Pesticide micro-granule for spraying foliage in air, and preparation method and application of pesticide micro-granule

A microparticle and foliar spray technology, which is applied in the field of new pesticide formulations, can solve problems such as loss and pesticide deposition rate of less than 50%, and achieve the effect of overcoming evaporation and drift, optimizing spraying and operating parameters

Pending Publication Date: 2022-04-01
INST OF PLANT PROTECTION CHINESE ACAD OF AGRI SCI
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

For a long time, spraying pesticides on water has been widely used. After spraying from the nozzle, the fog droplets are completely exposed to the open ecological environment, and are affected by environmental factors such as wind and sun to cause evaporation and drift; fog entering the crop canopy When the droplets are deposited on the surface of the leaves, they will also collide, bounce, coalesce, roll down and lose. The pesticide deposition rate is generally less than 50%.
To this end, people have carried out a large number of experiments, demonstrations and improvements on pesticide formulations and plant protection spraying machines. Technologies such as low-altitude spraying with plant protection drones and special spray auxiliaries for flight prevention have reduced the evaporation and drift of pesticide droplets to a certain extent. , but does not change the essential characteristics of water evaporation and drift of droplets, which has become a technical bottleneck for improving the utilization rate of pesticides

Method used

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  • Pesticide micro-granule for spraying foliage in air, and preparation method and application of pesticide micro-granule
  • Pesticide micro-granule for spraying foliage in air, and preparation method and application of pesticide micro-granule
  • Pesticide micro-granule for spraying foliage in air, and preparation method and application of pesticide micro-granule

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0052] 0.5% methylamino abamectin benzoate emulsifiable microgranules: fully shear and mix the original drug containing 2.5 g methylamino abamectin benzoate and 10 g alkylphenol polyoxyethylene ether, About 37.5 g of water were slowly added under shear to form a microemulsion. 5g lignosulfonate, 5g acrylic acid-sulfonate copolymer, 15g long-chain polycarboxylate, 10g dodecyl sulfate, 5g sodium carboxymethyl cellulose, 100g urea, 50g potassium dihydrogen phosphate, 10g of soluble starch and 280g of kaolin were accurately weighed and added to a shearing kettle containing about 500g of water for shearing and mixing, and then into a sand mill for sand grinding. When the average particle size reached about 2 microns, it was transferred to the modulation kettle.

[0053] The microemulsion containing methylamino abamectin benzoate prepared above was added to the above preparation kettle under stirring conditions, sheared and mixed for about 10 minutes, and spray-dried and granulated....

Embodiment 2

[0056] 3% trioxystrobin-tebuconazole emulsifiable microgranules: fully shear and mix the original drug containing 5g trichostrobin and 10g tebuconazole, 20g alkylphenol polyoxyethylene ether and 10g N-methylpyrrolidone, evenly, About 55 g of water was slowly added under shear to form a microemulsion. 10g dodecyl sulfate, 5g sodium carboxymethyl cellulose, 100g urea, 50g potassium dihydrogen phosphate, 10g soluble starch, 280g kaolin were respectively accurately weighed and added to a shearing kettle filled with about 500g water, shearing and mixing. , and then into a sand mill for sand grinding, and when the average particle size reaches about 2 microns, spray drying and granulation are performed.

[0057]At the same time as the above spray-drying granulation, the microemulsion containing tristrobin and tebuconazole prepared above was sprayed onto the boiling microparticles in the spray-drying granulator, together with a 5% polyvinyl alcohol aqueous solution. Adjust and contr...

Embodiment 3

[0061] 0.3% dicamba emulsifiable microgranules: the original drug containing 3g dicamba and 30g lignosulfonate, 15g long-chain polycarboxylate, 15g sodium carboxymethyl cellulose, 10g soluble starch, 100g dodecyl Sodium sulfate and 800g of bentonite were respectively accurately weighed and added to a shearing kettle containing about 1000g of water, sheared and mixed, and then entered into a sand mill for sand grinding. When the average particle size reached about 2 microns, they were transferred to the modulation kettle.

[0062] Shear mixing for about 10 minutes and spray drying granulation. Adjust and control the spray drying operation parameters [specifically, refer to the prior art in the field of spray granulation technology, and those of ordinary skill in the art can realize it without paying creative work], control the granulation, the average particle size is 100 microns, and the granulation is 32 mesh (495 microns in turn). micron) and 325 mesh (47 micron) sieve, the ...

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PUM

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Abstract

The invention discloses a pesticide micro-particle agent for air foliar spraying, and a preparation method and application thereof. At least the surface of the pesticide micro-particle agent is provided with a layer emulsified when encountering water or a layer gelatinized when encountering water; the preparation method comprises the following steps: fully shearing and uniformly mixing effective components of the pesticide and a surfactant to form a microemulsion; adding water into the carrier material, shearing and mixing uniformly, and sanding or granulating to form an inner core; finally, mixing the micro-emulsion with the inner core or spraying the micro-emulsion onto the inner core to form a layer emulsified when meeting water or a layer gelatinized when meeting water on the surface of the inner core; or directly mixing, crushing, grinding, spraying, drying and granulating; the particle size of the pesticide microgranule is 0.047-0.5 mm, and the specific gravity is 0.7-1.5 g/cm < 3 >. And an interface which is emulsified or gelled when meeting water is formed on the surface of the particle, so that the particle forms effective adhesion and deposition when reaching the leaf surface of a target crop, and the bounce loss of fog drops is overcome. The problems of mixing compatibility and stability of various pesticide preparations which are mixed and used at present when various diseases and insect pests are prevented and controlled at the same time in agricultural production are effectively solved.

Description

technical field [0001] The present invention relates to the technical field of new pesticide formulations. Specifically, the invention relates to a pesticide granule for aerial foliar spraying, a preparation method and an application thereof. Background technique [0002] The use of pesticides is an important means of effectively preventing and controlling agricultural pests. For a long time, spraying pesticides on water has been widely used. After the mist droplets are sprayed from the nozzle, they are completely exposed to the open ecological environment, and are affected by environmental factors such as wind and sunlight, resulting in evaporation and drift; mist entering the crop canopy When the droplets are deposited on the leaf surface, they will also collide, bounce, coalesce, and roll off, and the pesticide deposition rate is generally less than 50%. [0003] Studies have shown that when the pesticide droplets travel to the target crop canopy, the droplet particle s...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A01N25/28A01N25/30A01N25/24A01N43/90A01P7/04A01P3/00A01P13/00A01N37/50A01N43/653A01N37/40A01N47/02A01M7/00
CPCA01N25/28A01N43/653A01N25/26A01P7/04A01M7/00A01P13/00A01P3/00A01N43/58A01N25/24A01N47/02A01N51/00A01N37/50A01N37/40A01N43/90A01N25/30
Inventor 郑丽黄啟良陆宴辉曹立冬曹冲赵鹏跃李凤敏
Owner INST OF PLANT PROTECTION CHINESE ACAD OF AGRI SCI
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