Double-sided scaffold and preparation method and application thereof
A double-sided, composite fiber technology, applied in the field of biomaterials, stem cells, and tissue repair research, can solve the problems of degradable polymer materials such as lack of cell recognition signals, mechanical properties and easy degradation to limit applications, unfavorable cell recognition and adhesion, etc. Achieving good biocompatibility, avoiding incomplete periodontal regeneration, and good migration ability
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Embodiment 1
[0105] This embodiment provides a double-sided bracket, which is prepared by the following preparation method:
[0106] (1) configure the chitosan collagen spinning solution containing RGD: 3wt% chitosan (M W 3.1×10 5 ~3.75×10 5 Da), 3wt% collagen (M W 1.2×10 6 Da), 0.50wt% polyethylene oxide (M w 9.5×10 4 Da), 0.02mg / mL RGD (Arg-Gly-Asp) and 90wt% aqueous acetic acid were mixed to obtain a spinning solution;
[0107] Add the spinning solution into a 10mL needle tube, use a 23-gauge needle, at an extrusion rate of 0.5cm / min, carry out electrospinning under the conditions of low pressure -2kV and high voltage 20kV, and receive the composite fiber obtained by spinning with aluminum foil ; and then washed three times with ethanol and three times with deionized water; finally dried at -80°C for 18 hours to obtain the chitosan collagen composite fiber layer;
[0108] (2) Take 2g of chitosan collagen composite fiber layer and place it in 5mL of 1mg / mL hydroxyapatite depositi...
Embodiment 2
[0115] This embodiment provides a double-sided stent, and the only difference from Embodiment 1 is that in step (1), the content of polyethylene oxide in the spinning solution is 0.25 wt%, and the content of other components and the preparation steps are the same. example 1.
[0116] Figure 5 For the scanning electron micrograph of the chitosan collagen composite fiber that embodiment 2 provides, as Figure 5 As shown, the PEO content is less, the fiber diameter is lower, but the uniformity of the fiber is better.
Embodiment 3
[0118] This embodiment provides a double-sided stent, and the only difference from Embodiment 1 is that in step (1), the content of polyethylene oxide in the spinning solution is 0.75wt%, and the content of other components and the preparation steps are the same. example 1.
[0119] Figure 6 For the scanning electron micrograph of the chitosan collagen composite fiber that embodiment 3 provides, as Figure 6 As shown, the higher the PEO content, the higher the fiber diameter, but the uniformity of the fiber has decreased.
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