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184results about How to "Strong film forming" patented technology

Mono-component varnish composition, preparation method and purpose thereof

The invention discloses a mono-component varnish composition, which comprises at least a polymer having a hyper branched or dendritical structure; at least one type of hydroxyl acrylic resin or hydroxyl methacrylate resin; at least one type of organosilicon-modified acrylic resins; at least a crosslinking curing agent; at least an acid catalyst; at least a rheological control agent; at least an auxiliary agent and at least a solvent; and the mono-component varnish composition has the advantages of high scratch resistance and high weather resistance. The provided mono-component varnish composition can effectively increase the smoothness of the surface of a varnish composition film, and increases the rub resistance of the film; in addition, the introduction of the organosilicon-modified acrylic resin can further increase the weatherability of the varnish composition film.
Owner:LANGFANG NIPPON PAINT +2

Preparation method of modified cation waterborne polyurethane emulsion containing hydrophilic and hydrophobic side long chains and product thereof

The invention relates to a preparation method of modified cation waterborne polyurethane emulsion containing hydrophilic and hydrophobic side long chains and a product thereof. The method comprises the following steps that raw materials are prepared; polyester glycol dehydration pretreatment is carried out; polyester glycol obtained after dehydration pretreatment is subjected to a prepolymerization reaction with an end alkyl polysiloxane linear body, a nonionic chain extender, a functionality chain extender and diisocyanate under catalyzing of a polymerization catalyst so that a prepolymer can be obtained; the prepolymer reacts with a nonionic chain extender and a part diluent to prepare an intermediate; the intermediate reacts with a silane coupling agent, and is emulsified to prepare the modified cation waterborne polyurethane emulsion. The product is a polyester type cation waterborne polyurethane high-polymer material containing hydrophilic and hydrophobic side long chains, wherein polysiloxane is embedded into a main chain of the material, a side chain is grafted with long-chain polyether and long-chain alkyl, and the silane coupling agent is connected into the tail end of the material; the film-forming ability is high, and serving as a film, the emulsion has obvious water-repellent, antifouling and easy dirt-removing abilities, is excellent in compatibility with a cation softening agent, and has an excellent low-temperature soft feature; the product is safe, environmentally friendly and convenient to use.
Owner:HUBEI DAYA BIOLOGICAL TECH CO LTD

Polymer lithium ion secondary battery and isolating membrane thereof

The invention discloses an isolating membrane of lithium ion secondary battery, comprising a porous substrate and a polymer coating distributed only on a surface of the porous substrate which faces an anode of the lithium ion secondary battery, wherein the polymer in the polymer coating is selected from poly(methyl methacrylate-acrylonitrile), poly(methyl methacrylate-vinyl acetate), poly(methyl methacrylate-acrylonitrile-vinyl acetate), poly(n-butyl methacrylate-styrene), or blends of the polymers. The polymer unit in the polymer coating of the isolating membrane of the lithium ion secondary battery contains carbonyl, wherein very strong effect exists between the carbonyl and oxygen in carbonic acid ester type organic solvent so as to have fine solution suction ability and good interface stability of lithium electrode or anode; the membrane has strong adhesive property and film formation, and can provide fine mechanical tensile strength; and the membrane has fine cycle performance and safety performance. The invention further discloses a polymer lithium ion secondary battery using the membrane.
Owner:DONGGUAN NEWPOWER ELECTRIC SCI & TECH +1

PPTA paper using aramid nanofiber for self-reinforcement and preparation method thereof

