Phase-change temperature-regulating fiber blended yarn
A technology of blended yarn and temperature-regulating fiber, which is applied in fiber treatment, fiber chemical characteristics, yarn, etc., can solve problems such as unsatisfactory moisture absorption and air permeability, poor temperature-regulating effect, and low mechanical strength, so as to improve biocompatibility Good stability and degradability, avoiding agglomeration and precipitation
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Embodiment 1
[0047] S1. Preparation of spinning stock solution and related raw materials:
[0048] S2, preparation of phase-change thermoregulation microcapsules:
[0049] Mix paraffin, alkane, superfine iron powder, graphite powder, emulsifier A and add deionized water, keep the constant temperature at 60°C, and disperse at a high speed at 3000r / min; then slowly add 10% citric acid solution to adjust the pH value 3. React for 3 hours, and when the temperature drops to 60°C, emulsion A is obtained;
[0050] Add methyl-2,4-diisocyanate, diethylenetriamine and catalyst to emulsion A, continue to maintain a constant temperature of 60°C, and slowly add piperazine and emulsifier B dropwise, and emulsify at a high speed at 3000r / min. Continue constant temperature for 1h to obtain the phase change thermoregulation microcapsules;
[0051] S3, preparation of modified nano-silver hydrogel:
[0052] Preparation of gel wall: Mix F127 and F68 evenly, slowly add ethylparaben solution while stirring, ...
Embodiment 2
[0065] S1. Preparation of spinning stock solution and related raw materials:
[0066] S2, preparation of phase-change thermoregulation microcapsules:
[0067] Mix paraffin, alkane, superfine iron powder, graphite powder, emulsifier A and add deionized water, keep the constant temperature at 65°C, and disperse at a high speed at 3000r / min; then slowly add 10% citric acid solution to adjust the pH value 4. React for 3 hours, and when the temperature drops to 63°C, emulsion A is obtained;
[0068] Add methyl-2,4-diisocyanate, diethylenetriamine and catalyst to emulsion A, continue to maintain a constant temperature of 63°C, and slowly add piperazine and emulsifier B dropwise, and emulsify at a high speed at 3000r / min. Continue constant temperature for 1.2h to obtain the phase change thermoregulation microcapsules;
[0069] S3, preparation of modified nano-silver hydrogel:
[0070] Preparation of the gel wall: Mix F127 and F68 evenly, slowly add ethylparaben solution while stir...
Embodiment 3
[0083] S1. Preparation of spinning stock solution and related raw materials:
[0084] S2, preparation of phase-change thermoregulation microcapsules:
[0085]Mix paraffin, alkane, superfine iron powder, graphite powder, emulsifier A and add deionized water, keep the constant temperature at 70°C, and disperse at a high speed at 3000r / min; then slowly add 10% citric acid solution to adjust the pH value 5. React for 3 hours, and when the temperature drops to 65°C, emulsion A is obtained;
[0086] Add methyl-2,4-diisocyanate, diethylenetriamine and catalyst to emulsion A, continue to maintain a constant temperature of 65°C, and slowly add piperazine and emulsifier B dropwise, and emulsify at a high speed at 3000r / min. Continue constant temperature for 1.5h to obtain the phase change thermoregulation microcapsules;
[0087] S3, preparation of modified nano-silver hydrogel:
[0088] Preparation of gel wall: Mix F127 and F68 evenly, slowly add ethylparaben solution while stirring,...
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