Carbon material impregnant formula and preparation and application process thereof
A carbon material and impregnating agent technology, which is applied in the field of carbon material impregnating agent formulation and preparation and application technology, can solve the problems of unsatisfactory product purity, insufficient impregnation depth, long impregnation time, etc., and saves energy, time and production cost. Low and no pollution to the environment
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Embodiment 1
[0031] A carbon material impregnating agent. The impregnating agent is a glue solution prepared by mixing carbon materials, treatment agents and water. The specific raw material ratio is as follows:
[0032] 1. A carbon material with a total mass fraction of 30%, including 25% carbon black and 5% graphite powder;
[0033] 2. The total mass fraction is 6% of the treatment agent, including 2% of the oxidant hydrogen peroxide, 2% of the coupling agent vinyltriethoxysilane, 1% of the dispersant fatty alcohol polyoxyethylene ether sodium sulfate and 1% thickener aluminum silicate;
[0034] 3. 64% water.
[0035] Its process method concrete steps are as follows:
[0036] A. Calculate and weigh the raw material of the carbon material according to the requirements of the formula, and mix it with the dispersant to obtain the mixture I;
[0037] B. Transfer the mixture I to a ball mill for ball milling, use a medium ball with a diameter of 0.5 mm, set the rotor speed to 80 r / min, and...
Embodiment 2
[0047] The impregnating agent is a treatment agent with a total mass fraction of 35% of carbon materials (including 30% of carbon black and 5% of graphite micropowder) with a total mass fraction of 6.5% (including 2.3% of hydrogen peroxide oxidant, vinyl three 2.3% ethoxysilane coupling agent, 1.3% fatty alcohol polyoxyethylene ether sodium sulfate dispersant, 0.6% aluminum silicate thickener) and 58.5% water. Its processing method concrete steps are with embodiment 1.
[0048] The obtained air reactivity test results show that the loss rate of the anode carbon block is 4.32%, the residual rate is 95.25%, and the shedding degree is 0.52%; the current density test result is 1.31 A / cm2.
[0049] Experimental effect:
[0050] For the theoretical basis of the present invention, the following experiments are specifically carried out to prove the reliability of the inventive idea: 1. Air reactivity; 2. Current density.
[0051] Experiment 1: Air Reactivity
[0052] The air reacti...
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Abstract
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