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Superconducting graphite electrode nano antioxidant and preparation method thereof

A graphite electrode and anti-oxidant technology, which is applied in electric heating devices, electrical components, heating through discharge, etc., can solve the problems of insufficient anti-oxidation properties of antioxidants, and achieve the effects of improving anti-oxidation performance, prolonging service life, and reducing loss

Active Publication Date: 2020-11-06
北京中科原创节能环保科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0003] The present invention proposes a superconducting graphite electrode nano-antioxidant and its preparation method, which solves the problem that antioxidants still have insufficient oxidation resistance in the prior art

Method used

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  • Superconducting graphite electrode nano antioxidant and preparation method thereof

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Effect test

Embodiment 1

[0023] A preparation method of superconducting graphite electrode nano antioxidant, comprising the following steps:

[0024] A, prepare 95 parts of water, 30 parts of ceramic powder, 22 parts of graphene, 20 parts of polyethylene glycol, 10 parts of stabilizer, 8 parts of antioxidant additives, 12 parts of polyvinyl alcohol, and take each component for later use; Oxidation aids include calcium boride, vanadium diboride, and sodium dihydrogen phosphate with a mass ratio of 2:1:1; stabilizers include meglumine and zirconium nitride with a mass ratio of 1.2:1; ceramic powder consists of the following weight The composition of parts: 15 parts of cerium oxide, 11 parts of titanium dioxide, 12 parts of aluminum oxide;

[0025] B. Grinding the ceramic powder weighed in step A to a particle size of 80nm, adding polyethylene glycol to obtain a ceramic powder slurry;

[0026] C, adding step B ceramic powder slurry and graphene into water to obtain a premixed solution;

[0027] D. Add ...

Embodiment 2

[0029] A preparation method of superconducting graphite electrode nano antioxidant, comprising the following steps:

[0030] A, prepare 80 parts of water, 40 parts of ceramic powder, 20 parts of graphene, 25 parts of polyethylene glycol, 6 parts of stabilizer, 10 parts of antioxidant additives, 10 parts of polyvinyl alcohol, and take each component for later use; Oxidation aids include calcium boride, vanadium diboride, and sodium dihydrogen phosphate with a mass ratio of 2:1.2:1; stabilizers include meglumine and zirconium nitride with a mass ratio of 1:1; ceramic powder consists of the following weight The composition of parts: 20 parts of cerium oxide, 10 parts of titanium dioxide, 14 parts of aluminum oxide;

[0031] B. Grinding the ceramic powder weighed in step A to a particle size of 50nm, adding polyethylene glycol to obtain a ceramic powder slurry;

[0032] C, adding step B ceramic powder slurry and graphene into water to obtain a premixed liquid;

[0033] D. Add an...

Embodiment 3

[0035] A preparation method of superconducting graphite electrode nano antioxidant, comprising the following steps:

[0036] A, prepare 100 parts of water, 20 parts of ceramic powder, 25 parts of graphene, 10 parts of polyethylene glycol, 12 parts of stabilizer, 5 parts of antioxidant additives, 15 parts of polyvinyl alcohol, and take each component for later use; Oxidation aids include calcium boride, vanadium diboride, and sodium dihydrogen phosphate with a mass ratio of 2:0.8:1; stabilizers include meglumine and zirconium nitride with a mass ratio of 1.32:1; ceramic powder consists of the following weight The composition of parts: 10 parts of cerium oxide, 15 parts of titanium dioxide, 5 parts of aluminum oxide;

[0037] B. Grinding the ceramic powder weighed in step A to a particle size of 100nm, adding polyethylene glycol to obtain a ceramic powder slurry;

[0038] C, adding step B ceramic powder slurry and graphene into water to obtain a premixed liquid;

[0039] D. Ad...

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Abstract

The invention belongs to the technical field of graphite electrodes, and provides a superconducting graphite electrode nano antioxidant, which is prepared from the following components by weight: 80-100 parts of water, 20-40 parts of ceramic powder, 20-25 parts of graphene, 10-25 parts of polyethylene glycol, 6-12 parts of a stabilizer, 5-10 parts of an antioxidant aid and 10-15 parts of polyvinylalcohol. The antioxidant aid comprises calcium boride, vanadium diboride and sodium dihydrogen phosphate in a mass ratio of 2:(0.8-1.2):1. The preparation method includes: grinding the weighed ceramic powder to a particle size of 50-100nm, and adding polyethylene glycol to obtain ceramic powder slurry; adding the ceramic powder slurry and graphene into a solvent to obtain a premixed solution; andsequentially adding the antioxidant aid, the stabilizer and polyvinyl alcohol into the premixed solution, and performing mixing to obtain the superconducting graphite electrode nano antioxidant. By means of the technical scheme, the problem that in the prior art, the oxidation resistance of a graphite electrode nano antioxidant is not good enough is solved.

Description

technical field [0001] The invention belongs to the technical field of graphite electrodes, and relates to a superconductive graphite electrode nano antioxidant and a preparation method thereof. Background technique [0002] Graphite electrode is an important conductive material used in the field of metallurgy. Graphite electrodes are mainly used in electric furnace steelmaking. Electric furnace steelmaking uses graphite electrodes to introduce current into the furnace. The strong current passes through the gas at the lower end of the electrode to generate arc discharge, and the heat generated by the arc is used. However, the structure of the graphite electrode is not an ideal lattice structure. It has certain lattice defects, and there are also some impurities, unsaturated bonds and internal stress. These parts have a relatively strong ability to absorb and react to oxygen. This provides active sites for graphite electrodes, and these active sites begin to undergo oxidation...

Claims

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Application Information

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IPC IPC(8): C09D1/00C09D7/48C09D7/61C09D7/65C09D7/63H05B7/085
CPCC09D1/00C09D7/48C09D7/61C09D7/65C09D7/63H05B7/085
Inventor 于文齐熊进勇
Owner 北京中科原创节能环保科技有限公司
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