The invention discloses a PPTA paper using aramid nanofiber for self-reinforcement and a preparation method thereof. The preparation method includes: utilizing para-aramid paper nanofiber with the advantages of special nano-structure, small fiber diameter, large length-diameter ratio, high surface activity, excellent heat resistance and the like as the self-reinforcement material of para-aramid paper, conducting mixing, defibering and dispersion on aramid chopped fiber, pulp or fibrid and aramid nanofiber to make a uniform suspension, carrying out papermaking shaping, squeezing and drying, andfurther performing hot-pressing on a hot press to obtain aramid paper. The introduced aramid nanofiber enables nanoscale aramid fiber and an aramid nanofilm formed thereby to reach the good interfacefilling, coating and enhancement effects, provides more binding sites for the combination of components, at the same time reduces the pores and holes between components, significantly improves the bonding strength between the aramid paper components, and greatly enhances the mechanical and insulation properties.
Owner:SHAANXI UNIV OF SCI & TECH

Aramid paper compounded with aramid nanometer fiber thin film and preparation method thereof

The invention discloses an aramid paper compounded with an aramid nanometer fiber thin film and a preparation method thereof. The aramid paper is compounded by a surface layer, a core layer and a bottom layer through a wet type papermaking laminating method, wherein the ratio of the surface layer to the core layer to the bottom layer is (5 to 20):(60 to 90):(5 to 20) in parts by weight of absolutedry fiber; the surface layer and the bottom layer respectively adopt aramid nanometer films which are prepared from aramid nanometer fibers; the core layer adopts the aramid paper which is prepared from one of aramid chopped fibers and aramid pulp fibers or aramid precipitated fibers. The aramid paper has the advantages that because of excellent strength property and dense thin film structure ofthe aramid nanometer fiber film, more bonding sites are provided for bonding with the fiber components of the aramid paper, and the larger pores can be filled and coated; the comprehensive property ofthe final product is greatly improved, and the aramid paper is favorably widened to the high-end application field.
Owner:SHAANXI UNIV OF SCI & TECH

Novel modified emulsifying olefin concrete curing agent

ActiveCN101298373ASave labor, time and waterEasy to use in constructionParaffin waxAcrylic polymer
The invention relates to a novel modified emulsified paraffin concrete curing agent. Aiming at overcoming the defects that the existing concrete curing agent cannot reach the industrial standard on building material in terms of the water retention property and is unfavorable for environmental protection, the price is high and the decoration at later stage is also affected, the following technical proposal is provided: the curing agent is mixed with the following materials and water: 10-20% of vinyl acetate-ethene high molecular polymer emulsion, 0-5% of silicone resin modified acrylic polymer emulsion, 50-75% of paraffin emulsion, 0.1-0.5% of colloidal dispersing agent of the emulsified paraffin for stabilizing the emulsion state and 0.05-0.02% of special defoamer for emulsion. The invention has the beneficial effects that: the chemical curing method which is adopted for retaining water is an innovation for the traditional curing method; compared with the prior art, the method is labor-saving, time-saving and water-saving and is convenient to operate, can improve the film formation ability and the sealing ability of the emulsified paraffin emulsion, and can improve the bonding and absorbing capacity of the emulsified paraffin emulsion on the concrete surface, which leads the effective water retention rate of the coating film to reach more than 90%.
Owner:LIAONING BUILDING SCI RES INST

Passivator for treatment of electrolytic manganese metal surface and process for preparing same

The invention discloses a passivator and preparing method of electrolytic metal Mn surface, which comprises the following parts: 70-80 percent silicate, 0.1-0.2 percent cosolvent, 0.3-0.5 percent inhibitor, 0.05-0.1 percent accelerant and water. The invention improves the operational environment for workers, which solves the problem of serious pollution of electrolytic Mn factory.
Owner:CHINA UNIV OF GEOSCIENCES (WUHAN)

Vertical cotton breathable bra cup pad with silica gel net and preparation method thereof

