Li3PS4 solid electrolyte, solid mixed electrolyte, all-solid-state lithium-sulfur battery and production method thereof
A solid-state electrolyte, lithium-sulfur battery technology, applied in non-aqueous electrolyte batteries, solid electrolytes, lithium batteries, etc., to achieve the effects of improved performance, simple process, and excellent electrical conductivity
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Embodiment 1
[0055] Embodiment 1 (preparation of Li with DMC as organic solvent 3 P.S. 4 (lithium thiophosphate)):
[0056] Will Li 2 S (0.3827 g), P 2 S 5 (0.6170 g; Li 2 S:P 2 S 5 Molar ratio=3:1), 4 mm zirconia balls (30 g) and DMC (20 ml) were mixed in a 45 mL polypropylene centrifuge tube; shaken at a speed of 1500 rpm for 24 h in a dry Ar atmosphere, the amplitude was about Then, the test tube was sealed and centrifuged at 10,000rpm for 5 minutes, decanted; the solid phase was evacuated at room temperature, and then evacuated at 190°C for 2h at low pressure using a rotary vacuum pump to obtain a white powder product .
Embodiment 2
[0057] Embodiment 2 (preparation of Li with EA as organic solvent 3 P.S. 4 (lithium thiophosphate)):
[0058] Will Li 2 S (0.3827 g), P 2 S 5 (0.6170 g; Li 2 S:P 2 S 5 molar ratio=3:1), 4mm zirconia balls (30g) and EA (20ml) were mixed in a 45mL polypropylene centrifuge tube; shaken at a speed of 1500rpm in a dry Ar atmosphere for 24h, the amplitude was about Then, the test tube was sealed and centrifuged at 10,000rpm for 5 minutes, decanted; the solid phase was evacuated at room temperature, and then evacuated at 160°C for 2h at low pressure using a rotary vacuum pump to obtain a white powder product .
Embodiment 3
[0059] Embodiment 3 (preparation of Li with MPK as organic solvent 3 P.S. 4 (lithium thiophosphate)):
[0060] Will Li 2 S (0.3827 g), P 2 S 5 (0.6170 g; Li 2 S:P 2 S 5 Molar ratio=3:1), 4 mm zirconia balls (30 g) and MPK (20 ml) were mixed in a 45 mL polypropylene centrifuge tube; shaken at a speed of 1500 rpm for 24 h in a dry Ar atmosphere, with an amplitude of approx. Then, the test tube was sealed and centrifuged at 10,000rpm for 5 minutes, decanted; the solid phase was evacuated at room temperature, and then evacuated at 160°C for 2h at low pressure using a rotary vacuum pump to obtain a white powder product .
[0061] The following is the test characterization part:
[0062] (1) Thermogravimetric (TG) analysis
[0063] The TG curves of the samples prepared using MPK, EA and DMC are plotted in the attached figure 2 , where the horizontal axis is temperature (°C), and the vertical axis is weight change (%). At 250 °C, the weight losses of MPK, EA and DMC samp...
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