Rock core microscopic various light spectrum image-forming information comprehensive processing method

A spectral imaging and information synthesis technology, applied in color/spectral characteristic measurement, fluorescence/phosphorescence, Raman scattering, etc., can solve problems such as unseen reports, metamerism, and inability to understand rock distribution, and achieve high practicality value effect

Active Publication Date: 2009-01-07
BC P INC CHINA NAT PETROLEUM CORP +1
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Problems solved by technology

For example, conventional fluorescence detection, simultaneous fluorescence spectrum analysis, and three-dimensional fluorescence spectrum analysis in oil logging technology have certain limitations in the fluorescence analysis of core samples: usually, the petroleum hydrocarbons in the core are extracted in advance with a certain solvent substances, and their fluorescence spectroscopic analysis
This method destroys the original appearance of the rock, and cannot understand the important information necessary for evaluating oil, gas and water layers, such as the fabric information of the rock and the distribution of hydrocarbons in the rock; while the currently used fluorescence logging microscopic image Although the technology can more accurately observe the structure of the core and the distribution of hydrocarbon fluorescence, it still relies on the perception of the color and intensity of the fluorescence by the human eye or a true-color camera. This analysis method based on human color vision is not a complete spectrum analysis method. method, there is a fundamental shortcoming of metamerism, in order to obtain correct results, it is necessary to collect enough samples and establish a physical model
Similar to the fluorescence spectrum microprobe, in the existing work of infrared and Raman spectroscopic microprobe methods to study carbonaceous matter in rock cores, the experimental research is usually limited to tiny samples separated by complicated processing (such as cheese root) or individual sites in the sample, lack of research on the spatial distribution and interrelationship of components (or groups) in complex samples
In particular, methods for the unified and comprehensive analysis of microfluorescence, infrared, and Raman spectral imaging measurements of core samples have not been reported so far
This situation is far from meeting the needs of the further development of petroleum geological exploration logging technology.

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  • Rock core microscopic various light spectrum image-forming information comprehensive processing method
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  • Rock core microscopic various light spectrum image-forming information comprehensive processing method

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Embodiment Construction

[0009] The present invention will be described in detail below in conjunction with the examples.

[0010] The core samples used for the measurement were prepared in advance in accordance with the national petroleum and natural gas industry standard SY / T5913-2004 "rock slicing method" to make a light sheet (thickness 30 microns) and stick it on a glass slide. The following three spectral imaging methods were used respectively:

[0011] 1. Fluorescence microspectral imaging experiment: using a fluorescence microscope, when the light source is an ultra-high pressure mercury lamp, the excitation filter is configured as BG12 (2mm), and its central transmission wavelength is about 405nm, while the emission cut-off filter is configured For JB510, only fluorescence with a wavelength greater than 510nm can pass through. In order to facilitate the popularization of this method, the combination of the above two filters is selected for the higher fluorescence excitation and emission effic...

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Abstract

The invention discloses a comprehensive processing method of multi-spectral imaging information of core microscopy, which is used for comprehensively analyzing and processing the multi-spectral imaging data of the microscopic fluorescence, infrared and Raman of the core with oil in the geological logging of oil. At first, the color image of full color light of the polished section of the core is acquired with the fluorescence microscope; the three-spectral imaging analysis system of the microscopic fluorescence, infrared and Raman is then used for measuring the core sample in the geological logging to acquire the corresponding imaging ''spectral cube'' or spectral ''image cube''; the pixel level blending technology is used for data processing and comprehensive analysis of the three-spectral imaging information; a DWT is used for transforming; noise in the image is eliminated; the sub-images of each level are blended in a weighing way; the DWT is used for inverse transformation to acquire the blended multi-spectral image. The experiment has proven that the data blending technology of the spectral information of the image formed by multi microscopic spectra has higher practical value in the mineralogy, petrology and geochemistry of the core, when compared with each independent spectral imaging method.

Description

Technical field: [0001] The invention belongs to the technical field of petroleum geological exploration mud logging, in particular to a comprehensive analysis technique and method for the measurement and results of microscopic fluorescence, infrared and Raman spectral imaging of oil-bearing cores. Background technique: [0002] Mineralogical, petrological and geochemical research methods begin with observing, describing and identifying objects of interest. The classical techniques commonly used are optical microscopy and X-ray diffraction, supplemented by scanning or transmission electron microscopy and electron and ion beam analysis. However, these assays cannot distinguish between isoforms or determine partial order. Therefore, there is a need for an alternative microbeam approach that can both generate molecular fingerprints of samples and be used to study complex samples containing crystalline and amorphous materials. However, the spectroscopic (infrared, Raman, and f...

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N21/64G01N21/27G01N21/65
Inventor 黄乔松李静
Owner BC P INC CHINA NAT PETROLEUM CORP
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