The invention relates to the technical field of bra cup pad, and specifically relates to a vertical cotton breathable bra cup pad with a silica gel net and a preparation method thereof. The vertical cotton breathable bra cup pad comprises a vertical cotton outer layer and a vertical cotton inner layer; a vertical cotton interlayer is arranged between the vertical cotton outer layer and the vertical cotton inner layer; an adhesive layer is arranged between the vertical cotton interlayer and the vertical cotton inner layer; and a silica gel net layer is arranged between the vertical cotton outer layer and the vertical cotton interlayer. The vertical cotton breathable bra cup pad is prepared by a combined technology of hot pressing and cold pressing. The pad is made of vertical cotton, and is light, comfortable, and breathable. A silica gel layer is arranged between vertical cotton layers, the performance of the pad on resisting water washing is enhanced, the anti-collapse effect is good, three-dimensional effect of the cup pad is long-lasting and stable, and the deformation is difficult to happen.
Owner:HONGJI UNDERWEAR CO LTD

Water-based nano reflection and heat insulation transparent coating and preparation method thereof

The invention discloses a water-based nano reflection and heat insulation transparent coating and a preparation method thereof. The formula of the coating comprises the followings in percentages by weight: 35%-50% of a water-based acrylic emulsion, 5%-15% of water-based lithium silicate, 5%-15% of a water-based polyurethane emulsion, 5%-10% of a water-based heat insulation nano dispersion sizing agent, 5%-10% of a water-based heat insulation and heat preservation nano dispersion, 2%-12% of a wetting dispersant, 0.2%-0.5% of a flatting agent, 0.2%-1% of a thickener, 0.1%-0.2% of an antifungus and anti-mildew agent, 0.5%-2.5% of a coalescing agent, 0.5%-2% of a silane coupling agent and 5%-25% of deionized water. According to the water-based nano reflection and heat insulation transparent coating disclosed by the invention, under the precondition of without influencing lighting, heat radiation is blocked and infrared heat energy is prevented from being conducted into the interior of a base material through effective reflection and heat energy conduction, and thus the effects of heat insulation and heat preservation are reached. Heat energy, entering the room through the base material, generated by an outdoor heat source can be effectively blocked in summer, and indoor heat can be effectively blocked from being dispersed in winter, so that the application of refrigeration and heat preservation equipment can be effectively reduced, and the energy-saving effect is obvious.
Owner:CHANGSHA MINDE FIRE ENG PAINT CO LTD

Moisture curable compositions and low surface energy coating compositions made therefrom

A one-package moisture curable composition is provided. The composition comprises, by weight percentage based on the dry weight of the composition, from 10 to 99% at least one silane terminated polyurethane and from 1 to 90% at least one silane terminated polysiloxane! wherein the silane terminated polyurethane based polymer has at least one end group of the general formula^ - A-(CH2)m-SiR1 n (OR2)3-n, wherein A is a urethane or urea linkage group, R1 is selected from C1-12 alkyl, alkenyl, alkoxy, aminoalkyl, aryl and (meth)acryloxyalkyl groups, R2 is each substituted or unsubstituted C1-18 alkyl or C6-C20 aryl groups, m is an integer from 1 to 60, and n is an integer from 0 to V, and wherein the silane terminated polysiloxane can be the polysiloxane based polymer with hydrolysable silane group or the reaction products of at least one organofunctional polysiloxane and at least one organofunctional silane; and wherein the composition, after moisture cured, forms a surface whose water contact angle is larger than 101°. The composition is suitable for the applications in coatings which afford low surface energy surface and improved mechanical performance, such as marine antifouling coating, anti-icing coating, anti-stain coating, self-cleaning coating, and non-sticky coating, etc.
Owner:DOW GLOBAL TECH LLC +1

Application of polyimide in gas separation

The invention provides application of polyimide with a structure presented by a formula I (shown in the description) in gas separation. By introducing 2,2',3,3'-biphenyl tetracarboxylic acid dianhydride with a twisted structure to be polymerized with diamine monomers, polyimide with good film forming capacity is obtained. Synthesized polyimide is relatively low in cost, has relatively large specific surface area and good thermal heat stability, gas selectivity and gas permeability and further has good application prospects in the field of gas separation.
Owner:CHANGCHUN INST OF APPLIED CHEMISTRY - CHINESE ACAD OF SCI

Antibacterial wash-and-wear fire-retardant finishing liquid and finishing method thereof

