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Battery material roasting cooling system in inert atmosphere and application method thereof

A battery material and inert atmosphere technology, which is applied in the field of battery material preparation devices, can solve the problems affecting the normal process and cycle of battery material preparation, the inability to obtain fine grain crystallinity, and the electrode material is easily oxidized by air, so as to improve energy efficiency. Utilization rate, improvement of final performance, effect of enhanced warm-up effect

Active Publication Date: 2021-06-01
CENT SOUTH UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

After the former takes out the electrode material, the high-temperature electrode material placed in the air is easily oxidized by the air, which makes it difficult for the obtained electrode material to meet the requirements; the latter is naturally cooled in an argon atmosphere, but the cooling cycle is too long, which affects the battery material. The normal process and cycle of preparation will also cause too much waste of argon resources, and products with fine grains and high crystallinity cannot be obtained, and a large amount of heat converted from electric energy in the tube furnace will be directly dissipated, which is not conducive to energy consumption. maximize the use of

Method used

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  • Battery material roasting cooling system in inert atmosphere and application method thereof
  • Battery material roasting cooling system in inert atmosphere and application method thereof
  • Battery material roasting cooling system in inert atmosphere and application method thereof

Examples

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Embodiment 1

[0062] see figure 1 , which shows a battery material roasting cooling system under an inert atmosphere, the roasting cooling system includes a battery material roasting device and a battery material inert atmosphere cooling device.

[0063] The battery material roasting device includes a tube furnace 69 for roasting the battery material 108, which has an internal roasting area 68 inside. Specifically, the tube furnace 69 is an open tube furnace with dual temperature zones.

[0064] The battery material inert atmosphere cooling device is mainly composed of three parts: a radiation-convection comprehensive cooling and heat recovery device, a semiconductor module thermoelectric power generation device, and an argon preheating and recycling device.

[0065] Radiation-convection comprehensive cooling and heat recovery device is mainly composed of vortex tube cold end 11, cooling chamber 10, water cooling cooling interlayer 15, small cooling water pump 20, heat transfer oil chamber ...

Embodiment 2

[0109] This embodiment is basically the same as Embodiment 1, the main difference is: as Figure 8 As shown, in the present embodiment, the semiconductor thermoelectric power generation module 35 includes: two n-type semiconductors 91 and two p-type semiconductors 92, and the n-type semiconductors 91 and p-type semiconductors 92 are arranged alternately (that is, corresponding to the first one from left to right in the figure). One and the third are p-type semiconductors 92, the second and the fourth are n-type semiconductors 91), and adjacent n-type semiconductors 91 and p-type semiconductors 92 are arranged at intervals; two semiconductor hot end metal plates 90 and three A semiconductor cold-end metal plate 102, a semiconductor hot-end metal plate 90 and a semiconductor cold-end metal plate 102 are respectively located on both sides of the n-type semiconductor 91 and the p-type semiconductor 92, and the adjacent n-type semiconductor 91 and the p-type semiconductor 92 form a ...

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Abstract

The invention discloses a battery material roasting cooling system in an inert atmosphere, comprising an inert gas bottle, a vortex tube, an inert atmosphere cooling box, an inert gas storage bag, a tubular furnace, a semiconductor hot end heat conduction ceramic plate, a semiconductor thermoelectric power generation module, and a tubular furnace waste heat transfer mechanism. The invention further discloses an application method of the roasting cooling system; radiation-convection comprehensive heat exchange is carried out on a battery material in a cooling cavity; meanwhile, heat in the tubular furnace is recycled through the tubular furnace waste heat transfer mechanism; the semiconductor hot end heat conduction ceramic plate is used for absorbing heat, and the semiconductor temperature difference power generation module is used for generating power so as to provide power for fluid conveying in the roasting cooling system; and previous inert gas is blown into an internal roasting area during next roasting. Aiming at the particularity that the battery material cannot be naturally cooled, the battery material is roasted in the inert atmosphere and cooled in a closed environment, so that the performance of the battery material is improved, and waste heat in the tubular furnace can be fully recycled.

Description

technical field [0001] The invention relates to the technical field of battery material preparation devices, in particular to a battery material roasting and cooling system under an inert atmosphere and an application method thereof. Background technique [0002] Baking is usually required in the preparation of battery materials, and the morphology, crystal structure, and electrochemical properties of sintered products often have a great relationship with the sintering system and cooling system. Generally, rapid cooling can increase the degree of supercooling to increase the crystallinity of the material, refine the grains, and make the material have better electrochemical performance. Patent CN109148879A discloses a method for synthesizing lithium-rich manganese-based cathode materials by quenching with liquid nitrogen, which shows that increasing the cooling rate can improve the electrochemical performance of the material. [0003] At this stage, in the process of prepari...

Claims

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Application Information

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IPC IPC(8): F27B17/00F27D15/02F25B9/04F27D17/00F27D7/06H01L35/28H02N11/00
CPCF27B17/00F27D15/02F25B9/04F27D17/004F27D7/06H02N11/002H10N10/10Y02P10/25
Inventor 吴飞翔杨凌志于环宇薛智宸胡航
Owner CENT SOUTH UNIV