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Gel with high load of smoke agent and aroma substance

A smoking agent, high-load technology, used in tobacco, tobacco processing, tobacco preparation and other directions, can solve the problems of inability to bring characteristic aroma, mutual repulsion, volatilization loss of aroma components, avoid excessive dissipation, reduce raw material and Manufacturing cost, effect of reducing smoke volume

Active Publication Date: 2021-08-03
CHINA TOBACCO YUNNAN IND
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0010] Although nicotine salts have been widely used in e-cigarette liquids, there are still the following main sensory problems in e-cigarettes containing nicotine salts: when nicotine salts are heated and decomposed to form free nicotine and delivered to the atomized vapor, puff-by-puff nicotine The release behavior is inconsistent with the release behavior of the aromatizing ingredients, and it is difficult to achieve the synergistic delivery of the key aromatizing ingredients and nicotine. While bringing nicotine physiological satisfaction, it cannot bring the matching characteristic fragrance, resulting in the interaction between nicotine and flavoring substances. The sensory sensations are strong and weak, covering each other or even repelling each other, especially for volatile characteristic aroma substances, because they cannot be released stably throughout the smoking process (usually the release amount gradually decreases mouth by mouth), this sense of incongruity especially obvious
Another common problem with e-cigarettes is that during the storage of e-liquid or pods, there will inevitably be a problem of volatilization and loss of flavor components. Even closed pods also have the problem of deterioration of flavor substances.
At present, although microcapsule technology can be used to encapsulate volatile aroma components, since microcapsules mostly use sugars such as cyclodextrin as wall materials, there will be a problem caused by the wall material adhering to the heating element at the heating temperature of the electronic cigarette. burnt smell and discomfort

Method used

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  • Gel with high load of smoke agent and aroma substance
  • Gel with high load of smoke agent and aroma substance
  • Gel with high load of smoke agent and aroma substance

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0073] A method of preparation of gel of high-load changer and spices, including the following steps:

[0074] Step 1, the preparation of the gelling agent: Cinnamic acid and nicotine are soluble in the mixed solvent of water and ethanol in the mixed solvent of water and ethanol, and the mixed solvent mass ratio of cinnamic acid and ethanol dissolved thereof is 1 g: 28ml. Nicotine and the mixed solvent mass ratio of water and ethanol dissolved thereof were 1 g: 210 mL, stirred at room temperature to completely dissolve, and obtained the cinnamic acid solution and nicotine solution, and then the above two solutions were thoroughly mixed, and the mixture was obtained. The mixture was warmed to reflux, and the reaction was dried at 30 min, 160 mbar, 53 ° C, and then evaporated to drying at 36 ° C for 24 h to give a cinnametinic acid. In the mixed solvent of water and ethanol, the volume ratio of water and ethanol is 1: 5.

[0075] Step 2, the preparation of the gel:

[0076] The flav...

Embodiment 2

[0080] This example provides the application of a carrier super molecular gel prepared in the first embodiment of the present invention in a heating cigarette

[0081] The Ni Dated Salt Syrotic Molecular Gel can separately apply a single gel or different types of mixed gels in the manufacturing process of reacting cigarette and exciting pulp to heat the cigarette.

[0082] Papermaking method heating the cigarette use to make tobacco:

[0083] Method 1: A quantitative cosmetic (1,2-propanediol, glycerol or two proportible mixtures) is added to the preparation of the carrier super molecular gel, and the quality of the super molecular gel and the quality of the smoke. The ratio is 6: 1, warmed to 70 ° C, gel melting into a sol, uniformly mixed, forming a mixed coating liquid containing a molten gel and a hyperkecess, and sprayed a mixed coating liquid to paper. The preparative tobacco tablet is made. Reproduction tobacco the above mixed coating liquid is applied to room temperature, ...

Embodiment 3

[0095] This example provides the application of the carried abstentive ultra molecular gel prepared in Example 1 in the electronic smoke.

[0096] The Niurota salt hypermor gel can be applied to the electronic cigarette in two ways and can be used in accordance with the actual use of a single gel or different types of mixed gels.

[0097] Method 1: After 24-36 h, a hemolecular gel prepared in an oven at a 40 ° C oven 24-36 h, after the drying gel is ground into a uniform microparticle, and a certain amount of electronic smoke is added to a certain proportion. The mixture is thoroughly stirred in the changering agent, and the cigarette is a mixed solvent of glycerol and 1,2-propanediol 1: 1 (volume ratio), and the proportion of jaca ultra molecular gels and hairy tanks is 1: 120, and after mixing is uniform. Fragrant gel-containing cosmetic or as an excipients were added to the finished tofonic mixed uniform mixed uniform as a metallogenic gel.

[0098] Smoky in the electronic ciga...

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PUM

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Abstract

The invention belongs to the field of supramolecular gels, and particularly relates to a gel with high load of a smoke agent and an aroma substance. The gel comprises a nicotine cinnamate gelling agent, and the aroma substance and a solvent dispersed in the nicotine cinnamate gelling agent. Due to the inherent high load rate of the supramolecular gel on the solvent (the smoke agent) and the aroma substance dissolved in the solvent (the smoke agent), the problem that the aroma amount and the smoke amount are insufficient when the cigarette is heated can be solved, and effective supplement of the aroma amount and the smoke amount is achieved; particularly, the semi-volatile aroma substance is fixed in the nicotine salt gel releasing nicotine in the high-temperature section, so that the volatile loss of fragrance in the preheating stage or the low-temperature heating stage can be reduced, and the attenuated fragrance can be supplemented in the middle and rear sections of smoking.

Description

Technical field [0001] The present invention belongs to the field of super molecular gel, and is specifically related to a highly loaded cosmetic and spices. Background technique [0002] Alkaline nicotine can react with the carboxyl group of organic acid to generate nicotinuclearboxylates. Nicotine comprises a pyridine ring and a pyrrole ring, wherein the pyrrolei nitrogen is more basic, which is tended to react with a carboxylate of the carboxylic acid to generate nicotine salts, and the alkaline of pyridine is weak, and it is substantially ionized effect. Non-covalent effects such as hydrogen bonds are combined with carboxylic acids. Naturally containing a variety of carboxylic acid nuron salts in the tobacco leaves, nicotine salts can be divided into 1: 1 acid base ratio, 2: 1 acid base ratio, 3: 1 acid base ratio, 3: 1 acid base ratio, 3: 1 acid base ratio, 3: 1 acid base ratio, 3: 1 acid base ratio Among them, common nicotarboxylabic acid salts include tartaric acid nincton...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A24B3/14A24B15/26A24B15/28A24B15/167
CPCA24B3/14A24B15/26A24B15/28A24B15/167
Inventor 巩效伟韩熠赵伟杨柳朱东来张霞李寿波李廷华吕茜洪鎏李志强尤俊衡秦云华
Owner CHINA TOBACCO YUNNAN IND