The invention discloses an antibacterial wash-and-wear fire-retardant finishing liquid which is prepared from the following raw materials in parts by weight: 10-15 parts of glyoxal, 10-15 parts of citric acid, 5-8 parts of cyclic phosphate, 5-8 parts of a licorice extract, 3-5 parts of chitosan, 2-3 parts of magnesium chloride, 2-3 parts of sodium hypophosphite, 1-2 parts of a penetrant, 1-2 parts of a coupling agent, 1-2 parts of a softener, 1-2 parts of ethylene glycol, 1-2 parts of a fiber protecting agent, 1-2 parts of a pH adjusting agent and 1-2 parts of a dispersant. The prepared multifunctional antibacterial finishing liquid is environment-friendly and free of pollution, has good efficacies of being wash-and-wear, shrink-proof, antibacterial and flame-retardant, and can meet the requirements of people on various functional aspects of textiles.
Owner:SUNTEX

Preparation method of composite functional fresh-keeping paper based material with enhanced slow release function

The invention discloses a preparation method of a composite functional fresh-keeping paper based material with enhanced slow release function. The preparation method comprises following steps: 1, beta-cyclodextrin and essential oil are weighed to prepare essential oil microcapsules; 2, the essential oil microcapsules and a mesoporous molecular sieve are mixed, water is added, and high speed oscillation treatment is carried out so as to obtain a molecular sieve loaded with the essential oil microcapsules; 4, the molecular sieve loaded with the essential oil microcapsules, a starch solution, a chitosan solution, and an inorganic salt solution are mixed and stirred at a ratio, deionized water is added to adjust the solid content to be 5 to 10% so as to obtain a coating solution; 5, the surface of food package body paper is uniformly coated with the coating solution; and 6, the coated paper is dried fully at room temperature so as to obtain the functional fresh-keeping paper based material. The fresh-keeping paper prepared using the above preparation method is capable of prolonging the storage period of packaged products, and the service life of the fresh-keeping paper can be prolongedat the same time.
Owner:ZHEJIANG UNIV OF TECH

Fruit and vegetable fresh-keeping agent and preparation method thereof

The invention discloses a fruit and vegetable fresh-keeping agent and a preparation method thereof. The fruit and vegetable fresh-keeping agent comprises the following components in percentage by mass: 20-30 percent of lacquer wax emulsion, 0.5-2 percent of toxicodendron vernicifluum seed kernel oil, 45-70 percent of water, 5-15 percent of ethanol, 0.05-0.1 percent of nanometer titanium dioxide, 0.5-3 percent of propylene glycol or glycerin, 0.5-2 percent of Tween, 0.01-0.02 percent of a silane coupling agent, 1-2 percent of chitosan, 0.1-0.5 percent of acetic acid, 0.5-2 percent of maltodextrin, 0.1-1 percent of sucrose fatty acid ester and 0.5-2 percent of glycerin monostearate. The fruit and vegetable fresh-keeping agent has the advantages of high film-forming property, good emulsifying property, high stability, and good preservation property; the glossiness and commodity of fruits and vegetables coated with the fruit and vegetable fresh-keeping agent are good, and the shelf life of the fruits and the vegetables coated with the fruit and vegetable fresh-keeping agent is prolonged.
Owner:云南省轻工业科学研究院有限公司 +1

Method for producing high intensity modified starch

The present invention provides a method for producing high intensity modified starch, including a neutralization reaction, casting stock and precipitating; a clarified starch solution is sucked into a reaction tank, aqueous vapor is injected into the reaction tank, then the clarified starch solution is heated until 65 DEG C, during which agitating the solution continually to play a function of conditioning and high-temperature enzyme extinguishing, the heating and agitating time is from 20 to 40 minutes; then wood carbon dust is added to discolor and desludge; a clear starch solution will be obtained after filtering by a compressor; the impurity in the starch is removed step by step by steps of concentrating, batching and high speed centrifugation, the technique is reasonable, the high intensity modified starch has high purity and adequate quality, and the product grade is improved.
Owner:界首市鸿顺生物科技有限公司

