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183results about How to "Low solvent content" patented technology

Preparation method of modified cation waterborne polyurethane emulsion containing hydrophilic and hydrophobic side long chains and product thereof

The invention relates to a preparation method of modified cation waterborne polyurethane emulsion containing hydrophilic and hydrophobic side long chains and a product thereof. The method comprises the following steps that raw materials are prepared; polyester glycol dehydration pretreatment is carried out; polyester glycol obtained after dehydration pretreatment is subjected to a prepolymerization reaction with an end alkyl polysiloxane linear body, a nonionic chain extender, a functionality chain extender and diisocyanate under catalyzing of a polymerization catalyst so that a prepolymer can be obtained; the prepolymer reacts with a nonionic chain extender and a part diluent to prepare an intermediate; the intermediate reacts with a silane coupling agent, and is emulsified to prepare the modified cation waterborne polyurethane emulsion. The product is a polyester type cation waterborne polyurethane high-polymer material containing hydrophilic and hydrophobic side long chains, wherein polysiloxane is embedded into a main chain of the material, a side chain is grafted with long-chain polyether and long-chain alkyl, and the silane coupling agent is connected into the tail end of the material; the film-forming ability is high, and serving as a film, the emulsion has obvious water-repellent, antifouling and easy dirt-removing abilities, is excellent in compatibility with a cation softening agent, and has an excellent low-temperature soft feature; the product is safe, environmentally friendly and convenient to use.
Owner:HUBEI DAYA BIOLOGICAL TECH CO LTD

Elastic waterproof polyurea coating as well as preparation method and application method thereof

The invention belongs to the technical field of coating production and particularly relates to an elastic waterproof polyurea coating as well as a preparation method and application method thereof. The coating comprises a component A and a component B, wherein the component A comprises the main ingredients of aliphatic polyisocyanate trimer and an elastic isocyanate curing agent; the component B comprises the main ingredient of dimerization type asparaginic acid ester polyurea resin; the component A and the component B are packaged independently; a base coat layer is uniformly coated with the component A and the component B. The polyurea coating provided by the invention has the advantages as follows: the construction time of the polyurea coating is prolonged, the wettability is improved, and the performance of thick coating construction is provided, so that special polyurea coating equipment and special constructors are not required, the construction is facilitated, and the formed film has excellent elasticity. The polyurea coating can be dried after being coated for two hours, is high in curing speed, can be used outdoors, has excellent water resistance and chemical corrosion resistance of a swimming pool disinfectant, and can be soaked in water for a long time without cracking and leakage.
Owner:深圳市威尔地坪材料有限公司

Preparation method and product of modified polyurethane flexible high-molecular emulsion containing side long chain alkyl

The invention relates to a preparation method and product of a modified polyurethane flexible high-molecular emulsion containing side long chain alkyl. The preparation method comprises the following steps: preparing raw materials including a polymeric monomer, a modifying agent, an auxiliary agent and water; performing dehydration pretreatment on polyether triol and polyether glycol; performing prepolymerization; performing chain extension; sealing ends; and emulsifying to prepare a modified polyurethane flexible high-molecular emulsion product containing side long chain alkyl. According to the modified polyurethane flexible high-molecular emulsion disclosed by the invention, polysiloxane chain links and polyolefin chain links are embedded into a skeleton structure of the modified polyurethane flexible high-molecular emulsion, and polyurethane high molecules are modified by using long chain alkyl. The obtained modified polyurethane flexible high-molecular emulsion containing side long chain alkyl has a certain density of long chain crosslinking and side long chain alkyl, has excellent stability, can be applied to dry coating processing of various substrate coatings and artificial leathers, and ensures that significant water-repellent and anti-fouling abilities, extremely excellent extension performance, excellent low-temperature high flexibility and anti-bending performance of product coating films can be achieved; and the product is safe and environment-friendly, and is convenient to use.
Owner:HUBEI DAYA BIOLOGICAL TECH CO LTD

Refining and reclaiming technology of tail gas absorption solvent in production of toluene diisocyanate

