. It is conducive to full exposure, enhanced physical and chemical activity, and strong practicability
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Embodiment 1
[0033] a, Fabrication of thermocatalytic auxiliary electrode components
[0034] Disperse phosphotungstic acid and polybenzimidazole powder materials in a dimethylformamide solution at a mass ratio of 5:1, with a mass percentage concentration of 10%, and fully ultrasonically stir for 2 hours at 80 degrees Celsius; Add the mixed slurry to 85% concentrated phosphoric acid with twice the mass concentration, and stir at 150 degrees Celsius for 2 hours to fully volatilize the volatile solvent; impregnate the above mixed slurry in carbon paper to make the catalyst loading 5mg / cm 2 spare.
[0035] b, Preparation of fuel cell electrode components
[0036] Disperse a certain mass of carbon-supported platinum in a dimethylformamide solvent with a mass percentage concentration of 30 mg / ml, then add polybenzimidazole powder accounting for 20% by mass of the electrocatalyst, and stir at 80 degrees Celsius for 2 hours , so that it is fully dissolved, and then ultrasonically dispersed for ...
Embodiment 2
[0058] a, Fabrication of thermocatalytic auxiliary electrode components
[0059] Disperse phosphomolybdic acid and polybenzimidazole powder materials in a dimethylformamide solution at a mass ratio of 1:1, with a mass percentage concentration of 20%, and fully ultrasonically stir for 8 hours at room temperature; the above Add the mixed slurry to 5 times the mass concentration of 85% concentrated phosphoric acid, and stir at 200 degrees Celsius for 2 hours to fully volatilize the volatile solvent in it; impregnate the above mixed slurry in carbon felt to make the catalyst loading 10mg / cm 2 spare.
[0060] b, Preparation of fuel cell electrode components
[0061] Disperse a certain mass of platinum ruthenium black in a dimethylacetamide solvent with a mass percent concentration of 100 mg / ml, then add polybenzimidazole powder accounting for 50% of the mass ratio of the electrocatalyst, and stir at room temperature for 8 hour, so that it is fully dissolved, and then ultrasonical...
Embodiment 3
[0065] a, Fabrication of thermocatalytic auxiliary electrode components
[0066] Disperse phosphovanadic acid and polybenzimidazole powder materials in a dimethylformamide solution at a mass ratio of 1:1, with a mass percentage concentration of 20%, and fully ultrasonically stir for 8 hours at room temperature; the above Add the mixed slurry to 5 times the mass concentration of 85% concentrated phosphoric acid, and stir at 200 degrees Celsius for 2 hours to fully volatilize the volatile solvent therein; impregnate the above mixed slurry in porous graphite to make the catalyst loading 10mg / cm 2 spare.
[0067] b, Preparation of fuel cell electrode components
[0068] Disperse a certain mass of carbon-supported platinum-tin alloy in a dimethylacetamide solvent with a mass percentage concentration of 100 mg / ml, then add polybenzimidazole powder accounting for 50% of the mass ratio of the electrocatalyst. Stir for 8 hours to make it fully dissolve, then ultrasonically disperse f...
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