Bacteria cellulose pervaporation membrane and uses thereof

InactiveCN101234299ASolve the problem that the thickness uniformity is difficult to controlAddressing Chemical StabilityDistillationCulture fluidMicrobiology
The invention provides a bacterial cellulose pervaporation membrane, which is characterized in that the preparation method is as follows: Acetobacter xylinum DT4.2 strain of the active wood fermentation is put into the seed culture fluid and shaking cultured at constant temperature of 25 to 32 DEG C for 8 to 24 hours; the seed solution is put into the fermentation culture solution to be evenly shaken; and then the fermentation culture solution is moved to the container for culturing for 7 to 15 days at the constant temperature of 25 to 32 DEG C; pellicle membrane formed on the surface of the fermentation solution is taken out and then is processed by the alkali liquor with the quality concentration of 1 to 20 percent; the residual alkali liquor in the membrane is washed to neutrality by the deionized water to prepare into the membrane after drying. The invention also discloses the application of the membrane. The preparation method of the membrane has the advantages of simple preparation, good mechanical and chemical property, excellent heat stability, strong hydrophilicity, high separation choice to the water in the organic water solution at lower temperature, long service life; moreover, the membrane material itself can be biodegradation which is a environmental friendly material.
Owner:许春元

Polyurethane elastic fiber finishing agent

InactiveCN101666040AGood sealing and anti-sticking effectUniform sealing and anti-stick effectFibre typesAlcoholPhosphate
The invention discloses a polyurethane elastic fiber finishing agent, comprising the following components in parts by weight: 75.0-98.8 parts of at least one substrate selected from silicon oil and white mineral oil, 1.0-10.0 parts of isomerous high-carbon alcohol, 0.1-10.0 parts of MQ silicon resin of which the pour point is smaller than or equal to 100 DEG C and 0.1-5.0 parts of trisiloxane polyether organic phosphate. The finishing agent enables the polyurethane elastic fiber to have favorable antistatic property, lubricating property and grating balancing property in the filament reeling process, so that the polyurethane elastic fibers reeling at high speed have stable tension and do not skid or cause the filament roller to mess up, thereby endowing the polyurethane elastic fibers withfavorable reeling property. The finishing agent also enables the polyurethane elastic fibers rolled on the roller to have enduring anti-adhesion insulation property, so that the polyurethane elasticfibers have favorable cocoon reelability and thorough root unreeling property in the downstream unreeling process, thereby endowing the polyurethane elastic fibers with favorable unreeling property.
Owner:HUAIAN KAIYUE TECH DEV

Production method of anti-aging convenient cooked rice

The present invention provides a production method of anti-aging convenient cooked rice and belongs to the technical field of food processing. The anti-aging convenient cooked rice is obtained by thespecific method comprising the steps of rice washing, soaking liquid soaking, sub-packaging, cooking, sterile vacuum sealing, cooling and crystallization, etc. The technologies of soaking by the liquid containing an anti-aging agent and rapid cooling are used to inhibit aging of starch and improve eating quality of starch-based staple food. The aging rate and the aging degree of the obtained convenient cooked rice are low; the aging degree of the convenient cooked rice obtained after storage for 90 days reduces by about 30% compared with that of the traditional convenient cooked rice; and theanti-aging convenient cooked rice has advantages of excellent taste quality, long shelf life, etc.
Owner:JIANGNAN UNIV

Preparation method of degradable food packaging film

The invention discloses a preparation method of a degradable food packaging film, and relates to the field of packaging films. The preparation method comprises the following steps of (1) crushing teastems; (2) extracting tea polyphenols; (3) concentrating, spraying and drying; (4) dissolving by polylactic acid; (5) mixing the raw materials; (6) removing the bubbles in the mixture; (7) preparing the biodegradable food packaging film. The preparation method has the advantages that the tea polyphenols and chitosan are extracted from the discarded tea stems and are added into the solution of polylactic acid, so that the prepared material has good antibacterial and anti-oxidizing properties; the material is degradable, green and non-toxic; after the air bubbles can be removed, the surface of the prepared package is flat, and the appearance is attractive.
Owner:HEFEI HUAGAI BIOTECH CO LTD