The invention relates to a refining and reclaiming technology of a tail gas absorption solvent in the production of toluene diisocyanate (TDI). The solvent containing little phosgene, toluene diisocyanate and di-Et-1,3-benzenedicarboxylate (DEIP) performs two-stage refinement in an atmospheric refining tower and a vacuum refining tower, and a falling-film evaporator and a storage tank are arranged between the two towers. The overhead non-condensable gas phase of the atmospheric refining tower is returned to a phosgene absorption tower to recycle phosgene, the refined solvent is drawn from theside of the atmospheric refining tower, the temperature of the tower bottom is controlled to be 3-8 DEG C higher than the boiling point of the solvent, the discharged material of the tower bottom enters the falling-film evaporator, the evaporating temperature is 20-30 DEG C higher than the boiling point of the solvent, the unevaporated material enters the storage tank for storage, the material inthe storage tank performs batch vacuum rectification under the absolute pressure of 0.1-0.25bar, and the unevaporated residual material enters the residue evaporator of a TDI device to recycle TDI and DEIP. By using the solvent refining technology provided by the invention, the useful components in the solvent can be completely recycled, and the technology has the advantages of simple and stable operation and lower cost and energy consumption.
Owner:QINGDAO UNIV OF SCI & TECH +1

Hydroxyl-containing water-based acrylic ester polymer and preparation method thereof

The invention relates to a hydroxyl-containing water-based acrylic ester polymer and a preparation method thereof. The hydroxyl-containing water-based acrylic ester polymer is synthesized by two steps of: firstly, preparing a specific hydroxyl-containing acrylic ester aqueous dispersion; and secondly, carrying out free base polymerization on the specific hydroxyl-containing acrylic ester aqueous dispersion and 10-30 parts of hydroxyl-containing acrylic ester monomers, 30-50 parts of methacrylate monomers, 0.1-0.5 part of ammonium persulfate and/or potassium persulfate initiator and 30-50 parts of deionized water, wherein the percentage of Mn is mote than or equal to 10,000; the hydroxyl-containing water-based acrylic ester polymer has low content of solvent, high content of solid, low viscosity and low acid value; and the weight ratio of the specific hydroxyl-containing acrylic ester aqueous dispersion to the monomers and the initiator used for the free base polymerization with the specific hydroxyl-containing acrylic ester aqueous dispersion is 1:(1.40-2.0) counted according to the solid content. The hydroxyl-containing water-based acrylic ester polymer can be used for preparing a dual-component waterborne polymerization coating, or can be used for preparing a waterborne amino baking coating and has the advantages of high luster of a paint film, weather resistance, corrosion resistance, low VOC (Volatile Organic Compounds) and wide application range; and a preparation process is stable and controllable.
Owner:CNOOC CHANGZHOU PAINT & COATINGS IND RES INST +1

Swelling pre-squeezing leaching preparation method for high oil-containing material

InactiveCN101235340AAvoid excessive denaturationReduces loss of lysineFatty-oils/fats productionWater contentOil content
The invention relates to a high oil-content oil material expanding prepressing leaching oil preparation method, which is characterized in that the method comprises the following steps, firstly, cleaning, cleaning oiling to remove impurities, secondly, tempering, adjusting the water content of oiling whose impurities are removed, thirdly, rolling slab, rolling oiling whose water content is adjusted into material slab, fourthly, squeezing and swelling, squeezing and swelling, the material slab, fifthly, drying, drying the material slab which is squeezed and swelled, sixthly, prepressing, prepressing the material slab which is dried to press one portion of oil, seventhly, leaching, leaching prepressed cake of the oil which is prepressed to get another portion of oil and meal from solvent extraction. A squeezing and swelling step in the invention is utilized to replace a cooking step in the existing method, which improves the quality and amounts of prepressing crude palm oil, increases handling capacity of a prepress expeller, and reduces power consumption and abrasion of a prepress expeller. The method of the invention is mainly applicable for oil preparation enterprises which utilize high oil-content oiling such as rapeseed and the like to be raw material.
Owner:中机康元粮油装备(北京)有限公司 +1

