Attapulgite-based acid soil conditioner and preparation method thereof
A technology of soil conditioner and attapulgite, which is applied in the field of attapulgite acidic soil conditioner and its preparation, and can solve problems such as environmental pollution, energy consumption, and increased cost of soil improvement
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Embodiment 1
[0029] A preparation method of attapulgite-based acidic soil conditioner, the specific steps are as follows:
[0030] (1) First use urea, ferric chloride hexahydrate and succinic acid as raw materials to make doped graphite phase carbon nitride, and then add doped graphite phase carbon nitride to the mixed aqueous solution of sodium molybdate-thioacetamide, Hydrothermal reaction to obtain doped graphite phase carbon nitride-molybdenum disulfide composite;
[0031] (2) 1 kg of fresh Enteromorpha pulverized and added to 60 kg of water, beaten to obtain Enteromorpha pulp, heated and pressurized to obtain pretreated Enteromorpha pulp;
[0032] (3) Finally, add 55kg attapulgite, 2kg soda lime and 0.05kg doped graphite phase carbon nitride-molybdenum dioxide compound to the pretreated Enteromorpha pulp, dipping treatment, and drying to obtain the conditioner .
[0033] In step (1), the preparation method of carbon nitride doped with graphite phase is as follows: First, 10 kg of ur...
Embodiment 2
[0043] A preparation method of attapulgite-based acidic soil conditioner, the specific steps are as follows:
[0044] (1) First use urea, ferric chloride hexahydrate and succinic acid as raw materials to make doped graphite phase carbon nitride, and then add doped graphite phase carbon nitride to the mixed aqueous solution of sodium molybdate-thioacetamide, Hydrothermal reaction to obtain doped graphite phase carbon nitride-molybdenum disulfide composite;
[0045] (2) 1 kg of fresh Enteromorpha pulverized and added to 70 kg of water, beaten to obtain Enteromorpha pulp, heated and pressurized to obtain pretreated Enteromorpha pulp;
[0046] (3) Finally, add 45kg attapulgite, 3kg soda lime and 0.03kg doped graphite phase carbon nitride-molybdenum dioxide compound to the pretreated Enteromorpha pulp, dipping treatment, and drying to obtain the conditioner .
[0047] In step (1), the preparation method of carbon nitride doped with graphite phase is as follows: First, 10 kg of ur...
Embodiment 3
[0057] A preparation method of attapulgite-based acidic soil conditioner, the specific steps are as follows:
[0058] (1) First use urea, ferric chloride hexahydrate and succinic acid as raw materials to make doped graphite phase carbon nitride, and then add doped graphite phase carbon nitride to the mixed aqueous solution of sodium molybdate-thioacetamide, Hydrothermal reaction to obtain doped graphite phase carbon nitride-molybdenum disulfide composite;
[0059] (2) Add 1 kg of fresh Enteromorpha into 65 kg of water after pulverization, beating to obtain Enteromorpha pulp, heat and pressurize to obtain pretreated Enteromorpha pulp;
[0060] (3) Finally, add 50kg attapulgite, 2.5kg soda lime and 0.04kg doped graphite phase carbon nitride-molybdenum dioxide compound to the pretreated Enteromorpha pulp, dipping treatment, drying, and obtain the conditioning agent.
[0061] In step (1), the preparation method of carbon nitride doped with graphite phase is as follows: First, 10...
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