Collagen casing and preparation method thereof

The invention discloses a collagen casing and its preparation method. The collagen casing is composed of the following ingredients, by weight, 55-65% of collagen, 4-8% of soybean dietary fiber, 4-8% of high amylose modified starch, 0.02-0.05% of a cross-linking agent, 3-10% of a plasticizer, 0.01-0.03% of an antiseptic and 15-25% of water. The collagen casing provided by the invention has advantages of small casing thickness, smooth and crispy taste, good permeability, high tensile strength, high compression strength, high stretching rate, high temperature boiling resistance and the like. As auxiliary materials of the collagen casing are soybean dietary fiber and high amylose modified starch, the collagen casing has high safety, high nutritive value, strong film-forming property and good heat stability, is low-cost, and has a certain air permeability and moisture-penetrability. Due to the functionality, the collagen casing completely can replace other edible celluloses of synthetic chemical materials and can meet requirements of mechanical coloclysis.
Owner:INNER KIRIN CO LTD PEARL COLLAGEN CASINGS

Micro-crosslinking type poly(methacryloxyethyltrimethyl ammonium chloride) modified color fixing agent and preparation method thereof

The invention relates to the technical field of color fixing agents and provides a micro-crosslinking type poly(methacryloxyethyltrimethyl ammonium chloride) modified color fixing agent which is capable of well improving the fastness of the textile to wet rubbing and the color fastness of the textile to washing. The micro-crosslinking type poly(methacryloxyethyltrimethyl ammonium chloride) modified color fixing agent comprises the following raw material components in parts by weight: 50-60 parts of methacryloxyethyltrimethyl ammonium chloride, 0.25-5 parts of epoxy compound, 0.1-2 parts of crosslinking agent, 0.02-0.3 part of initiator and 35-45 parts of deionized water, wherein the methacryloxyethyltrimethyl ammonium chloride is a water solution with a weight percent concentration of 65-98 percent. Meanwhile, the invention provides a preparation method of the micro-crosslinking type poly(methacryloxyethyltrimethyl ammonium chloride) modified color fixing agent.
Owner:FUJIAN QINGYUAN TECH

Seed treatment agent composition having sustained release and repellent effects

The invention aims to provide a seed treatment agent composition having mouse or bird repellent effects and an application method thereof and provides a composition of a suspension concentrate for seed dressing and a sustained release repellent. The contact between seeds and chemical components is reduced to the largest extent through layered coating, the goal of driving mice or birds can be achieved while insect killing and sterilization for promoting plant growth are achieved, the goal of adding a sustained release agent is to reduce the influence of the repellent on pesticide active ingredients and avoid pesticide hazard, and the mouse and bird repellent duration of the repellent can be prolonged. The composition can be widely applied to agriculture, forestry and grassland farming seed ratproof treatment, and the blank of a seed treatment agent in the function is filled.
Owner:ZHEJIANG XINAN CHEM INDAL GROUP

Silicon or silicon alloy composite lithium ion battery negative electrode material containing lithium bis(oxalate)borate as well as preparation method and application of negative electrode material

The invention belongs to the technical field of energy materials and energy conversion and in particular relates to a silicon-based lithium ion battery composite negative electrode material, a negative electrode using the material, and a lithium ion battery. The silicon or silicon alloy composite lithium ion battery negative electrode material containing lithium bis(oxalate)borate contains 1-20 mass percent of lithium bis(oxalate)borate (LiBOB). The negative electrode material disclosed by the invention is obtained by adding lithium bis(oxalate)borate into a silicon or silicon alloy-carbon composite lithium ion battery negative electrode material, or is obtained by introducing the lithium bis(oxalate)borate in the process of preparing the battery negative electrode material. According to the battery negative electrode material, the highest first charge and discharge capacity can reach 1800-2000 mAh per gram, the capacity after 100 times of cycle can reach 1200-1500 mAh per gram, and the capacity retention ratio reaches 69-85%.
Owner:ZHEJIANG UNIV

