Warm-keeping and moisture-absorbing composite polyester fiber with synergistic effect of skin-core components and preparation method thereof
A synergistic, composite polyester technology, applied in the direction of fiber chemical characteristics, conjugated synthetic polymer rayon, rayon manufacturing, etc., to achieve high-efficiency light-to-heat conversion, reduce frictional resistance, and good lubricity
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Embodiment 1
[0072] A method for preparing a warm-keeping and moisture-absorbing composite polyester fiber with synergistic effect of sheath and core components, comprising:
[0073] Step 1: Preparation of modified polyester A.
[0074] (1.1) Esterification reaction:
[0075] Esterification of dibasic acid, mixed diol and catalyst according to a certain molar ratio;
[0076] The dibasic acid is one of terephthalic acid, isophthalic acid, succinic acid, adipic acid, suberic acid and sebacic acid;
[0077] The mixed glycol is composed of a short-chain glycol and a long-chain glycol, the short-chain glycol is one of ethylene glycol, propylene glycol and butanediol, and the long-chain glycol is diethylene glycol , one of pentanediol and hexanediol;
[0078] The molar ratio of described dibasic acid and mixed dibasic alcohol is 1:1.1, and wherein the molar ratio of short-chain dibasic alcohol and long-chain dibasic alcohol is 4:6;
[0079] The catalyst is one of antimony ethylene glycol, an...
Embodiment 2
[0111] A method for preparing a warm-keeping and moisture-absorbing composite polyester fiber with synergistic effect of sheath and core components, comprising:
[0112] Step 1: Preparation of modified polyester A.
[0113] (1.1) Esterification reaction:
[0114] Esterification of dibasic acid, mixed diol and catalyst according to a certain molar ratio;
[0115] The dibasic acid is one of terephthalic acid, isophthalic acid, succinic acid, adipic acid, suberic acid and sebacic acid;
[0116] The mixed glycol is composed of a short-chain glycol and a long-chain glycol, the short-chain glycol is one of ethylene glycol, propylene glycol and butanediol, and the long-chain glycol is diethylene glycol , one of pentanediol and hexanediol;
[0117] The molar ratio of described dibasic acid and mixed dibasic alcohol is 1:1.5, and wherein the molar ratio of short chain dibasic alcohol and long chain dibasic alcohol is 6:4;
[0118] The catalyst is one of antimony ethylene glycol, an...
Embodiment 3
[0150] A method for preparing a warm-keeping and moisture-absorbing composite polyester fiber with synergistic effect of sheath and core components, comprising:
[0151] Step 1: Preparation of modified polyester A.
[0152] (1.1) Esterification reaction:
[0153] Esterification of dibasic acid, mixed diol and catalyst according to a certain molar ratio;
[0154] The dibasic acid is one of terephthalic acid, isophthalic acid, succinic acid, adipic acid, suberic acid and sebacic acid;
[0155] The mixed glycol is composed of a short-chain glycol and a long-chain glycol, the short-chain glycol is one of ethylene glycol, propylene glycol and butanediol, and the long-chain glycol is diethylene glycol , one of pentanediol and hexanediol;
[0156] The molar ratio of described dibasic acid and mixed dibasic alcohol is 1:2.0, and wherein the molar ratio of short-chain dibasic alcohol and long-chain dibasic alcohol is 8:2;
[0157] The catalyst is one of antimony ethylene glycol, an...
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