Method for preparing graphite series nano fluid
A nanofluid and graphite technology, applied in chemical instruments and methods, heat exchange materials, etc., can solve problems such as general thermal conductivity, wear and corrosion of heat exchangers, achieve good product stability, improve thermal conductivity, and source of raw materials wide effect
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Embodiment 1
[0019] (1) Oxidation of graphite: 100 grams of natural graphite powder and 50 grams of sodium nitrate are added to 4000 grams of 98% concentrated sulfuric acid cooled to 0°C, and after mixing, add 300 grams of potassium permanganate under stirring, and the temperature during the feeding process Control the temperature below 10°C, continue to stir for 30 minutes after the addition is complete, add 4500 grams of water, increase the temperature to 98°C, maintain at this temperature for 15 minutes, and then add 7000 grams of 40°C water and 210 grams of hydrogen peroxide, mix well and take advantage of Hot filter, wash the filter cake with water until there is no sulfate ion in the filtrate, and finally the filter cake is vacuum dried at 50°C to obtain graphite oxide;
[0020] (2) Surface modification: Use 100 grams of graphite oxide obtained in step (1) to contain 10 grams of polystyrene sodium sulfonate, 4 grams of polyvinylpyrrolidone, 4 grams of sodium polynaphthalene sulfonate, an...
Embodiment 2
[0023] (1) Oxidation of graphite: 100 grams of natural graphite powder and 20 grams of sodium nitrate are added to 1000 grams of 98% concentrated sulfuric acid cooled to 0℃, and after mixing, add 100 grams of potassium permanganate under stirring. The temperature during the addition Control the temperature below 10°C, continue stirring for 10 minutes after the addition is complete, add 1000 grams of water to increase the temperature to 60°C, maintain at this temperature for 30 minutes, then add 4000 grams of 40°C water and 120 grams of hydrogen peroxide, mix well and take advantage of Hot filter, wash the filter cake with water until there is no sulfate ion in the filtrate, and finally the filter cake is vacuum dried at 50°C to obtain graphite oxide;
[0024] (2) Surface modification: Use 100 grams of graphite oxide obtained in step (1) with 5 grams of sodium polystyrene sulfonate, 3 grams of sodium polynaphthalene sulfonate, 1 gram of polyvinylpyrrolidone, 1 gram of maleic acid a...
Embodiment 3
[0027] (1) Oxidation of graphite: 100 grams of natural graphite powder and 30 grams of sodium nitrate are added to 3000 grams of 98% concentrated sulfuric acid cooled to 0℃, and after mixing, add 200 grams of potassium permanganate under stirring, and the temperature during the feeding process Control the temperature below 10°C, continue to stir for 30 minutes after the addition is complete, add 2000 grams of water, increase the temperature to 90°C, maintain at this temperature for 30 minutes, then add 4000 grams of 40°C water and 90 grams of hydrogen peroxide, mix well and take the Hot filter, wash the filter cake with water until there is no sulfate ion in the filtrate, and finally the filter cake is vacuum dried at 70°C to obtain graphite oxide;
[0028] (2) Surface modification: Use 100 grams of graphite oxide obtained in step (1) with 8 grams of sodium polystyrene sulfonate, 1 gram of sodium polynaphthalene sulfonate, 1 gram of acrylamide copolymer, and 1 gram of polyethylene...
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