Liquid-state mulching film taking sludge as skeleton and preparation and use methods of liquid-state mulching film

The invention belongs to the technical field of mulching films and particularly discloses a liquid-state mulching film and preparation and use methods thereof. The main technical scheme is as follows: the preparation and use methods comprise the steps of taking sludge, and adding a sterilizing agent prepared from water-dissolved trichloroisocyanuric acid, so as to deodorize and sterilize; then, adding humic acid raw powder, inorganic salts and water, mixing, stirring and homogenizing, then, grinding and reacting, so as to prepare a master batch formed by a paste body; taking polyacrylamide and derivatives thereof, lignosulfonate or / and cellulose derivatives, so as to form a sub-material with film forming, penetration, dispersion, chelation and water retention properties; during use, dissolving the sub-material by water, adding the dissolved sub-material into the master batch, stirring to prepare a porridge-like body, then, adding water, uniformly stirring and diluting, and spraying by a mist sprayer, thereby forming the mulching film. The liquid-state mulching film is prepared in a manner that the sludge serves as a main material, so that the problem of sludge treatment is basically solved, especially, the waste is changed into the valuable, and the land capability can be greatly increased; the liquid-state mulching film has the functions of increasing temperature, preserving soil moisture and promoting crop growth, the elimination of white pollution is realized, the flying dust factor of agriculture is controlled, the soil is improved, water resources are conserved, the revenue of farmers is increased, the expenditure of farmers is reduced, and the sustainable development of agriculture is promoted.
Owner:王书秀

Method for manufacturing nano titanium dioxide thin film through photocuring

The invention belongs to the technical field of functional materials and photopolymerization and relates to a method for manufacturing a nano titanium dioxide thin film through photocuring. According to the method, a nano titanium dioxide colloid and a photopolymerisable monomer material are mixed to manufacture a colloid titanium dioxide dispersoid, the colloid titanium dioxide dispersoid is coated on the surface of a base material and polymerized and curied through radiation of ultraviolet to manufacture a film, and finally, the porous nano titanium dioxide thin film is obtained by performing thermal treatment on the film. The invention also provides a method for manufacturing the porous nano titanium dioxide thin film by photocuring an organic and inorganic mixed system coating. The method accords with a '5E' principal of a photocuring technology, the morphology, the thickness, the pore dimension and the like of the thin film are regulated and controlled by changing reaction conditions such as types of a monomer and a photoinitiator, the monomer addition amount, a film coating method and the like; the manufactured porous nano titanium dioxide thin film has the advantages of high specific surface area, smooth and uniform surface, high porosity and the like and is difficultly peeled. The method can be applied to a dye-sensitized solar cell; through a porous structure, the dye adsorption capacity can be enhanced, the light scattering performance is enhanced, and the photoelectric conversion efficiency of the cell is improved; and the manufactured thin film has a high practical value and a application prospect.
Owner:BEIJING UNIV OF CHEM TECH

