Monocrystalline silicon preparation method, solar cell and photovoltaic module
A technology for solar cells and single crystal silicon, applied in the field of solar cells, can solve the problems of solar cell light decay limiting battery replacement efficiency, etc., and achieves the advantages of solving the light decay problem, solving the resistivity distribution problem of gallium single crystal, and improving the defect distribution. Effect
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Embodiment 1
[0036] This embodiment provides a method for preparing gallium-doped nitrogen-doped single crystal silicon, comprising the following steps:
[0037] (1) Loading
[0038] The gallium-containing dopant source and the polysilicon material are mixed and charged into the single crystal furnace. Optionally, the gallium-containing dopant source includes, but is not limited to, gallium simple substance, gallium-containing compound, gallium-containing alloy, and the like. In some embodiments, in order to introduce other impurities in the dopant source during crystal pulling, preferably, the gallium-containing dopant source uses gallium simple substance.
[0039] Specifically, a mixture of gallium simple substance and polycrystalline silicon material is placed in a quartz crucible in a single crystal furnace.
[0040] In some embodiments, the gallium-containing dopant source and the polysilicon material can be added in various ways. For example, it can be added through a re-feeding b...
Embodiment 2
[0062] This embodiment provides gallium-doped and nitrogen-doped Czochralski monocrystalline silicon rods prepared by means of multiple feeding cylinders.
[0063] (1) Loading
[0064] Mix gallium as a dopant with polysilicon, put the mixed material in a quartz crucible, and send them together into a single-crystal re-injection furnace; the mixed material of polysilicon and gallium needs to be placed in a quartz crucible.
[0065] (2) Molten silicon
[0066] Vacuum the single crystal furnace. After vacuuming, nitrogen and argon from independently adjustable nitrogen source and argon source are passed into the single crystal furnace through a three-way valve, and the ratio of nitrogen to argon is adjusted to 0.8. At the beginning of silicon melting, the heater adjusts the rotation speed of the quartz crucible. The pressure in the cavity of the single crystal furnace is maintained at 0.7 kPa by controlling the opening of the throttle valve of the vacuum pump.
[0067] At the ...
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