Method for separating sodium fluoride crystals from silicon dioxide
A silica and separation method technology, applied in the direction of alkali metal fluoride, silicate, alkali metal silicate, etc., can solve the problems such as the difficulty of separating sodium fluoride and silica, achieve small investment and improve utilization rate, reduce the effect of process loss
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[0021] Example 1
[0022] Equipped with heating device, stirring device, concentration device, weigh 482g solid sodium carbonate, add 1100g process water to make a 30% solution, heat to 85℃, press Na 2 SiF 6 : Na 2 CO 3 =1:1.05~1.1 for batching, slowly adding 400g of solid sodium fluorosilicate, the feeding time is 30 minutes, and the reaction is continued for 30 minutes at a temperature of 93°C. Add sodium hydroxide solution, the NaOH addition amount is 35% of the theoretical amount by molar ratio. Weigh 58g solid NaOH and prepare a 50% solution, slowly add it to the above solution, and continue the reaction for 30 minutes. Filter and wash the sodium fluoride filter cake with 600g hot water to obtain a wet filter cake and dry it in an oven at 120°C for 2 hours to obtain 494g of finished sodium fluoride with a product yield of 92%. The standard analysis results of the product fully meet the GB4293-84 standard First-class product requirements.
[0023] Filtrate contains SiO 2 11.4...
Example Embodiment
[0024] Example 2
[0025] Equipped with heating device, stirring device, concentration device, weigh 482g solid sodium carbonate, add 1100g process water to make a 30% solution, heat to 85℃, press Na 2 SiF 6 : Na 2 CO 3 =1:1.05 for batching, slowly adding 400 g of solid sodium fluorosilicate, the feeding time is 30 minutes, and the reaction is continued for 30 minutes at a temperature of 93°C. Add sodium hydroxide solution, the NaOH addition amount is 35% of the theoretical amount by molar ratio. Weigh 58g solid NaOH and prepare a 50% solution, slowly add it to the above solution, and continue the reaction for 30 minutes. Filter and wash the sodium fluoride filter cake with 600g hot water to obtain a wet filter cake and dry it in an oven at 120°C for 2 hours to obtain 494g of finished sodium fluoride with a product yield of 92%. The standard analysis results of the product fully meet the GB4293-84 standard First-class product requirements.
[0026] Filtrate contains SiO 2 11.46%,...
Example Embodiment
[0027] Example 3
[0028] Equipped with heating device, stirring device, concentration device, weigh 482g solid sodium carbonate, add 1417g process water to make a 25% solution, heat up to 85℃, press Na 2 SiF 6 : Na 2 CO 3 =1:1.05~1.1 for batching, slowly adding 400g of solid sodium fluorosilicate, the feeding time is 30 minutes, and the reaction is continued for 30 minutes at a temperature of 93°C. Add sodium hydroxide solution, NaOH adding amount is 40% of the theoretical amount. Weigh 67g of solid NaOH and prepare a 50% solution, slowly add it to the above solution, and continue the reaction for 30 minutes. Filter and wash the sodium fluoride filter cake with 600g of hot water to obtain a wet filter cake and dry it in an oven at 120°C to obtain 483g of finished sodium fluoride with a product yield of 90%. The standard analysis results of the product fully reach the GB4293-84 standard level 1 Product requirements.
[0029] Filtrate contains SiO 2 12.43%, Na 2 O5.21%, density 1.1...
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