Phase-change temperature-regulating fiber blended yarn

A technology of blended yarn and temperature-regulating fiber, which is applied in fiber treatment, fiber chemical characteristics, yarn, etc., can solve problems such as unsatisfactory moisture absorption and air permeability, poor temperature-regulating effect, and low mechanical strength, so as to improve biocompatibility Good stability and degradability, avoiding agglomeration and precipitation

Active Publication Date: 2020-09-15
JIANGYIN HAOYE TEXTILE
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] The object of the present invention is to provide a kind of phase-change temperature-regulating fiber blended yarn and its preparation method to solve the problems in the prior art that the products have poor hand feeling, are not resistant to washing, have poor temperature-regulating effect, unsatisfactory moisture absorption and air permeability, and low mechanical strength. low level problem

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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  • Phase-change temperature-regulating fiber blended yarn

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0047] S1. Preparation of spinning stock solution and related raw materials:

[0048] S2, preparation of phase-change thermoregulation microcapsules:

[0049] Mix paraffin, alkane, superfine iron powder, graphite powder, emulsifier A and add deionized water, keep the constant temperature at 60°C, and disperse at a high speed at 3000r / min; then slowly add 10% citric acid solution to adjust the pH value 3. React for 3 hours, and when the temperature drops to 60°C, emulsion A is obtained;

[0050] Add methyl-2,4-diisocyanate, diethylenetriamine and catalyst to emulsion A, continue to maintain a constant temperature of 60°C, and slowly add piperazine and emulsifier B dropwise, and emulsify at a high speed at 3000r / min. Continue constant temperature for 1h to obtain the phase change thermoregulation microcapsules;

[0051] S3, preparation of modified nano-silver hydrogel:

[0052] Preparation of gel wall: Mix F127 and F68 evenly, slowly add ethylparaben solution while stirring, ...

Embodiment 2

[0065] S1. Preparation of spinning stock solution and related raw materials:

[0066] S2, preparation of phase-change thermoregulation microcapsules:

[0067] Mix paraffin, alkane, superfine iron powder, graphite powder, emulsifier A and add deionized water, keep the constant temperature at 65°C, and disperse at a high speed at 3000r / min; then slowly add 10% citric acid solution to adjust the pH value 4. React for 3 hours, and when the temperature drops to 63°C, emulsion A is obtained;

[0068] Add methyl-2,4-diisocyanate, diethylenetriamine and catalyst to emulsion A, continue to maintain a constant temperature of 63°C, and slowly add piperazine and emulsifier B dropwise, and emulsify at a high speed at 3000r / min. Continue constant temperature for 1.2h to obtain the phase change thermoregulation microcapsules;

[0069] S3, preparation of modified nano-silver hydrogel:

[0070] Preparation of the gel wall: Mix F127 and F68 evenly, slowly add ethylparaben solution while stir...

Embodiment 3

[0083] S1. Preparation of spinning stock solution and related raw materials:

[0084] S2, preparation of phase-change thermoregulation microcapsules:

[0085]Mix paraffin, alkane, superfine iron powder, graphite powder, emulsifier A and add deionized water, keep the constant temperature at 70°C, and disperse at a high speed at 3000r / min; then slowly add 10% citric acid solution to adjust the pH value 5. React for 3 hours, and when the temperature drops to 65°C, emulsion A is obtained;

[0086] Add methyl-2,4-diisocyanate, diethylenetriamine and catalyst to emulsion A, continue to maintain a constant temperature of 65°C, and slowly add piperazine and emulsifier B dropwise, and emulsify at a high speed at 3000r / min. Continue constant temperature for 1.5h to obtain the phase change thermoregulation microcapsules;

[0087] S3, preparation of modified nano-silver hydrogel:

[0088] Preparation of gel wall: Mix F127 and F68 evenly, slowly add ethylparaben solution while stirring,...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Abstract

The invention discloses a phase-change temperature-regulating fiber blended yarn and a preparation method thereof. The preparation method comprises the following steps of firstly, mixing paraffin hydrocarbon, graphite powder and methyl-2, 4-diisocyanate, and stirring at a high speed to obtain a phase-change temperature-regulating microcapsule; adding the prepared phase-change temperature-regulating microcapsule into nano-silver hydrogel to obtain modified nano-silver hydrogel; adding chitosan into sodium alginate hydrogel to obtain modified sodium alginate hydrogel; mixing the modified nano-silver hydrogel and the modified sodium alginate hydrogel into a spinning solution, and performing electrostatic spinning to obtain composite fibers; and spirally twisting the composite fibers, wool fibers and combed cotton to obtain the phase-change temperature-regulating fiber blended yarn. According to the phase-change temperature-adjusting fiber blended yarn and the preparation method thereof, the prepared phase-change temperature-adjusting fiber blended yarn has good temperature-adjusting and antibacterial properties, is more washable, keeps good water absorption and air permeability of fabric, and has high practicability.

Description

technical field [0001] The invention relates to the technical field of blended yarns, in particular to a phase-change temperature-regulating fiber blended yarn and a preparation method thereof. Background technique [0002] Phase-change temperature-regulating fiber blended yarn refers to a high-tech fiber blended yarn that can respond to external temperature changes obtained by blending phase-change temperature-regulating fibers with other types of yarns. The fabric made of the blended yarn can undergo phase reversible reactions according to temperature changes, thereby improving the comfort of clothing. When the temperature rises, it absorbs and stores heat, and the phase-change substance changes from solid to liquid. When the temperature drops, the stored heat is released, the phase change material changes from liquid to solid, and the temperature around the fiber is kept constant to a certain extent through the heat-absorbing and exothermic process. This performance is n...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D02G3/04D01F8/08D01F8/10D01F1/10D01D5/00
CPCD01D5/0015D01F1/10D01F1/103D01F8/08D01F8/10D02G3/04D10B2201/02D10B2211/02
Inventor 孙千涵王文娟许露蓉
Owner JIANGYIN HAOYE TEXTILE
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