High-efficiency slow-release compound fertilizer containing Crotalaria pallida

The invention relates to the field of compound fertilizers, in particular to a high-efficiency slow-release compound fertilizer containing Crotalaria pallid. The fertilizer is prepared from the following raw materials by weight part: 10-15 of 1250-2000 mesh diatomite, 10-12 of calcium carbonate, 6-8 of borax, 2-3 of magnesium ascorbyl phosphate, 8-10 of disodium hydrogen phosphate, 5-6 of pyracetic acid, 10-12 of potassium bitartrate, 20-22 of urea, 25-28 of diammonium phosphate, 12-15 of crop leftover, 3-5 of plasma protein powder, 1-3 of Crotalaria pallid fine powder, 4-5 of potassium alginate, 2-4 of stearic acid, 10-12 of gelatin, 1-3 of Vaseline, 1-2 of Tween 80, 2-4 of medical stone powder, 6-8 of polymeric ferric silicate sulfate, and 4-5 of an assistant. The compound fertilizer provided by the invention utilizes diatomite and a coating agent with good slow release ability to form dual cladding on the multielement nutrients, so that the nutrients are difficult to lose, and the fertilizer efficiency can be more lasting. The Crotalaria pallid fine powder in the coating agent has certain insecticidal and antibacterial ability, provides good growing environment for crop roots, and does not destroy the soil ecological environment. The fertilizer provided by the invention can significantly improve the crop yield and quality and enhance economic benefits.
Owner:安徽红三星磷复肥有限责任公司

Cowpea seed treatment agent and treatment method thereof

The present invention discloses a cowpea seed treatment agent and a treatment method thereof. The cowpea seed treatment agent comprises the following components by weight: 0.1-5 parts of a non-photo catalyst, 0.005-0.1 part of nano-silver, 0.1-3.5 parts of antimicrobial peptides, 1-20 parts of pyroligneous liquor, 0.01-0.3 part of a surfactant and 70-80 parts of sterile water. Treatment on the cowpea seed can effectively kill the fungi and bacteria attached to cowpea seeds; a polyvinyl alcohol film containing fungicides, insecticides and water retention agent coats on the surface of cowpea seed, and through degradation of polyvinyl alcohol and the effect of water retention agent, the active ingredients in fungicides and insecticides slowly release to protect the cowpea seed from dangers of bacteria, fungi and insects for a long time.
Owner:韦永梁

Preparation method and application of label-free type electrochemical immunosensor based on MoS2/Au composite material

The invention relates to the technical field of electrochemical immune sensing and particularly relates to a preparation method and application of a label-free type electrochemical immunosensor based on a MoS2 / Au composite material. H2O2 is used as an electrochemical probe and the MoS2 / Au composite material is used as a substrate material; and the stability and sensitivity of the immunosensor are remarkably improved based on the advantages of good film-forming capability and biocompatibility, large specific surface area, and excellent catalytic properties on the H2O2 by MoS2 and the like. A detection principle utilizes the change of current before and after an antigen-antibody immune reaction. After an antigen is reacted with an antibody modified on the current, an immune compound is formed and is a non-active substance, so that a channel from an electron to the surface of an electrode is seriously hindered. Along the increasing of the concentration of the antigen, more immune compounds are formed, and the channels from the electron to the surface of the electrode are fewer, so that a current signal is reduced. The sensor is used for detecting alpha fetoprotein; and a detection linear range is 0.005ng / mL-100ng / mL and the detection limit is 2.5pg / mL.
Owner:UNIV OF JINAN

Cationic type formaldehyde-free color fixing agent for reactive dye and preparation method thereof

The invention relates to the technical field of color fixing agents, and provides a cationic type formaldehyde-free color fixing agent for reactive dye, wherein through the cationic type formaldehyde-free color fixing agent, the wet rubbing fastness and washing color fastness of textiles can be better improved. The cationic type formaldehyde-free color fixing agent for the reactive dye is prepared from, by mass, 50-60 parts of dimethyl diallyl ammonium chloride, 0.2-10 parts of monomers containing tertiary amino groups, 0.1-5 parts of cross-linking agents, 0.01-0.3 part of initiating agents and 30-48 parts of deionized water, wherein an aqueous solution with the mass percentage concentration of 60+ / -0.5% or 65+ / -0.5% is adopted as the dimethyl diallyl ammonium chloride. Meanwhile, the invention further provides a preparation method of the cationic type formaldehyde-free color fixing agent for the reactive dye.
Owner:SHISHI QINGYUAN FINE CHEM
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