Nickel electrode slurry, resistor and preparation method of resistor
A nickel electrode and resistor technology, applied in the field of electronic components, can solve problems such as weak conductivity, lower electrical performance of products, and increased cost, and achieve good electrical conductivity, reduce adverse effects, and low production costs
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[0073] In one embodiment, the preparation method of described coated nickel powder comprises the following steps:
[0074] Dissolving nickel source and boron source in a solvent, adding organic matter to prepare nickel boride organic precursor;
[0075] mixing and stirring the nickel boride organic precursor and nickel powder, evaporating the solvent, and preparing nickel powder coated with organic matter;
[0076] The organic matter is selected from one or more of perchlorethylene, polyvinyl alcohol and ethyl cellulose. Preferred is polyvinyl alcohol.
[0077] In one embodiment, the nickel source is Ni(CO) 4 , the boron source is boric acid.
[0078] Alternatively, the solvent can be acetone, which is subsequently removed by evaporation. Optionally the temperature at which the solvent is evaporated is 80°C ± 5°C.
[0079] It can be understood that after evaporating the solvent, a step of pulverizing and grinding the product is also included to adjust the size of the coat...
Embodiment 1
[0111] This embodiment provides a nickel electrode slurry, a resistor and a method for preparing the resistor, in parts by weight, the steps are as follows:
[0112] 1) Take the first nickel powder with a particle size of 0.1 μm to 1 μm, the second nickel powder with a particle size of 1 μm to 3 μm, and the third nickel powder with a particle size of 3 μm to 10 μm, and mix them in a weight ratio of 2:1.5:1 to obtain a mixture type nickel powder.
[0113] 2) In 1L of acetone, add 1L of Ni(CO) 4 and 300g of boric acid, then add 0.8L of polyvinyl alcohol, and mix thoroughly to obtain a nickel boride organic precursor, then add 800g of nickel powder, heat to 80°C, evaporate and dry to remove acetone, then pulverize and grind the product to obtain a particle size of 0.5μm~2μm nickel powder coated with organic matter.
[0114] 3) 1L of terpineol, 1L of mineral spirits and 2kg of ethyl cellulose were mixed, then heated to 90° C., and stirred at 90° C. for 2 hours to dissolve the et...
Embodiment 2
[0119] This embodiment provides a nickel electrode slurry, a resistor and a method for preparing the resistor, in parts by weight, the steps are as follows:
[0120] 1) Take the first nickel powder with a particle size of 0.1 μm to 1 μm, the second nickel powder with a particle size of 1 μm to 3 μm, and the third nickel powder with a particle size of 3 μm to 10 μm, and mix them in a weight ratio of 1:1:1 to obtain a mixture type nickel powder.
[0121] 2) In 0.8L acetone, add 1L Ni(CO) 4 and 200g of boric acid, then add 1L of polyvinyl alcohol, and mix thoroughly to obtain a nickel boride organic precursor, then add 600g of nickel powder, heat to 80°C, evaporate and remove acetone, and then pulverize and grind the product to obtain a particle size of 0.5μm~ 2μm nickel powder coated with organic matter.
[0122] 3) 1L of terpineol, 1L of mineral spirits and 2kg of ethyl cellulose were mixed, then heated to 90° C., and stirred at 90° C. for 2 hours to dissolve the ethyl cellul...
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