Preparing method for ultra-high molecular weight polyethylene fibers and washing device

The invention discloses a preparing method for ultra-high molecular weight polyethylene fibers. The method specifically includes the following steps that firstly, a spinning solution is prepared; secondly, spinning is conducted; thirdly, extracting is conducted; fourthly, drying is conducted; fifthly, drafting is conducted; a washing step is added between the third step and the fourth step, and according to the washing step, thread lines which are discharged from an extracting groove are washed in a washing groove, a second solvent and a residual first solvent which are carried on the surfaces of the thread lines are removed, and the washed thread lines are sent to the four step to be dried. According to the preparing method for ultra-high molecular weight polyethylene fibers, the washing technology is added after extracting in an existing preparation technology processes for ultra-high molecular weight polyethylene fibers, and the preparing method for ultra-high molecular weight polyethylene fibers has the advantages that the fibers are lower in solvent content rate, manufactured finished products are higher in strength, the hand feeling is soft, and subsequent processing is facilitated; the production process of the technology is safe, toxicity and pollution are avoided, and environment friendliness is facilitated; the solvent is recycled, the solvent dosage is reduced, and cost is saved; the technology is simple, the process is short, and operation is convenient. The invention further discloses a washing device used in the preparing method.
Owner:SURREY HI TECH INC

Polymer solution steam stripping flocculation separation method and apparatus

The invention belongs to the polymer production technical field, relating to a highly-efficient energy-saving method for separating a polymer solution of synthetic rubber, synthetic resin and plastic by stripping condensation and a device for carrying out the same. A concentration separator for polymer grainy water is arranged on a polymer grainy water pipe between a first condensation boiler and a second condensation boiler which are in serial connection in a two-boiler condensation process of a polymer solution to increase the polymer concentration of the polymer grainy water, and carry out phrase separation in the concentration separator; the concentration separator is arranged vertically, and consists of a cylindrical suspension section at the lower part, a cone-shaped transition section in the middle and a cylindrical lifting section at the upper part which are communicated; a metal wire net cage is arranged outside the export pipe of the concentration water at the bottom of the suspension section, a steam lifting pipe is arranged at the lower part of the lifting section; the device can improve the condensation effect, obviously reduces the content of the remaining solvent of polymer particles, has remarkable economic benefits, and reduces environmental pollution caused by the solvent.
Owner:FUSHUN YIKESI NEW MATERIAL

Rubber toughened SBS aldehyde removed all-purpose adhesive and preparation method thereof

The invention relates to a rubber-toughened SBS formaldehyde-free universal adhesive and the preparation method thereof. The rubber-toughened SBS formaldehyde-free universal adhesive is characterized in that the adhesive is composed of linear butadiene-styrene thermoplastic elastomer 3% to 5%, star-shaped butadiene-styrene thermoplastic elastomer 7% to 9%, styrene-butadiene rubber 2.7% to 3.7%, petroleum resin 20.8% to 24.8%, formaldehyde-removing additive 1.4% to 2.6%, antioxidant 1.2% to 1.8%, petroleum ether 37% to 43%, oil solvent 16.5% to 19.5% and essence 0.4% to 0.6%. The preparation method comprises the following steps: (1) weighting the above materials according to the ratio; (2) adding styrene-butadiene rubber in the step (1) into a mixing roll machine for plasticizing, thin-passing and discharging sheets, adding the sheet material into a vertical high-speed stirring kettle, adding the oil solvent in the step (1) into the high-speed stirring kettle, dissolving, and stirring until the sheet material is dissolved completely to obtain the semi-product; and (3) respectively adding the residual material components into the stirring kettle implementing step (2), stirring and dissolving to obtain the final product. The rubber-toughened SBS formaldehyde-free universal adhesive can remove free formaldehyde released from boards and has the remarkable effects on protecting environment and maintaining human health during house decoration.
Owner:GUANGDONG MAYDOS BUILDING MATERIALS LTD CO
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