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185results about How to "Improve elution" patented technology

Method for extracting and purifying cannabidiol from China-hemp

The invention belongs to the technical field of extraction and purification of plant ingredients and particularly relates to a method for extracting and purifying cannabidiol from China-hemp. In the method, an ingredient of cannabidiol is extracted from floral leaves in a mature period of the China-hemp according to a supercritical CO2 extraction technique, a cannabidiol extract is further purified by macroporous adsorbent resin and a rapid purification system, a cannabidiol content of an obtained product is 98% or higher, and the cannabidiol product does not contain a psychotoxic ingredient tetrahydrocannabinol. According to the method, a chemical organic solvent is not used in an extraction process, so that the method is environment-friendly and is low in toxicity and high in efficiency; the loss of cannabidiol in an adsorption elution process is reduced in a purification process, so that the impurity ingredients such as tetrahydrocannabinol and the like are effectively removed, and the use of an organic regent is decreased, so that the purification cost is lowered, and the environmental pollution is reduced. The product is high in yield and purity, and the requirement for development of a value-added product of the China-hemp, in particular to the market requirement of the active ingredient of the cannabidiol product in the China-hemp, can be met, and especially, the cannabidiol product has the great application advantage in the pharmaceutical field.
Owner:DAQING BRANCH OF HEILONGJIANG ACAD OF SCI

Efficient acidic oil sludge decomposing agent, and preparation method and application thereof

The invention discloses an efficient acidic oil sludge decomposing agent, comprising the following component materials in percentages by weight: 1-15% of oxidant, 1-10% of coprecipitator, 5-30% of flocculating agent, 1-10% of surfactant, 0.5-10% of emulsion breaker, 1-10% of acidity regulator and 50-90% of water. The invention further discloses a preparation method of the efficient acidic oil sludge decomposing agent. The preparation method comprises the following steps of: 1, preparing sodium carboxymethylcellulose hydrosol; 2, dissolving all kinds of component materials; and 3, adding the sodium carboxymethylcellulose hydrosol prepared in the first step into the solution obtained in the second step so as to obtain the efficient acidic oil sludge decomposing agent. The invention further discloses application of the efficient acidic oil sludge decomposing agent. The efficient acidic oil sludge decomposing agent disclosed by the invention has the advantages of simple preparation process, low cost and easy industrialization; by means of chemical reaction, surface activation action, flocculation and salting-out emulsion breaking actions, the viscosity of the oil sludge is reduced, the oil phase, the water phase and the sludge phase are effectively separated, and the efficient acidic oil sludge decomposing agent can be used for recovering the crude oil from the oil sludge and quickly treating the petroleum pollution soil.
Owner:重庆融极环保工程有限公司

Multielement ex-situ remediation equipment and method used for organo-chlorine pesticide contaminated soil

The invention discloses multielement ex-situ remediation equipment and method used for organo-chlorine pesticide contaminated soil, belongs to the technical field of materializing remediation equipment for contaminated sites. The equipment comprises a stirring device, an eluent injecting device, an eluent recovery device, an ultrasonic generator and a heater. The equipment has extremely strong remediation broad-spectrum performance for organo-chlorine pesticide site soil with different characteristics such as organo-chlorine pesticide substance types, soil contamination incidents, soil contamination concentration, soil organic matter content, soil texture and the like, and a removal rate by single or repeated continuous elution is higher (larger than or equal to 85%); the equipment can form a good matching technology with a patent eluent (ZL201010547630.2), and is developed specially aiming at solving actual contamination situation of organo-chlorine pesticide sites in our country; and during a process of manufacturing the equipment, on the basis of synergistic effects generated by multielement strengthening components such as stirring, ultrasonic, heating and the like, the parameter condition design is optimized, the distribution is scientific and reasonable, and the optimal integration of multielement strengthening components is reflected.
Owner:INST OF SOIL SCI CHINESE ACAD OF SCI

Method for extracting tea polyphenol from glede tea

The invention relates to a method for extracting tea polyphenol from glede tea, comprising the following process flows: glede tea is dried and crushed, and is screened by a 60-mesh sieve, refluxed and extracted by 80% ethanol, and pH is adjusted to be 2; then glede tea is treated by high-speed centrifugation, supernatant fluid treatment, polyamide absorption, elution, concentration, refrigeration and drying in vacuum, so as to obtain pure tea polyphenol. 80% ethanol is used to crudely extract the tea polyphenol of glede tea, and extraction rate is relatively higher than hot-water extraction rate; the pH of crude extract is adjusted to be 2, and pigment, caffeine and large-molecule substance are separated in advance by high-speed centrifugation; de-ionized water is used to adjust the concentration of the supernatant fluid to ensure low ethanol content in the supernatant fluid, which is convenient for follow-up 80% ethanol to elute tea polyphenol; polyamide has strong adsorbability to tea polyphenol, and has low cost and easy regeneration; the elution rate of 80% ethanol which is used as main eluent can reach 97.2%, and ethanol has no pollution and is safe and easy to recover. The method has simple technical process and high tea polyphenol extraction rate, and EGCG content in the pure product is higher than that in common green tea. The method has the advantages of low production cost and low energy consumption.
Owner:HEFEI UNIV OF TECH

