A kind of thermal insulation coating and preparation method thereof
A thermal insulation and coating technology, which is applied in the direction of anti-corrosion coatings, fireproof coatings, coatings, etc., can solve the problems of poor adhesion between thermal insulation coatings and coke oven bodies, and achieve low thermal conductivity, strong adhesion, excellent The effect of thermal insulation performance
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[0044] Another object of the present invention is to provide a method for preparing the above-mentioned thermal insulation coating, the preparation method comprising the following steps:
[0045] S1: preparing an organosilicon modification solution;
[0046] S2: preparing nano hollow microbeads;
[0047] S3: preparing fumed silica gel;
[0048] S4: According to parts by weight, add 25-35 parts of nano-hollow microbeads to 15-20 parts of organosilicon modification solution, and mix uniformly to obtain solution A;
[0049] S5: In terms of parts by weight, add 10 to 20 parts of nano silicate inorganic binder, 10 to 15 parts of fumed silica gel, 5 to 15 parts of inorganic hollow fiber powder, 2 -8 parts of nano-rare earth oxide, 1-5 parts of additives, and 0.5 parts of water are uniformly mixed to obtain a thermal insulation coating.
[0050] For the thermal insulation coating provided by this application, firstly, the prepared nano hollow microspheres are fully mixed with the ...
Embodiment 1
[0067] This embodiment provides a method for preparing a thermal insulation coating, comprising the following steps:
[0068] S1: In parts by weight, 1.5 parts of methyl monomer and 1 part of tetrafluoroethylene monomer were polymerized at 85° C. to obtain a silicone modified solution;
[0069] S21: According to parts by weight, mix 1 part of BN-1000 stabilizer with 5 parts of ethanol to obtain solution B;
[0070] S22: According to parts by weight, 15 parts of nano-ceramic hollow microspheres are added to solution B, and mixed uniformly to obtain solution C;
[0071] S23: Add 1 part of neodymium nitrate and 5 parts of nickel nitrate to the solution C in parts by weight, heat to 30° C., and mix uniformly to obtain a dispersed liquid;
[0072] S24: After filtering, cleaning and drying the dispersed liquid in sequence, sintering at 600° C. for 5 hours to obtain nano hollow microspheres; the nano hollow microspheres are nano hollow microspheres coated with neodymium nitrate and ...
Embodiment 2
[0081] This embodiment provides a method for preparing a thermal insulation coating, comprising the following steps:
[0082] S1: In parts by weight, 1.5 parts of methyl monomer and 1 part of tetrafluoroethylene monomer were polymerized at 85° C. to obtain a silicone modified solution;
[0083] S21: According to parts by weight, mix 5 parts of BN-1000 stabilizer with 1 part of ethanol to obtain solution B;
[0084] S22: According to parts by weight, 25 parts of nano-ceramic hollow microspheres are added into solution B, and mixed evenly to obtain solution C;
[0085] S23: Add 5 parts of neodymium nitrate and 1 part of nickel nitrate to the solution C in parts by weight, heat to 35° C., and mix uniformly to obtain a dispersed liquid;
[0086] S24: After filtering, washing and drying the dispersed liquid in sequence, sintering at 900° C. for 3 hours to obtain nano hollow microspheres; the nano hollow microspheres are nano hollow microspheres coated with neodymium nitrate and ni...
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