Novel compound having immune disease treatment effect and use thereof
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example 1
Synthesis of Novel Compound having Effect of Treating Immune Diseases according to the Present Invention
[0166]The novel compounds represented by chemical formulas in the following Table 1 were prepared by a method of the following reaction formula. In detail, first, in a sealed reactor, an aniline compound of 1.0 mmol was dissolved in an acetonitrile solvent and then added with 1.0 mmol dicyandiamide and 1.0 mmol concentrated sulfuric acid, sealed, and stirred for 1 hr at 175° C. Thereafter, the solution was cooled at room temperature to produce a white solid and washed by hexane and isopropyl alcohol after the solvent was removed to synthesize the following compounds having a white solid form.
[0167]In processes for synthesizing a total of 24 compounds, other compounds except for an aniline compound were synthesized under the same condition, and a kind of aniline used for the synthesis of each compound and chemical names and structural formulas of the synthesized compounds are as di...
experimental example 1
Analysis Result of Cytotoxicity of Novel Compounds according to the Present Invention
[0189]In order to verify whether the novel compounds synthesized in Example 1 have the cytotoxicity, a cell survival rate was verified through the MTT assay by targeting cells in each test group disclosed in Table 3 above. That is, the cells of each test group were divided according to the number of 2×105 cells per well and treated with the novel synthesized compounds of the present invention for each concentration, and the cell survival rate was analyzed.
[0190]As a result, in SD-281, SD-282, SD-283, and SD-284 compounds, it can be seen that when compared with a control group or a metformin-treated group, the cytotoxicity was not observed according to treatment for each cell concentration and the compounds had no cytotoxicity according to normal cells and disease-group cells.
experimental example 2
[0191]Result of Effect on Autoantibody Production and Immune Response Regulation of Novel Compounds according to the Present Invention
[0192]In order to examine an effect on an immune response by producing auto-antibodies of the novel compounds synthesized in Example 1, the blood was obtained from each mouse group through orbital bleeding from mice in the four groups described above and the serum was isolated from the blood, and the amount of IgG, IgG1, and IgG2a was measured.
[0193]As a result, in the compounds of the present invention, it was shown that the amount of immunoglobulin (total IgG, IgG1, and IgG2) which was in the auto-antibody production state under the disease condition was reduced for each processing concentration of the compound, and it can be seen that in compounds disclosed in the following Table 4, an immunoregulatory function of inhibiting excessive immune response was excellent.
TABLE 4Total IgGIgG1IgG2ABCABCABCControl1183.2141.5311.4286422.3103.2109.6151.9groupS...
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