Purification method of echinocandins antifungal drug anidulafungin

The invention discloses a purification method of echinocandins antifungal drug anidulafungi. The method comprises the following steps of: (1) preparing a dry sample: adding organic solvent in a crude product of the anidulafungin to dissolve the crude product, adding silica gel after the crude product of the anidulafungin is adequately dissolved, and uniformly mixing and drying the mixture to obtain the anidulafungin dry sample; (2) pressurizing and eluting: uniformly filling the anidulafungin dry samples in the top end of a chromatographic column with silica gel, pressurizing and eluting the chromatographic column with the anidulafungin dry samples by adding elution solvent, utilizing a high-effective liquid phase chromatography to monitor, and collecting the elution solution with the anidulafungin content being greater than 98 percent; and (3) concentrating: concentrating the elution solution with the anidulafungin content being greater than 98 percent until dryness to obtain a pure product with the anidulafungin content being greater than 98 percent. By adopting the column chromatography, simplicity in operation is realized, and the equipment cost is low; the organic solvent with low toxicity and low boiling point is adopted as the elution solution, so that the subsequent recycling treatment is simple, and the environmental pressure can be greatly reduced; and the purification separation time is short, the purification effect is good, the purification yield is high, and the purification method is applicable to industrialized mass production.
Owner:NCPC NEW DRUG RES & DEV

Method for separating component from direct-coal-liquefaction full distillate oil by utilizing solid-phase extraction method

The invention provides a method for separating a component from direct-coal-liquefaction full distillate oil by utilizing a solid-phase extraction method. The method comprises the steps of: S1, sampling and absorbing the direct-coal-liquefaction full distillate oil to be separated to a separation column which is formed by a fixed phase; S2, washing at a washing speed of 20-50 ml / min by adopting a saturated hydrocarbon eluting agent having a weight ratio of (10-50):1 to the full distillate oil and collecting a first eluent, wherein the saturated hydrocarbon eluting agent is one or more selected from a group which is composed of n-hexane, n-pentane and petroleum ether; and S3, volatilizing the saturated hydrocarbon eluting agent in the first eluent to obtain a saturated hydrocarbon component. Aiming at the special chemical composition of the direct-coal-liquefaction full distillate oil, the saturated hydrocarbon eluting agent having an excellent elution effect on saturated hydrocarbon is selected in the method; and as the saturated hydrocarbon is separated under the condition of controlling an agent-to-oil ratio and the washing speed, an ideal separation effect of the saturated hydrocarbon and aromatic hydrocarbon in the full distillate oil having high-content aromatic hydrocarbon is achieved.
Owner:CHNA ENERGY INVESTMENT CORP LTD +2

Method for simultaneously detecting multiple types of persistent organic pollutants in water body

The invention discloses a method for simultaneously detecting multiple types of persistent organic pollutants in a water body. The persistent organic pollutants comprise polychlorinated biphenyl, polybrominated diphenyl ethers and polycyclic aromatic hydrocarbon. The method comprises the following steps: (1) sample pre-treatment is conducted, specifically, a to-be-detected water sample is taken to be filtered, standard substitutions and internal standard substances of the persistent organic pollutants are added to be evenly mixed, and a pretreated water sample is obtained; (2) solid-phase extraction is conducted, specifically, the pretreated water sample is guided into a solid-phase extraction column to be subjected to solid-phase extraction, and the solid-phase extraction column is driedand eluted through eluents, namely n-hexane and acetone; (3) purification is conducted, specifically, dried eluate is purified through a Florisil column; (4) gas chromatography-mass spectrometry combined detection is conducted; and (5) the content of the persistent organic pollutants is calculated. By selecting the appropriate eluents and adopting a triple quadrupole gas chromatography-mass spectrometry combined instrument, the polychlorinated biphenyl, the poly brominated diphenyl ethers and the polycyclic aromatic hydrocarbon are simultaneously detected, the detection limits are all low, and the method has great significance in the field of persistent organic pollutant detection.
Owner:SHENZHEN ACAD OF ENVIRONMENTAL SCI

