Non-noble metal bifunctional catalyst as well as preparation method and application thereof
A dual-functional catalyst and non-precious metal technology, applied in chemical instruments and methods, physical/chemical process catalysts, organic compounds/hydrides/coordination complex catalysts, etc., can solve insufficient electrical conductivity, instability of MOFs materials, etc. problem, to achieve the effect of improving physical and chemical activity, facilitating full exposure, and a wide range of effects
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0031] a, Preparation of carbon-based sheet material The carbon-based sheet material uses graphite oxide prepared by the Hummer method as a precursor, and the prepared graphite oxide is dispersed in deionized water at a concentration of 5 mg / ml, and ultrasonically stirred for 4 hours, and condensed to a solid state with liquid nitrogen, and placed in a freeze dryer for 24 hours of freeze-drying process until the solvent was completely removed; the above-mentioned dried samples were dispersed in concentrated nitric acid solution for deep oxidation, and condensed at room temperature under the condition of reflux Oxidation reaction for 4 hours, washing, filtering and drying for later use; disperse the above sample in deionized water at a concentration of 10 mg / ml, add melamine, the molar ratio of nitrogen to carbon is 1:1, and fully stir at 80 degrees Celsius for 4 hours , then condensed to a solid state with liquid nitrogen, placed in a freeze dryer for 24 hours of freeze-drying ...
Embodiment 2
[0041] a, Preparation of carbon-based sheet material The carbon-based sheet material uses graphite oxide prepared by the Hummer method as a precursor, and the prepared graphite oxide is dispersed in deionized water at a concentration of 10 mg / ml, and the ultrasonic stirring is continued for 8 Hours, condensed to solid state with liquid nitrogen, placed in a freeze dryer for 24 hours of freeze-drying process, until the solvent was completely removed; the above-mentioned dried samples were dispersed in concentrated nitric acid solution for deep oxidation, and condensed at 60 degrees Celsius under reflux conditions Under the oxidation reaction for 6 hours, wash, filter and dry for later use; disperse the above sample in deionized water according to the concentration of 10 mg per ml, add boric acid, the molar ratio of boron element to carbon is 2:1, and fully stir at 80 degrees Celsius for 4 hours, then condensed to a solid state with liquid nitrogen, placed in a freeze dryer and c...
Embodiment 3
[0044] a, Preparation of carbon-based sheet material The carbon-based sheet material uses graphite oxide prepared by the Hummer method as a precursor, and the prepared graphite oxide is dispersed in deionized water at a concentration of 1 mg / ml, and the ultrasonic stirring is continued for 2 Hours, condensed to solid state with liquid nitrogen, placed in a freeze dryer for 24 hours of freeze-drying process, until the solvent was completely removed; the above-mentioned dried samples were dispersed in concentrated nitric acid solution for deep oxidation, and condensed at 50 degrees Celsius under reflux conditions Under the oxidation reaction for 4 hours, wash, filter and dry for later use; disperse the above sample in deionized water according to the concentration of 20 mg per ml, add ferric chloride, the molar ratio of iron element to carbon is 1:5, fully Stir for 4 hours, then condense to a solid state with liquid nitrogen, place in a freeze dryer for 24 hours of freeze-drying ...
PUM
| Property | Measurement | Unit |
|---|---|---|
| Thickness | aaaaa | aaaaa |
| The average diameter | aaaaa | aaaaa |
| Thickness | aaaaa | aaaaa |
Abstract
Description
Claims
Application Information
Login to View More