Cigarette filter with smoke odor selection function

The invention relates to a cigarette filter with a smoke odor selection function. The cigarette filter consists of a cavity-containing mouth stick and a perfuming thread/rod-containing mouth stick, which are mutually connected, wherein the cavity-containing mouth stick is formed by forming a cavity in a filter stick, and the perfuming thread/rod-containing mouth stick is formed by adding at least two perfuming thread/rods into another filter stick; a layer of hard forming paper wraps the part of the perfuming thread/rod-containing mouth stick, so that the perfuming thread/rod-containing mouth stick and the cavity-containing mouth stick are controlled to be connected during rotation so as not to be separated from each other. By the adoption of the cigarette filter, a consumer can enable the cavity to be aligned with the perfuming threads/rods through rotating the perfuming thread/rod-containing mouth stick, so that the elution function of smoke to specific odor ingredients is improved, and the content of some odor ingredient in smoke is increased to achieve the smoke odor selection purpose. Meanwhile, owing to the unique appearance, various filters with different appearances can be formed by combination, the recognition degree of the filters and the product differentiation are improved.
Owner:CHINA TOBACCO YUNNAN IND

Activation extraction separation method for fluorine and chloride ions in zinc sulfate solution

The invention relates to an activation extraction separation method for fluorine and chloride ions in a zinc sulfate solution, which comprises the following steps: acid adjustment activation: adding concentrated sulfuric acid into the zinc sulfate solution to adjust the pH value and temperature, and mixing and blending the solution with an activating agent to damage the fluorine-containing metal complexes in the solution and decompose the fluorine-containing metal complexes into free-state fluorine ions and convert into HF molecules; extraction separation: separating the fluorine and chloride ions in the activated zinc sulfate solution by use of an extraction agent to obtain an organic phase loaded with fluorine and chloride and a raffinate with low content of fluorine and chloride; raffinate purification: removing most of the extraction organic phase through multi-segment standing clarification and ultrasonic air flotation; performing deep adsorption by use of powdery active carbon to remove residual organic phase in the raffinate to obtain adsorption residue and qualified raffinate; and impurity washing and back extraction of the loaded organic phase. According to the method provided by the invention, the key reason hindering the extraction fluorine removal effect in the zinc sulfate solution as well as the crystallization and scaling in the back extraction process is found so that the different problems are simple and easy to impellent. The fluorine removal rate exceeds 60%, and the chlorine removal rate reaches about 90%. The liquid after impurity washing and the liquid after back extraction directly return to an alkali washing process of a zinc hydrometallurgy system to be comprehensively utilized.
Owner:GREENNOVO ENVIRONMENTAL TECH CO LTD

Large-volume enrichment liquid aerosol liquid sampler suitable for air microbe analysis

ActiveCN110387318AFully elutedReduce sampling efficiencyBiological material testing proceduresSingle stageDNA extraction
The invention discloses a large-volume enrichment liquid aerosol liquid sampler suitable for air microbe analysis. The large-volume enrichment liquid aerosol liquid sampler is mainly used for correlation analysis of air microbes, and can be in single-stage or multi-stage series with enrichment bottles; large-volume enrichment liquid can be filled in each enrichment bottle, the large-volume enrichment liquid aerosol liquid sampler is characterized in that the enrichment of more microbes is conducted, a gas jet column is arranged at the bottom of the sampler, an air inlet is connected with a flowmeter, aerosol firstly enters the first stage of single-stage or multi-stage enrichment bottles; if the multi-stage series enrichment bottles are arranged, the air microbes not eluting in the first stage enrichment bottle can enter the second stage enrichment bottle again or more-stage enrichment liquid after the second stage enrichment bottle is further fully eluted; and the last stage enrichment bottle of single-stage or multi-stage enrichment bottles is connected with a diaphragm vacuum pump, and the enrichment liquid of the enrichment microbes is collected from the outlets under the enrichment bottles. According to the aerosol liquid sampler, the long-term sampling without obvious microbe secondary proliferation can be realized; samples can guarantee the microbe activity and culturability, and can guarantee the high-quality DNA extraction; and the microbial concentration at sampling sites is not limited, adaptable sampling types are wide, simple and efficient, and the production cost is low.
Owner:NANKAI UNIV

Washing desalination system and method for waste incineration fly ash or kiln dust

The invention relates to a washing desalination system and method for waste incineration fly ash or kiln dust. The invention aims at providing the washing desalination system and method with multiplegrading manners, good desalination effect and low cost. The washing desalination system comprises a conveying system and multiple stages of elution systems, wherein the elution systems include a first-stage elution system, a second-stage elution system and a multi-stage elution system; the content of chlorine salt in to-be-processed fly ash or kiln dust is more than or equal to 4% and less than orequal to 10%, and the first-stage elution system is adopted when the chlorine content is more than or equal to 2% and less than or equal to 5%; the content of chlorine salt in to-be-processed fly ashor kiln dust is more than or equal to 10% and less than or equal to 20%, and the first-stage elution system and the second-stage elution system are sequentially adopted when the chlorine content is more than or equal to 5% and less than or equal to 10%; and the content of chlorine salt in to-be-processed fly ash or kiln dust is more than or equal to 20%, and the first-stage elution system, the second-stage elution system and the multi-stage elution system are sequentially adopted when the chlorine content is more than or equal to 10%.
Owner:BEIJING ZKGR ENVIRONMENTAL PROTECTION TECH CO LTD
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